Difference between revisions of "Colorimetric reagent results"
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− | + | Reagent - Color(->Changing color) - (Medium) - (Reference) | |
− | + | Classic psychedelics and naturally found entheogens: | |
− | + | DMT | |
− | + | α-Nitroso-β-naphthol-nitrous acid - Negative - (silica gel) - (23) | |
- Weak brown (on paper) - (18 ) | - Weak brown (on paper) - (18 ) | ||
[b]Chloranil[/b] - No Reaction - (silica gel) - ( 8 ) | [b]Chloranil[/b] - No Reaction - (silica gel) - ( 8 ) |
Revision as of 17:02, 22 October 2011
Reagent - Color(->Changing color) - (Medium) - (Reference)
Classic psychedelics and naturally found entheogens:
DMT α-Nitroso-β-naphthol-nitrous acid - Negative - (silica gel) - (23)
- Weak brown (on paper) - (18 )
[b]Chloranil[/b] - No Reaction - (silica gel) - ( 8 ) [b]CNTF[/b] - Gray (light) - (silica gel) - ( 8 ) [b]Diazotized p-Nitroaniline[/b] - Very weak yellow - (on paper) - (18 ) [b]Dragendorff's[/b] - positive with spray - (silical gel) - (5)
- Red-Brown - (paper) - (18 ) - Orange - (silica gel) - (23)
[b]Ehrlich[/b] - Reddish purple - (as acetate on paper) - (26) [b]Fluoranil[/b] - Purple - (silica gel) - ( 8 ) [b]Fluorescence with PENE[/b] - Violet under 254nm UV - (silica gel with PENE) - (24) [b]HNS[/b] - No reaction - (silica gel) - ( 8 ) [b]HNO3 atmosphere[/b] - yellow - (silica gel) - (25) [b]Iodine vapor[/b] - Red-Brown - (paper) - (18 ) [b]Iodoplatinate[/b] - Purple - (silica gel) - (25)
- Blue (silica gel) - (17)
[b]Iodoplatinate, acidified[/b] - Positive - (silica gel) - (5) [b]Marquis[/b] - Yellow - (NA) - (13) [b]Marquis[/b] - GreenYellow - (silica gel) - (7) [b]Marquis[/b] - Orange->red - (NA) - (5) [b]Mecke[/b] - Brown->red over time time. - (NA) - (13) [b]Mandellin[/b] - yellow - (NA) - (13) [b]Ninhydrin, acetic acid[/b] - No UV fluorescence - (acetate on paper) - (26)
- No visible color - (acetate on paper) - (26)
[b]NNCD[/b] - Weak orange - (on paper) - (19) [b]p-DMAB, ethanol:sulphuric[/b] - Red solution, Violet when diluted with water - (5) [b]p-DMAB-TS[/b] - Yellow - (pure compound) - (3, 27) [b]p-DMAB, ethanolic[/b] - Purple - (pure compound) - (3) [b]TACOT[/b] - Purple (light) - (silica gel) - ( 8 ) [b]TCBI[/b] - Brown-green - (silica gel) - ( 8 ) [b]TCNE[/b] - Brown (light and fading) - (silica gel) - ( 8 ) [b]TetNF[/b] - Brown (light) - (silica gel) - ( 8 ) [b]TNB[/b] - Yellow->Brown - (silica gel) - ( 8 ) [b]TNF[/b] - Brown (light) - (silica gel) - ( 8 ) [b]Van Urk[/b] - Blue - (silica treated with 0.1M KOH) - (16) [b]Xanthydrol[/b] - Purple - (silica gel & celulose) - (15)
- Purple - (tlc & on paper) - (5, 20) - Pink - (on paper) - (21) - Lavender - (on paper) - (22)
[size=6][color=red]
[b]5-MeO-DMT[/b][/color][/size]
[b]Acid-Induced Fluorescence[/b] - Bright Yellow under 254nm UV - (Avicel) - (28 )
[b]Chloranil[/b] - No reaction - (Silica gel) - ( 8 )
[b]CNTNF[/b] - Gray - (Silica gel) - ( 8 )
[b]Dragendorff[/b] - Red-brown - (Paper) - (18 )
- Orange precipitate - (ethanol solution) - (31)
