The Tao of Rue Extraction - Revision history

Melodic Catastrophe: /* Initial Notes and Tips */

2014-08-20T02:12:26Z

‎Initial Notes and Tips

Melodic Catastrophe at 02:11, 20 August 2014

2014-08-20T02:11:21Z

Melodic Catastrophe: /* Final Notes and Tips */

2014-08-20T02:07:54Z

‎Final Notes and Tips

Melodic Catastrophe: /* Step 6 - Manske */

2013-01-24T18:31:13Z

‎Step 6 - Manske

Melodic Catastrophe: /* Step 6 - Manske */

2013-01-24T18:21:39Z

‎Step 6 - Manske

Melodic Catastrophe: /* Step 6 - Manske */

2013-01-24T18:20:43Z

‎Step 6 - Manske

Melodic Catastrophe: /* Step 5 - Base */

2013-01-24T18:15:54Z

‎Step 5 - Base

Melodic Catastrophe: /* Step 5 - Base */

2013-01-24T18:14:05Z

‎Step 5 - Base

Melodic Catastrophe at 21:14, 8 September 2012

2012-09-08T21:14:13Z

Melodic Catastrophe at 20:47, 8 September 2012

2012-09-08T20:47:44Z

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 * Be sure to keep all used filters and cotton balls to the side and perform at least one final acid wash on them. I got 1.9g of clean harmalas from the used filters alone.
 * Patience is key for this Tek. Be prepared to spend at least two or more days working on this, especially if you're working with large quantities.
-* Be careful about spills! Syrian Rue is a very powerful dye and it WILL stain if it isn't cleaned up immediately. It's best to work in an area that the stains won't matter or on stainless steel if possible. Another alternative is to put down some cardboard on your counter tops and floors where you'll be working.
+* Be careful about spills! Syrian Rue is a very powerful dye and it WILL stain if it isn't cleaned up immediately. It's best to work in an area that the stains won't matter or on stainless steel if possible. Another alternative is to put down some cardboard on your countertops and floors where you'll be working. Mr. Clean brand Magic Erasers work exceptionally well for removing the stains with a bit of elbow grease.
 * When waiting for the freebased harmalas to settle, setting the container on a subwoofer or washing machine helps speed the process along.
 * Keep all of the wash water and allow everything to settle for a couple of days. Sometimes those cloudy solutions can contain some extra harmalas if you want to get every last MG. *Kudos to evil804 for the last two tips.

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 * '''Patience'''
 }}
-== Initial Notes ==
+== Initial Notes and Tips ==
+* As stated throughout the Tek, the most important part is getting the brew as clean as possible.
-There really isn't anything new in this Tek, it's just refining what is already known. This is more about streamlining the process and making it easier to work with. Please take the time to review and integrate the existing harmala teks so you have a general idea of the process.
+* Be sure to keep all used filters and cotton balls to the side and perform at least one final acid wash on them. I got 1.9g of clean harmalas from the used filters alone.
+* Patience is key for this Tek. Be prepared to spend at least two or more days working on this, especially if you're working with large quantities.
-* [[Harmalas Extraction and Separation Guide]]
+* Be careful about spills! Syrian Rue is a very powerful dye and it WILL stain if it isn't cleaned up immediately. It's best to work in an area that the stains won't matter or on stainless steel if possible. Another alternative is to put down some cardboard on your counter tops and floors where you'll be working.
-* [[Easy Caapi Vine Alkaloid Extraction Guide]]
+* When waiting for the freebased harmalas to settle, setting the container on a subwoofer or washing machine helps speed the process along.
-* [[Phlux's Telepathine Tek]]
+* Keep all of the wash water and allow everything to settle for a couple of days. Sometimes those cloudy solutions can contain some extra harmalas if you want to get every last MG. *Kudos to evil804 for the last two tips.
 == Background ==
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 == Credits ==
 * Kudos to Endlessness for putting together the harmala extraction and separation guide<ref>[[Harmalas Extraction and Separation Guide]]</ref> and to everyone who contributed to it.
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   Please refer to Gibran's [[Easy Caapi Vine Alkaloid Extraction Guide]], [[Easy Caapi Vine Alkaloid Extraction Guide#Remove Excess NaOH, Salts, Etc.|Step 6 Removing Excess NaOH, Salts etc]] for more info.
 == Reference ==

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 * When waiting for the freebased harmalas to settle, setting the container on a subwoofer or washing machine helps speed the process along.
 * Keep all of the wash water and allow everything to settle for a couple of days. Sometimes those cloudy solutions can contain some extra harmalas if you want to get every last MG. *Kudos to evil804 for the last two tips.
 == Reference ==
 <references/>

