The FASA Method - Revision history

TheTraveler at 19:42, 17 September 2013

2013-09-17T19:42:51Z

TheTraveler at 19:41, 17 September 2013

2013-09-17T19:41:55Z

TheTraveler: Text replace - "dmt-nexus.com" to "dmt-nexus.me"

2012-01-31T19:57:02Z

Text replace - "dmt-nexus.com" to "dmt-nexus.me"

TheTraveler at 14:00, 2 December 2010

2010-12-02T14:00:00Z

Amor fati: /* Further Elaboration and Technical Support */

2010-01-15T21:10:21Z

‎Further Elaboration and Technical Support

Amor fati: amended link from fasa

2010-01-12T15:19:15Z

amended link from fasa

Amor fati at 21:28, 22 December 2009

2009-12-22T21:28:26Z

Amor fati: created page for handbook transclusion

2009-12-17T05:28:15Z

created page for handbook transclusion

New page

<noinclude>{{Handbook Transclusion Header}}</noinclude>

{{materials_list
|
* Freebase DMT Saturated Acetone or [[NPS]]
|
* Anhydrous Acetone
|
* Fumaric Acid
}}

[[Image:Dmt fumarate bond.JPG|thumb|Two DMT molecules forming a complex with one fumaric acid molecule to form [[DMT Fumarate|DMT Fumarate]].]]

The [[FASA|FASA]], or fumaric acid saturated acetone, method is a method employed to render [[DMT Fumarate|DMT Fumarate]].

Considerations:
: [[DMT Fumarate|DMT Fumarate]] is reportedly quite stable and resistant to oxidization or other forms of degradation. It is notably resistant to heat, and as such is able to withstand low-temperature oven-drying. Certain other related compounds, such as jungle-spice and bufotenine are also able to crystallize as a fumarate. Defatting is not required prior to employing [[FASA|FASA]] methods, as oils and most other impurities should not interfere with this method's procedure or the yield

: Because [[DMT Fumarate|DMT Fumarate]] is water-soluble, it is also well-suited for oral administration in conjunction with harmaloids, either mixed into a beverage or encapsulated.

Methods:
:The [[FASA|FASA]] method employs the firstly, the solubility of fumaric acid in acetone, and secondly, solubility of freebase DMT in acetone, and thirdly, the insolubility of [[DMT Fumarate|DMT Fumarate]] in acetone or the non-polar solvents commonly utilized for extraction. The solubility of both DMT and fumaric acid in acetone facilitates their reaction to produce a crystalline DMT salt which is completely insoluble in acetone or non-polar solvents.

{{procedure
|Rendering Crystalline DMT Fumarate
|
# Dissolve about 7mg fumaric acid per mL of fresh anhydrous acetone to prepare a FASA solution, allotting adequate time and stirring for complete saturation, and allowing any excess to settle to the bottom.
#* ''It is recommended that the solution be prepared in slight excess of fumaric acid rather than an excess of acetone for the procedure to be most effective.''
# Prepare a DMT-saturated solution using either acetone or an [[NPS]] ensuring that its container will facilitate the collection of a precipitate and protect the solution from moisture.
#* ''Naphtha, however, is reported to cause fumaric acid to precipitate out of acetone, disrupting any significant chemical reaction from occurring.''
# Add FASA dropwise to the DMT saturated solution until no more reaction can be observed.
#* ''A precipitate should form wherever the drops are added, but will eventually become too thick of a cloud to observe any new reaction occurring.''
# Once the solution settles enough for a clear segment of the solution to be observed where drops of FASA are to be added, repeat step 3.
# Repeat steps 3-4 until no more reaction occurs, and allow to settle completely.
# Carefully decant the solvent.
#* If acetone is the only solvent used, it can be reused as FASA, or if no significant excess of FASA has be added, it can be reused for drytek extraction.
#* If an [[NPS|NPS]] is used, the acetone and fumaric acid can be wash out with water and separated by standard separatory methods.
# Collect the salted product onto an evaporation dish and dry by air-drying or by oven-drying on the lowest possible heat setting.
#* ''It is advisable to wash the product with anhydrous acetone to remove any potential excess of fumaric acid or NPS.''
# Store the dry product away from heat and moisture.
}}