[b]Echtrotsalz B[/b] - Light brown-yellow - (Paper) - (30) [b]Ehrlich[/b] - Royal blue - (Silica gel and cellulose) - (15)
- Dark blue - (Paper) - (18 )
[b]Fluoranil[/b] - Purple - (Silica gel) - ( 8 ) [b]Fluorescence with PENE[/b] - Pale yellow under 254nm UV - (Silica gel) - (24) [b]Gibbs[/b] - No reaction - (Paper) - (30) [b]HNS[/b] - No reaction - (Silica gel) - ( 8 ) [b]Iodine vapor[/b] - Red-brown - (Paper) - (18 ) [b]Marquis[/b] - Orange [b]Mecke[/b] - Red/Brown [b]Mandellin[/b] - Yellow [b]NNCD[/b] - Orange brown - (Paper or TLC) - (30) [b]p-DMAB-TS[/b] - Yellow->Green->Blue - (NA) - (3) [b]p-DMAB[/b] - Blue - (Paper) - (29)
- Blue - (Paper or TLC) - (30)
[b]Pauly[/b] - Light olive yelow - (Paper) - (30) [b]TACOT[/b] - Purple (light) - (Silica gel) - ( 8 ) [b]TCNE[/b] - Green (light and fading - (Silica gel) - ( 8 ) [b]TetNF[/b] - Purple (light) - (Silica gel) - ( 8 ) [b]TNB[/b] - Yellow -> Brown - (Silica gel) - ( 8 ) [b]TNF[/b] - Brown (light) - (Silica gel) - ( 8 ) [b]Van Urk-Salkowski[/b] - Blue (Cornflower blue) - (In ethanol solution) - (31) [b]Xanthydrol[/b] - Blue - (Silica gel & cellulose) - (15)
- Blue - (Paper) - (22)
[color=red][size=6][b]NMT[/b][/size][/color]
[b]Chloranil[/b] - light gray
[b]TNB[/b] - light yellow
[b]TACOT[/b] - pink
[b]Sodium Nitroprusside[/b] - Purple - NA
[size=6][color=red][b]Mescaline HCl:[/b][/color][/size] [b]Marquis[/b] - Strong orange - (chloroform solution) - (2) [b]Mandelin[/b] - Dark yellowish brown - (chloroform solution) - (2) [b]Nitric Acid[/b] - Dark red [b]Mecke[/b] - Moderate olive
[size=6][color=red][b]LSD[/b][/color][/size] [b]Nitric Acid[/b] - Strong Brown - (chloroform solution) - (2) [b]Ethanolic P-DMAB[/b] - Deep Purple - (chloroform solution) - (2) [b]Methanol P-DMAB with Ortophosphoric acid[/b] - Blue to Purple - (methanol solution) - (10) [b]Froede Reagent[/b] - Moderate yellow green - (chloroform solution) - (2) [b]Mecke[/b] - Greenish black - (chloroform solution) - (2) [b]Marquis[/b] - Brown->violet - (NA) - (5) [b]Marquis[/b] - Black - (NA) - (6) [b]Marquis[/b] - Olive black - (chloroform solution) - (2) [b]Marquis[/b] - Grey - (silica gel) - (7) [b]Nitric acid[/b] - Strong Brown - (chloroform solution) - (2)
[size=6][color=red][b]Psilocybin[/b][/color][/size] [b]Keller test[/b] - red-violet [b]p-DMAB-TS[/b] - Yellow-green - (NA) - (3) [b]Ethanolic p-DMAB[/b] - Purple - (NA) - (3) [b]Mecke[/b] - Yellow-green->brown - (NA) -
[size=6][color=red][b]Psilocin[/b][/color][/size] [b]Keller test[/b] - Olive green [b]p-DMAB-TS[/b] - Brown - (NA) - (3) [b]Ethanolic p-DMAB[/b] - Deep blue - (NA) - (3)
[size=6][color=red][b]Bufotenine[/b][/color][/size] [b]p-DMAB-TS[/b] - Green - (NA) - (3) [b]Ethanolic p-DMAB[/b] - Blue - (NA) - (3)
[size=6][color=red][b]Ibogaine[/b][/color][/size] [b]p-DMAB-TS[/b] - Yellow-green - (NA) - (3) [b]Ethanolic p-DMAB[/b] - Green-blue - (NA) - (3) [b]Mandelin[/b] - Grey->Violet - (NA) - (5)
[size=6][color=red][b]THC[/b][/color][/size] [b]Modified Duquenois-Levine Reagent[/b] - Purplish blue - (NA) - (3)
[size=7][u][b]Harmalas[/b][/u][/size]
[size=6][color=red][b]Harman[/b][/color][/size] [b]Mandelin[/b] - Green - (NA) - (5)
