Difference between revisions of "69ron's D-Limonene Mescaline Extraction"

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(Pure white mescaline HCl from cactus using d-limonene)
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|Add 300 ml of d-limonene. Mix well. Let sit a few hours.
 
|Add 300 ml of d-limonene. Mix well. Let sit a few hours.
 
|Pour off the d-limonene through a filter.
 
|Pour off the d-limonene through a filter.
|Add 25 ml of water with 5 ml of 10% HCl solution to the d-limonene. Mix thoroughly. NOTE: DO NOT USE CONCENTRATED HYDROCHLORIC ACID. IT MUST BE DILUTED AS SPECIFIED OR A BUNCH OF JUNK WILL PRECIPITATE OUT OF THE D-LIMONENE.
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|Add 25 ml of water with 5 ml of 10% HCl solution to the d-limonene. Mix thoroughly.  
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DO NOT USE CONCENTRATED HYDROCHLORIC ACID. IT MUST BE DILUTED AS SPECIFIED OR A BUNCH OF JUNK WILL PRECIPITATE OUT OF THE D-LIMONENE.
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|Separate the water from the d-limonene (the water is at the bottom, the d-limonene at the top). This water will contain mescaline HCl. Evaporate your water in a food dehydrator at 155 F to get sticky brown impure mescaline HCl.
 
|Separate the water from the d-limonene (the water is at the bottom, the d-limonene at the top). This water will contain mescaline HCl. Evaporate your water in a food dehydrator at 155 F to get sticky brown impure mescaline HCl.
 
|Repeat steps 4 and 5 at least 2-3 times,
 
|Repeat steps 4 and 5 at least 2-3 times,

Revision as of 00:51, 16 March 2009

Pure white mescaline HCl from cactus using d-limonene

Note error.png Note: This section is a transcription of 69ron's Pure white mescaline HCl from cactus using d-limonene tek[1]. The content is to remain accurate as such.


Procedure for Pure white mescaline HCl from cactus using d-limonene Cog.png
1. Powderize your cactus. Mix 100 grams of bark with 25 grams of calcium hydroxide. Add 300 ml water to make it feel wet but not watery. Mix for about 5 minutes.
2. Add 300 ml of d-limonene. Mix well. Let sit a few hours.
3. Pour off the d-limonene through a filter.
4. Add 25 ml of water with 5 ml of 10% HCl solution to the d-limonene. Mix thoroughly.
NOTE Alert.png

DO NOT USE CONCENTRATED HYDROCHLORIC ACID. IT MUST BE DILUTED AS SPECIFIED OR A BUNCH OF JUNK WILL PRECIPITATE OUT OF THE D-LIMONENE.

5. Separate the water from the d-limonene (the water is at the bottom, the d-limonene at the top). This water will contain mescaline HCl. Evaporate your water in a food dehydrator at 155 F to get sticky brown impure mescaline HCl.
6. Repeat steps 4 and 5 at least 2-3 times,
7. Repeat steps 2 - 6 at least 2 times.
Ok, now you have a bunch of sticky brown impure mescaline. You first wash it with acetone about 2 times. You use about 20 ml of acetone for each wash. With the acetone covering the mescaline, you small the mescaline and much as you can. You want to powderize it in the acetone. Wait for all the particles to settle down and then carefully decant your acetone so that none of the mescaline is decanted with the acetone. Repeat it with 20 ml more acetone.
Ok, at this point the mescaline is usually very light tan and it's difficult to get it pure white with more acetone washes. So we now wash with 99% isopropyl alcohol one time. We use about 20 ml. It must be 99% isopropyl alcohol. Pour it over your light tan crystals and mix it. Let all the pieces settle down. Now carefully decant the IPA leaving behind pure white mescaline HCl.


Non toxic food safe extraction of mescaline using d-limonene

Note error.png Note: This page is a transcription of 69ron's Non toxic food safe extraction of mescaline using d-limonene tek[2]. The content is to remain accurate as such.

1 - Powderize your cactus. Mix 100 grams of bark with 25 grams of calcium hydroxide. Add 300 ml water to make it feel wet but not watery. Mix for about 5 minutes.

2 - Add 300 ml of d-limonene. Mix well. Let sit a few hours.

3 - Pour off the d-limonene through a filter. (It's really cool if you use a French Coffee Press for this. Using a French Coffee Press you press the cactus mix and squeeze out the d-limonene to get every last drop of d-limonene out. Then filter it through a paper coffee filter.)

4 - Add 25 ml of vinegar to the d-limonene. Mix thoroughly.

5 - Separate the vinegar from the d-limonene (the vinegar is at the bottom, the d-limonene at the top). This vinegar will contain mescaline acetate. Evaporate your vinegar in a food dehydrator at 155 F to get waxy amber slightly impure mescaline acetate.

6 - Repeat steps 4 and 5 at least 2-3 times,

7 - Repeat steps 2 - 6 at least 2 times.

The great thing about this tech is that is it 100% food grade and non-toxic. You can buy food grade calcium hydroxide at many places. Make sure to use food grade d-limonene. Use regular white vinegar that is 5% acetic acid.

The result is a waxy amber colored slightly impure mescaline acetate approximately 85-95% pure.

SWIM has used this tech and got yields you cannot believe. Mescaline acetate is a little waxy, and tends to stick to things. It's texture is not as nice as mescaline HCl which is much more powdery in texture. However, SWIM has found that mescaline acetate is stronger by weight than mescaline HCl. He's not sure why. It should be weaker because it's heavier. I believe it absorbs faster and that's why it's stronger. It definitely comes on much quicker than mescaline HCl does.

The purity of this extraction is good enough for a great trip. You really don't need 99% purity. At about 90% pure, it's concentrated enough to put into gel tabs for a really nice convenient trip without all the bulk of the cactus. At this purity level mescaline acetate is still a little stronger than 99% pure white mescaline HCl. SWIM has both and has compared them many times already. The white 99% pure mescaline is prettier and is not waxy, so it's easier to deal with, but it's less potent with otherwise identical effects.

Note that this tech was developed for San Pedro cactus.


Reference

  1. Pure white mescaline HCl from cactus using d-limonene[1]
  2. Non toxic food safe extraction of mescaline using d-limonene[2]