Difference between revisions of "Enoons Cold Caapi Tek"
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The orange liquid is decanted off and the alkaloids are washed with fresh distilled water 4 times. | The orange liquid is decanted off and the alkaloids are washed with fresh distilled water 4 times. | ||
| − | Using sodium carbonate will require you to perform more cleaning steps than using lye but it will work in the end nonetheless. Your end product should be white or off white. If it's darker like in the pic below, another A/B step for getting rid of the impurities is in order. | + | Using sodium carbonate will require you to perform more cleaning steps than using lye but it will work in the end nonetheless. Your end product should be white or off white. If it's darker like in the pic below, another A/B step for getting rid of the impurities is in order. Please refer to [[Easy Caapi Vine Alkaloid Extraction Guide]] for purification procedures. |
| − | [[File:EnoonColdCaapi-06.jpg|thumb|c|center|370px| | + | [[File:EnoonColdCaapi-06.jpg|thumb|c|center|370px|From left to right: Na2CO3, decanted water, free-base harmalas in suspension after 2 washes. Notice the based alks (using Na2CO3) - to get a cleaner product A/B steps are required.]] |
=== Step 6 - Filter === | === Step 6 - Filter === | ||
Revision as of 11:31, 22 September 2011
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Note: | This page is a transcription of Enoon's Cold Acetic Acid Extraction of Caapi Tek [1]. The content is to remain accurate as such. |
Contents
Initial Notes
I performed a cold acetic acid extraction of white Caapi from the MHUK vendor. A previous extraction via Easy Caapi Vine Alkaloid Extraction Guide boiling 5x45min yielded ~ 1.2% alkaloids after several prufication steps. So I want to see if I can reach the same with a cold extraction.
Method
Step 1 - Shred Vine
Begin with whole or partially shredded vine and shred it up as much as possible. This will allow the alkaloids to migrate to the solution easier.
Step 2 - Collect and Add Acid
This is added to my favorite PP container and approx. 300ml of 3% acetic acid is added.
Step 3 - Soak
Allow this to soak at room temperature (RT) for 3 days / 72 hours with occasional shaking.
Step 4 - Filter and Collect
After soaking for 72 hours, filter the liquid and set aside. Add another 300ml of 3% acetic acid to the vine and allow to soak for another 72 hours.
Step 5 - Repeat
Repeat step 4 again 4 times for a total of 5 x 3 day soaks.
Combine the pulls and reduce a bit. After you have reduced the pulls to a manageable level, base with sodium carbonate or lye.
The orange liquid is decanted off and the alkaloids are washed with fresh distilled water 4 times. Using sodium carbonate will require you to perform more cleaning steps than using lye but it will work in the end nonetheless. Your end product should be white or off white. If it's darker like in the pic below, another A/B step for getting rid of the impurities is in order. Please refer to Easy Caapi Vine Alkaloid Extraction Guide for purification procedures.
Step 6 - Filter
After you are finished rinsing the alkaloids, it's time to filter them. If you do not have a food dehydrator it is recommended to hang the filter to allow it to dry from all sides.
Yield & Conclusion
Yield: After 5, 3 day pulls, the yield was 1.2% which is the same yield as doing 5 boils.
Conclusion: Save some energy and soak your vine in the fridge!