[size=6][color=red][b]Norharman[/b][/color][/size] [b]Mandelin[/b] - Green->yellow - (NA) - (5) [color=red] [size=6][b]Harmine[/b][/size][/color] [b]Mandelin[/b] - Blue-green - (NA) - (5) [b]Marquis[/b] - Orange->Violet - (NA) - (5)
[u][size=7][b]Synthetic tryptamines[/b][/size][/u] [size=6][color=red] [b]4-AcO-DMT[/b][/color][/size] [b]Marquis[/b] - grey-green, white precipitate forming over time. [b]Mecke[/b] - Brown/black [b]Mandellin[/b] - yellow/orange [b]p-DMAB-TS[/b] - light brown - (NA) - (4)
[size=6][color=red][b]4-AcO-DiPT[/b][/color][/size] [b]Marquis[/b] - yellow [b]Mecke[/b] - Brown/Black. [b]Mandellin[/b] - orange [b]p-DMAB-TS[/b] - Brown - (NA) - (4)
[size=6][color=red][b]4-HO-MiPT[/b][/color][/size] [b]Marquis[/b] - grey/green [b]Mecke[/b] - Brown [b]Mandellin[/b] - brown/orange
[size=6][color=red][b]4-HO-MET[/b][/color][/size] [b]p-DMAB-TS[/b] - Brown - (NA) - (3)
[size=6][color=red][b]5-MeO-MiPT[/b][/color][/size] [b]Marquis[/b] - yellow to black [b]Mecke[/b] - Red/Brown [b]Mandellin[/b] - yellow [b]Ehrlich[/b] (ethanolic p-DMAB?)- Purple to light blue
[size=6][color=red][b]5-MeO-DiPT HCL[/b][/color][/size] [b]Marquis[/b] - Yellow To black [b]p-DMAB-TS[/b] - yellow-green-blue - (NA) - (4)
[size=6][color=red][b]4-HO-DALT[/b][/color][/size] [b]Marquis[/b] - yellow, white precipitate over time [b]Mecke[/b] - Brown [b]Mandellin[/b] - orange
[size=6][color=red][b]5-MeO-DALT[/b][/color][/size] [b]Marquis[/b] - slight yellow [b]Mecke[/b] - Red/Brown [b]Mandellin[/b] - yellow
[size=6][color=red][b]4-MeO-PCP[/b][/color][/size] [b]Marquis[/b] - no change [b]Mecke[/b] - very slight brown [b]Mandellin[/b] - very slight yellow
[size=6][color=red][b]5-MeO-AMT HCl[/b][/color][/size] [b]Marquis[/b] - Yellow to Black [b]Ehrlichs (ethanolic p-DMAB?)[/b] - Purple to Blue [b]Sodium Nitroprusside[/b] - Cherry Red
[size=6][color=red][b]AMT[/b][/color][/size] [b]Sodium Nitroprusside[/b] - Purple [b]p-DMAB-TS[/b] - Yellow - (NA) - (4) [b]Mandelin[/b] - Green->Orange - (NA) - (5)
[size=6][color=red][b]DiPT[/b][/color][/size] [b]p-DMAB-TS[/b] - Yellow - (NA) - (4)
[size=6][color=red][b]DPT HCl[/b][/color][/size] [b]Marquis[/b] - Yellow [b]Ehrlich[/b] (ethanolic p-DMAB ?) - Violet [b]p-DMAB-TS[/b] - Yellow - (NA) - (4)
[size=6][color=red][b]DET[/b][/color][/size] [b]p-DMAB-TS[/b] - Yellow - (NA) - (3) [b]ethanolic p-DMAB[/b] - Purple - (NA) - (3) [b]Marquis[/b] - Yellow->Brown - (NA) - (5)
[size=7][u][b]Synthetic Phenethylamines[/b][/u][/size]
[size=6][color=red][b]DOB:[/b][/color][/size] [b]Marquis[/b] - Bright yellow/green [b]Simons[/b] - No reaction [b]Chens[/b] - No reaction - (NA) - (1) [b]Gallic Acid[/b] - No reaction
[size=6][color=red][b]DOC[/b][/color][/size] [b]Marquis[/b] - Dark green [b]Simons[/b] - No reaction [b]Chens[/b] - No reaction - (NA) - (1) [b]Gallic Acid[/b] - No reaction - (NA) - (1)
[size=6][color=red][b]DOI[/b][/color][/size] Marquis - Dark green Simons - No reaction Chens - No reaction - (NA) - (1) Gallic Acid - No reaction - (NA) - (1) p-DMAB-TS - Dark green - (NA) - (4)
