https://wiki.dmt-nexus.me/w/index.php?action=history&feed=atom&title=STB_Freebase_Conversion_of_DMT 2026-05-10T12:25:52Z Revision history for this page on the wiki MediaWiki 1.22.1 https://wiki.dmt-nexus.me/w/index.php?title=STB_Freebase_Conversion_of_DMT&diff=1980&oldid=prev 2010-01-04T08:00:12Z

<p>created page for handbook transclusion, needs markup for uniform appearance</p> <p><b>New page</b></p><div>&lt;noinclude&gt;{{Handbook Transclusion Header}}&lt;/noinclude&gt;<br /> <br /> &lt;onlyinclude&gt;<br /> ===== STB Conversion =====<br /> <br /> This conversion is simplistic in that it almost exactly resembles the methods used in [[The_Nexian_DMT_Handbook#STB_Techniques|STB Techniques]], though it is significantly simpler in that it involves less material, fewer impurities, and does not require a strong base.<br /> <br /> {{materials_list<br /> |<br /> * [[DMT Fumarate]]<br /> |<br /> * [[NPS|Nonpolar Solvent]]<br /> * Distilled Water<br /> |<br /> * Household Base:<br /> ** Either Sodium Carbonate (Washing Soda)<br /> ** or Calcium Hydroxide (Pickling Lime)<br /> ** or Sodium Bicarbonate (Baking Soda)<br /> *** [[The_Nexian_DMT_Handbook#Material_Preparation_3|Converted to Sodium Carbonate]]<br /> }}<br /> <br /> Procedure for [[STB Freebase Conversion of DMT]]:<br /> # Dissolve [[DMT Fumarate|DMT Fumarate]] in an adequate amount of water.<br /> #* ''No reaction occurs at this point.''<br /> # Add a concentrated solution of weak base until total precipitation is observed by the cloudiness of the solution.<br /> #* ''The fumaric acid undergoes reaction with the base, effectively neutralizing the acid and freeing the product in its pure alkaloid form, or freebase.''<br /> # Stir in [[NPS]] thoroughly and allow to separate from the aqueous solution.<br /> #* ''The more contact allotted between the product and the [[NPS]], the greater the saturation.''<br /> # Collect the top layer of [[NPS]], being careful not to allow any aqueous contamination.<br /> #* ''Aqueous contamination may result in an impure product or may disrupt subsequent crystallization.''<br /> # Repeat steps 3-4 with fresh or unsaturated [[NPS]] until the aqueous solution is exhausted to satisfaction.<br /> #* ''Three washes is generally considered sufficient.''<br /> # See [[The_Nexian_DMT_Handbook#Crystallization|Crystallization]] in order to render crystalline freebase product.<br /> <br /> &lt;/onlyinclude&gt;<br /> <br /> {{Page_Footer|Conversion_Tek}}</div>

Amor fati