← Older revision		Revision as of 19:42, 17 September 2013
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	[[Category:Conversion Tek]]		[[Category:Conversion Tek]]
		+	[[Category:Extraction Tek]]

@@ Line 1: / Line 1: @@
 <noinclude>{{Handbook Transclusion Header}}</noinclude>
-====='''[[The FASA Method]]'''=====
 {{materials_list
@@ Line 11: / Line 13: @@
 * Fumaric Acid
 }}
 The [[FASA|FASA]], or fumaric acid saturated acetone, method is a method employed to render [[DMT Fumarate|DMT Fumarate]].
@@ Line 23: / Line 23: @@
 Methods:
 :The [[FASA|FASA]] method employs the firstly, the solubility of fumaric acid in acetone, and secondly, solubility of freebase DMT in acetone, and thirdly, the insolubility of [[DMT Fumarate|DMT Fumarate]] in acetone or the non-polar solvents commonly utilized for extraction.  The solubility of both DMT and fumaric acid in acetone facilitates their reaction to produce a crystalline DMT salt which is completely insoluble in acetone or non-polar solvents.
 {{procedure
@@ Line 43: / Line 51: @@
 }}
-====== Further Elaboration and Technical Support ======
+=== Links ===
-: [http://www.dmt-nexus.me/forum/default.aspx?g=posts&t=2546 The FASA Method: A Summary - DMT Fumarate and Beyond]
+* [http://www.dmt-nexus.me/forum/default.aspx?g=posts&t=2546 The FASA Method: A Summary - DMT Fumarate and Beyond]
 [[Category:Conversion Tek]]

@@ Line 45: / Line 45: @@
 ====== Further Elaboration and Technical Support ======
-: [http://www.dmt-nexus.com/forum/default.aspx?g=posts&t=2546 The FASA Method: A Summary - DMT Fumarate and Beyond]
+: [http://www.dmt-nexus.me/forum/default.aspx?g=posts&t=2546 The FASA Method: A Summary - DMT Fumarate and Beyond]
 [[Category:Conversion Tek]]

← Older revision		Revision as of 14:00, 2 December 2010
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	: [http://www.dmt-nexus.com/forum/default.aspx?g=posts&t=2546 The FASA Method: A Summary - DMT Fumarate and Beyond]		: [http://www.dmt-nexus.com/forum/default.aspx?g=posts&t=2546 The FASA Method: A Summary - DMT Fumarate and Beyond]
		+
		+	[[Category:Conversion Tek]]

← Older revision		Revision as of 21:10, 15 January 2010
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	====== Further Elaboration and Technical Support ======		====== Further Elaboration and Technical Support ======

−	[http://www.dmt-nexus.com/forum/default.aspx?g=posts&t=2546 The FASA Method: A Summary - DMT Fumarate and Beyond]	+	: [http://www.dmt-nexus.com/forum/default.aspx?g=posts&t=2546 The FASA Method: A Summary - DMT Fumarate and Beyond]

← Older revision		Revision as of 15:19, 12 January 2010
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	# Store the dry product away from heat and moisture.		# Store the dry product away from heat and moisture.
	}}		}}
		+
		+	====== Further Elaboration and Technical Support ======
		+
		+	[http://www.dmt-nexus.com/forum/default.aspx?g=posts&t=2546 The FASA Method: A Summary - DMT Fumarate and Beyond]

← Older revision		Revision as of 21:28, 22 December 2009
Line 1:		Line 1:
	<noinclude>{{Handbook Transclusion Header}}</noinclude>		<noinclude>{{Handbook Transclusion Header}}</noinclude>
		+
		+	====='''[[The FASA Method]]'''=====

	{{materials_list		{{materials_list