[size=6][color=red][b]DOM:[/b][/color][/size] Marquis - Bright yellow/green Simons - No reaction Chens - No reaction - (NA) - (1) Gallic Acid - No reaction - (NA) - (1) p-DMAB-TS - Light yellow - (NA) - (4)
[size=6][color=red][b]MDMA:[/b][/color][/size] Marquis - Dark purple->Black Simons - Dark blue Chens - No reaction - (NA) - (1) Gallic Acid - Green - (NA) - (1)
[size=6][color=red][b]Amphetamine:[/b][/color][/size] Mandelin - Moderate bluish green Marquis - Strong reddish orange Simons - No reaction Chens - No reaction - (NA) - (1) Gallic Acid - No reaction - (NA) - (1)
[size=6][color=red][b]Methamphetamine:[/b][/color][/size] Mandelin - Dark yellowish green Marquis - Deep reddish orange Simons - Dark blue Chens - No reaction - (NA) - (1) Gallic Acid - No reaction - (NA) - (1)
[size=6][color=red][b]MDA[/b][/color][/size] Marquis - Dark Blue/Black Nitric Acid - Light greenish yellow Froede Reagent - greenish black Mecke - Very dark bluish green Gallic acid - green Mandelin - green->blue - (NA) - (5)
[size=6][color=red][b]n,n-DimethylAmphetamine[/b][/color][/size] Marquis - Orange/Brown Simons - No reaction Chens - No reaction - (NA) - (1) Gallic Acid - No reaction - (NA) - (1)
[size=6][color=red][b]PMA[/b][/color][/size] Marquis - No reaction to green Simons - No reaction Chens - No reaction - (NA) - (1) Gallic Acid - No reaction - (NA) - (1)
[size=6][color=red][b]TMA[/b][/color][/size] Marquis - Orange/red Simons - No reaction Chens - No reaction - (NA) - (1) Gallic Acid - No reaction - (NA) - (1)
[size=6][color=red][b]4-Flouroamphetamine:[/b][/color][/size] Marquis - no reaction Mecke - no reaction Mandellin - no reaction Robadope - Positive Simons - Negative
[size=6][color=red][b]2C-C:[/b][/color][/size]
Marquis - yellow, changing to light green, and then fading over time
Mecke - yellow/brown/green, green fades over time
Mandellin - clear
Simons - No reaction
Chens - No reaction - (NA) - (1)
Gallic Acid - No reaction - (NA) - (1)
[size=6][color=red][b]2C-B:[/b][/color][/size] Marquis - yellow, changing to green, and then fading over time Mecke - yellow/brown Mandellin - yellow fading to clear Simons - No reaction Chens - No reaction - (NA) - (1) Gallic Acid - No reaction - (NA) - (1)
[size=6][color=red][b]2C-I:[/b][/color][/size] Marquis - Dark green - (NA) - (1) Marquis - Green-blue with yellow edges, fades to blue, fades over time Mecke - dark brown, very fast Mandellin - clear Simons - No reaction Chens - No reaction - (NA) - (1) Gallic Acid - No reaction - (NA) - (1)
[size=6][color=red][b]2C-D:[/b][/color][/size] Marquis - Very faint brown/pink, fading to clear. Mecke - Yellow-brown fading to reddish brown Mandellin - Yellow w/tinge of green fades to clear over time
[size=6][color=red][b]2C-E:[/b][/color][/size] Marquis - Very faint brown, fading to clear. Mecke - Dark brown Mandellin - Yellow w/tinge of green fades to clear over time p-DMAB-TS - Light green - (NA) - (4)
[size=6][color=red][b]2C-P:[/b][/color][/size] Marquis - Very faint brown, fading to clear. Mecke - Yellow-brown fading to Rusty Brown Mandellin - Yellow w/tinge of green fades to clear over time Slow reactions.