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 === Step 6 - Manske ===
-Once you have redissolved your alkaloids in a minimal amount of fresh, hot vinegar or as The Day Tripper pointed out, a fumaric acid solution, it's time to manske them. Day Trippers fumaric acid approach leads to chunkier crystals later. Vinegar will lead to needle like crystals as pictured to the right. The appearance of the crystals doesn't really matter at this point because they'll be redissolved several times during the cleanup steps.
+Once you have redissolved your alkaloids in a minimal amount of fresh, hot vinegar and then filtered the solution, it's time to perform the manske.
-−
 There are three ways you can perform the manske.

← Older revision		Revision as of 18:21, 24 January 2013
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	=== Step 6 - Manske ===		=== Step 6 - Manske ===
−	Once you have redissolved your alkaloids in a minimal amount of fresh, hot vinegar or as The Day Tripper pointed out, a fumaric acid solution, it's time to manske them. Day Trippers fumaric acid approach leads to chunkier crystals later. Vinegar will lead to needle like crystals as pictured to the right. The appearance of the crystals doesn't really matter at this point because they'll be redissolved several times during the cleanup steps~~. This mainly comes in handy at the end of the tek when your alks are clean and you'd like to store your harmalas as a salt instead of as a freebase~~.	+	Once you have redissolved your alkaloids in a minimal amount of fresh, hot vinegar or as The Day Tripper pointed out, a fumaric acid solution, it's time to manske them. Day Trippers fumaric acid approach leads to chunkier crystals later. Vinegar will lead to needle like crystals as pictured to the right. The appearance of the crystals doesn't really matter at this point because they'll be redissolved several times during the cleanup steps.

← Older revision		Revision as of 18:20, 24 January 2013
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	=== Step 6 - Manske ===		=== Step 6 - Manske ===
−	Once you have your ~~freebase alks, redissolve them~~ in a minimal amount of fresh, hot vinegar or as The Day Tripper pointed out, a fumaric acid solution. Day Trippers fumaric acid approach leads to chunkier crystals later. Vinegar will lead to needle like crystals as pictured to the right.	+	Once you have redissolved your alkaloids in a minimal amount of fresh, hot vinegar or as The Day Tripper pointed out, a fumaric acid solution, it's time to manske them. Day Trippers fumaric acid approach leads to chunkier crystals later. Vinegar will lead to needle like crystals as pictured to the right. The appearance of the crystals doesn't really matter at this point because they'll be redissolved several times during the cleanup steps. This mainly comes in handy at the end of the tek when your alks are clean and you'd like to store your harmalas as a salt instead of as a freebase.

← Older revision		Revision as of 18:15, 24 January 2013
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−	After you have decanted the basic (high ph) lye water off the top, you want to add some hot vinegar and water to your alks to redissolve ~~all of your freebase alkaloids~~ back into the solution as harmala acetates. Once your alkaloids are redissolved, filter out anything that won't dissolve. This is mostly plant matter and oils.	+	After you have decanted the basic (high ph) lye water off the top, you want to add some hot vinegar and water to your freebase alks to redissolve everything back into the solution as harmala acetates. Once your alkaloids are redissolved, filter out anything that won't dissolve. This is mostly plant matter and oils.

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-After you have decanted, you want to add some hot vinegar and water to your alks to redissolve all of your alkaloids. Once everything is redissolved, filter out anything that won't dissolve. This is mostly plant matter and oils.
+After you have decanted the basic (high ph) lye water off the top, you want to add some hot vinegar and water to your alks to redissolve all of your freebase alkaloids back into the solution as harmala acetates. Once your alkaloids are redissolved, filter out anything that won't dissolve. This is mostly plant matter and oils.
 [[File:Tao_of_rue_05.jpg|thumb|400px|Let them sit as long as possible undisturbed so they can grow as big as possible. 24 hours is usually enough.]]
 === Step 6 - Manske ===
 Once you have your freebase alks, redissolve them in a minimal amount of fresh, hot vinegar or as The Day Tripper pointed out, a fumaric acid solution. Day Trippers fumaric acid approach leads to chunkier crystals later. Vinegar will lead to needle like crystals as pictured to the right.

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 * '''Patience'''
 }}
 == Initial Notes ==
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 * Kudos for Plumsmooth for pointing out the text book Manske technique.
 * Kudos to everyone who has been pioneering harmala extractions this whole time.
 == Method ==