[size=6][color=red][b]2C-T-2:[/b][/color][/size] Marquis - Slight brown/orange. Mecke - Black/dark purple fading to orangy-red Mandellin - Orange fading to clear over time Simons - No reaction Chens - No reaction - (NA) - (1) Gallic Acid - No reaction - (NA) - (1) p-DMAB-TS - Light pink - (NA) - (4)
[size=6][color=red][b]2C-T-4:[/b][/color][/size] Marquis - Almost no reaction, slight brown. Mecke - Black/dark purple fading to reddish-orange Mandellin - Orange fading to clear over time
[size=6][color=red][b]2C-T-7:[/b][/color][/size] Marquis - Almost no reaction, slight brown. Mecke - Black/dark purple, fading slowly if at all. Mandellin - Orange fading to clear over time
[size=6][color=red][b]2C-T-21:[/b][/color][/size] Marquis - Pink Mecke - Purple Simons - No reaction Chens - No reaction - (NA) - (1) Gallic Acid - No reaction - (NA) - (1)
[size=7][u][b]Synthetic Dissociatives:[/b][/u][/size]
[size=6][color=red][b]DXM:[/b][/color][/size] Marquis - Grey to Black (releases smoke) Mecke - Yellow
[size=6][color=red][b]Ketamine:[/b][/color][/size] Mandelin - Orange
[u][size=7][b]Synthetic Cannabinoids:[/b][/size][/u]
[size=6][color=red][b]JWH-018, JWH-073, JWH-081[/b][/color][/size] Marquis - Yellow quickly changing to brown Mecke - Brown/Yellow Mandellin - Dark brown
[size=6][color=red][b]JWH-200[/b][/color][/size] Marquis - Yellow/orange Mecke - Yellow Mandellin - Dark red-brown
[size=6][color=red][b]JWH-250[/b][/color][/size] Marquis - Red, fading to orange over time Mecke - Orange Mandellin - Dark grey-brown
[size=6][color=red][b]AM-694[/b][/color][/size] Marquis - Brown/yellow, hints of green Mecke - grey/brown Mandellin - Dark red-brown
[size=6][color=red][b]CP-47,497[/b][/color][/size] Marquis - Red/orange Mecke - Blue, fading over time. Mandellin - Brown
[size=6][color=red][b]CP-55,940[/b][/color][/size] Marquis - red/orange Mecke - Blue-green, fading over time Mandellin - Brown
[u][size=7][b]Other synthetic substances/RCs[/b][/size][/u]
[size=6][color=red][b]Naphyrone[/b][/color][/size] Marquis - yellow Mecke - no reaction (kept the brownish color it had out of bottle) Mandellin - Clear Robadope - Negative Simons - Negative
[size=6][color=red][b]Cathinone[/b][/color][/size] Marquis - No reaction Simons - No reaction Chens - Yellow/orange - (NA) - (1) Gallic Acid - No reaction - (NA) - (1)
[size=6][color=red][b]Methcathinone[/b][/color][/size] Marquis - No reaction Simons - Light blue Chens - orange - (NA) - (1) Gallic Acid - No reaction - (NA) - (1)
[size=6][color=red][b]4-MEC[/b][/color][/size] p-DMAB-TS - Light yellow - (NA) - (4)
[size=6][color=red][b]Mephedrone, Buphedrone, Ethcathinone, 3 and 4 Flouromethcathinone:[/b][/color][/size] Marquis - no reaction Mecke - slight brown, almost no change. Mandellin - slight browning. Robadope - Negative Simons - Positive
[size=6][color=red][b]MDPV, MDPPP, Methylone, Butylone:[/b][/color][/size] Marquis - yellow Mecke - red-brown Mandellin - clear Robadope - Negative Simons - MDPPP/MDPV Negative, Methylone/Butylone Positive
[size=6][color=red][b]Methedrone[/b][/color][/size] Marquis - yellow-orange Mecke - orange Mandellin - orange Robadope - Negative Simons - Positive
[size=6][color=red][b]5-IAI[/b][/color][/size] Marquis - brown-grey Mecke - yellow Mandellin - no reaction Robadope - Positive Simons - Negative
[size=6][color=red][b]Desoxypipiradrol[/b][/color][/size] All slow and weak color changes. Marquis - brown Mecke - brown Mandellin - yellow/brown Robadope - Negative Simons - Negative
[size=6][color=red][b]MDAI[/b][/color][/size] Marquis - Light brown to very dark brown depending on trace impurities. Mecke - Dark Brown Mandellin - Dark Brown Robadope - Positive Simons - Negative
[size=6][color=red][b]2-Aminoindane[/b][/color][/size] Marquis - no reaction Mecke - brown Mandellin - light blue Robadope - Positive Simons - Negative
[size=6][color=red][b]Pseudoephedrine[/b][/color][/size] Marquis - No reaction Chens - Purple Gallic Acid - No reaction
[size=6][color=red][b]pFPP[/b][/color][/size]
Marquis - no reaction
Mecke - slight browning
Mandellin - no change
Robadope - Negative
Simons - Positive? It should be positive...
[size=6][color=red][b]MDAT:[/b][/color][/size] Not shown. All reactions slow. Strange colors, changing over time, all colors weak. Robadope - Positive Simons - Negative
[size=6][color=red][b]Methylphenidate (ritalin)[/b][/color][/size] Cobalt Thiocyanate: brilliant greenish blue Mandelin - Brilliant orange yellow Marquis - Moderate orange yellow Simons - Pale violet
[size=7][u][b] Opiates[/b][/u][/size]
[size=6][color=red][b]Heroin HCl[/b][/color][/size] Cobalt Thiocyanate - Strong greenish blue Mandelin - Moderate reddish brown Marquis - Deep purplish red Nitric Acid - Pale yellow Froede Reagent - Deep purplish red Mecke - Deep bluish green
[size=6][color=red][b]Opium[/b][/color][/size] Mandelin - Dark brown Marquis - Dark greyish reddish brown Nitric Acid - Dark orange yellow Froede Reagent - Brownish black Mecke - Olive black
[size=6][color=red][b]Morphine monohydrate[/b][/color][/size] Mandelin - Dark greyish reddish brown Marquis - purple / violet Nitric Acid - Bright orange yellow Ferric Chloride - dark green Froede Reagent - Deep purplish red Mecke - Very dark bluish green
[size=6][color=red][b]Methadone[/b][/color][/size] Cobalt Thiocyanate - Brilliant greenish blue Mandelin - Dark greyish blue Mandelin - Green->Blue - (NA) - (5) Marquis - light yellowish pink
[size=6][color=red][b]Oxycodone[/b][/color][/size] Mandelin - Dark greenish yellow Marquis - pale violet Nitric Acid - Brilliant yellow Froede Reagent - Strong yellow Mecke - Moderate olive
[size=6][color=red][b]Propoxyphene[/b][/color][/size] Cobalt Thiocyanate - Strong greenish blue Mandelin - Dark reddish brown Marquis - Blackish purple Froede Reagent - Dark greyish red Mecke - Deep reddish brown
[size=6][color=red][b]Hydrocodone tartrate:[/b][/color][/size] Cobalt Thiocyanate - Brilliant greenish blue Mecke - dark bluish green
[size=6][color=red][b]Codeine[/b][/color][/size] Marquis - purple/violet Nitric Acid - light greenish yellow Mecke - Very dark bluish green Mandelin - Olive green - (NA) - (6)
[size=7][u][b]Other non-psychedelic natural compounds[/b][/u][/size]
[size=6][color=red][b]Hordenine[/b][/color][/size] Mandelin - grey-green - (NA) - (5) Marquis - Brown->green - (NA) - (5)
[size=6][color=red][b]Hyosciamine[/b][/color][/size] Liebermann - red-orange - (NA) - (5)
[size=6][color=red][b]Atropine[/b][/color][/size] Liebermann - red-orange - (NA) - (5)
[size=6][color=red][b]Strychnine[/b][/color][/size] Mandelin - Violet - (NA) - (5)
[size=6][color=red][b]Yohimbine[/b][/color][/size] Liebermann - Blue - (NA) - (5)
[size=6][color=red][b]Cocaine HCl[/b][/color][/size] Cobalt Thiocyanate - Strong greenish blue Mandelin - Deep orange yellow
[size=6][color=red][b]Caffeine (anhydrous, USP)[/b][/color][/size] Marquis - no reaction Mecke - slight browning Mandelin - no change Robadope - Positive Simons - Negative Amalic acid - Orange->violet
[size=6][color=red][b]Ephedrine[/b][/color][/size] Sample from BOLT brand single constituant ephedrine pills. Marquis - no reaction Mecke - no reaction Mandellin - yellow-orange Robadope - Negative
[size=7][u][b]Common adulterants[/b][/u][/size]
[size=6][color=red][b]Procaine[/b][/color][/size] Cobalt Thiocyanate - Strong greenish blue
[size=6][color=red][b]Paracetamol[/b][/color][/size] Ferric Chloride - Blue - (NA) - (5)
Note: These tests wont be accurate for mixtures of alkaloids. Darker color reactions will generally overpower the lighter colors.
More info on colorimetric tests, where to buy or how to make them (and other analytical methods such as TLC for separating mixtures): https://www.dmt-nexus.me/forum/default.aspx?g=posts&t=24225
Sources for information on this thread: > (1) http://www.hipforums.com/newforums/showthread.php?t=342330 > (2) [url=http://www.google.com/url?sa=t&rct=j&q=Color%2BTest%2BReagents%252FKits%2Bfor%2BPreliminary%2BIdentification%2Bof%2BDrugs%2Bof%2BAbuse&source=web&cd=2&ved=0CCQQFjAB&url=http%3A%2F%2Fwww.ncjrs.gov%2Fpdffiles1%2Fnij%2F183258.pdf&ei=6GyETse1K8yV0QXs88zeDw&usg=AFQjCNF70kraIkyd9Tv6lQDHDl0N_v9okA]Fatah, A., (2000) Color Test Reagents/Kits for Preliminary Identification of Drugs of Abuse[/url] > (3) https://mycotopia.net/forums/456210-post2.html > (4) Energy Control (p-DMAB-TS preparation instructions in (3) ) > (5) [url=http://depositfiles.com/files/2820408]Clarke's isolation and identification of drugs (1986) Pharmaceutical press[/url] > (6) [url=http://books.google.com/books?id=hluBF0hAyvIC&dq=LSD+mandelin&q=LSD#v=snippet&q=LSD&f=false]Newton, M., French,J. (2007) Encyclopedia of crime scene investigation[/url] > (7) Van Welsum (1973) Journal of Chromatography 78:237-240 > ( 8 ) [url=http://wiki.dmt-nexus.me/w/images/f/f4/The_use_of_electron-acceptor_reagents_for_the_detection_of_some_hallucinogens.pdf]Heacock, R., Forrest, J. (1973) The use of electron-acceptor reagents for the detection of some hallucinogens[/url] > (9) [url=http://www.google.com/url?sa=t&rct=j&q=UN%2Bmescaline%2Bforensics&source=web&cd=1&ved=0CB0QFjAA&url=http%3A%2F%2Fwww.unodc.org%2Funodc%2Fen%2Fscientists%2Frecommended-methods-for-testing-peyote-cactus.html&ei=bmyETvPKM4OR0QWy3JTpDw&usg=AFQjCNHt-imbcCwydyfNcMlAq0eiBS4ddQ]UN Recommended methods for testing cactus and mushrooms[/url] > (10) [url=http://www.unodc.org/unodc/en/scientists/recommended-methods-for-testing-lysergide.html]UN recommended methods for testing LSD[/url] > (11) http://www.erowid.org/chemicals/mdma/mdma_faq_testing_kits.shtml > (12) http://www.eztest.com/dir2/ez-test-mandelin-for-ecstasy-speed-and-ketamine/ > (13) [url=https://www.euphoricknowledge.com/showthread.php?t=3981&highlight=marquis+mecke]theazo2 @ euphoricknowledge[/url] > (14)* Lou, V.; Koo, W. Y.; Ramstad, E. (1965) Isolation of N-methyltryptamine from Acacia confusa bark. Lloydia, 28(3), 207-208 > (15 )* [url=https://www.soils.org/publications/cs/abstracts/11/1/CS0110010121] Woods, D., Clark, K. (1970) Variation in the Content of Tryptamines in Clones of Phalaris Arundinacea L.1. Vol. 11 No. 1, p. 121-122.[/url] > (16) Trout - Some simple tryptamines > (17)* [url=http://www.sciencedirect.com/science/article/pii/S002196730092956X]Brown et al (1972) A rapid screening procedure for some “street drugs” by thin-layer chromatography. Journal of Chromatography 64; 128-133[/url] > (18 ) [url=http://wiki.dmt-nexus.me/w/images/d/d9/CH9641301.pdf]Culvenor, C.C.J. et al. (1964) “The occurrence of indolealkylamine alkaloids in Phalaris tuberosa L. and P. arundinacea L.” Australian Journal of Chemistry 17:1301-1304.[/url] > (19) [url=http://wiki.dmt-nexus.me/w/images/5/50/J_Physiol-1955-Erspamer-118-33.pdf]Erspamer, Vittorio (1955) “Observations on the Fate of Indolealkylamines in the Organism.” Journal of Physiology 127: 118-133.[/url] > (20)* [url=http://www.sciencedirect.com/science/article/pii/S0021967301915328]Frahn, J.L. & R.J. Illman (1973) “Separation of Some Indolylalkylamines From Their Metho Cation Derivatives Using Neutral Polystyrene Resin. Application to the Alkaloids of Phalaris tuberosa (Gramineae).” Journal of Chromatography 87: 187-191.[/url] > (21) [url=http://wiki.dmt-nexus.me/w/images/f/f9/CH9712189.pdf]Frahn, J.L. & D.F. O’Keefe (1971) “The Occurrence of Tetrahydro-β−carboline Alkaloids in Phalaris tuberosa (Graminae).” Australian Journal of Chemistry 24: 2189-2192[/url]. > (22) [url=http://wiki.dmt-nexus.me/w/images/0/0c/Science.pdf]Gander, J.E. et al. (1976) “The Occurrence of 2-Methyl-1,2,3,4-Tetrahydro-b-carboline and Variation in Alkaloids in Phalaris arundinacea.” Phytochemistry 15: 737-738.[/url] > (23)* [url=http://onlinelibrary.wiley.com/doi/10.1002/jps.2600600819/abstract]Ghosal, S. et al. (1971) “Chemical and Pharmacological Evaluation of Banisteriopsis argentea Spring ex Juss.” Journal of Pharmaceutical Sciences 60( 8 ): 1209-1212.[/url] > (24) [url=https://www.dmt-nexus.me/forum/resource.ashx?a=6456]Majak, W. et al. (1978 ) “TLC Luminescence of Gramine and Related indole Alkaloids in Phalaris arundinacea.” Phytochemistry 17: 301-303. [/url] > (25)* [url=http://www.ncbi.nlm.nih.gov/pubmed/2051748]Schnoll, S.H. et al. (1972) “A Rapid Thin Layer Chromatographic Screening Procedure for Various Abused Psychotropic Agents. Journal of Psychedelic Drugs 5 (1):75-78.[/url] > (26)* Smith, Ivor (1969) Chromatographic and Electrophoretic Techniques. Volume I. Chromatography.” 3rd Edition. William Heinemann Medical Books Ltd., London/ Interscience Publishers: New York. > (27) [url=http://ebookee.org/Psychedelic-Chemistry_865196.html]Smith, Michael Valentine (1981) Psychedelic Chemistry. Loompanics; Port Townsend. ISBN 0-915179-10-5 (page 173)[/url] > (28 ) [url=http://wiki.dmt-nexus.me/w/images/4/47/Further_determination.pdf]majak, W. & Bose, R. (1977) Further characterization and quantitative determination of 5-methoxy-N-methyltryptamine in Phalaris arundinacea[/url] > (29) [url=http://wiki.dmt-nexus.me/w/images/b/b5/Jo01345a047.pdf]Ghosal, S & Mukherjee, B. (1966) Indole-3-alkylamine Bases of Desmodium pulchellum[/url] > (30) [url=http://wiki.dmt-nexus.me/w/images/e/e8/Bufo.pdf]Erspamer et al (1967) 5-Methoxy- and 5-Hydroxyindoles in the skin of Bufo alvarius[/url] > (31) [url=http://wiki.dmt-nexus.me/w/images/a/a7/Jf00077a037.pdf]Miles, D. et al (1987) Alkaloidal insect antifeedants from Virola calophylla[/url]
- These references were found through the book from K. Trout's - Some Simple tryptamines, second edition. We did not get direct access to these publications