Kash's A/B Mescaline Extraction - Revision history

Kash: /* Procedure */

2018-07-28T00:13:04Z

‎Procedure

Kash: /* Procedure */

2018-07-28T00:11:33Z

‎Procedure

Kash: /* Procedure */

2018-07-28T00:00:35Z

‎Procedure

Kash: /* Procedure */

2018-07-27T23:59:21Z

‎Procedure

Kash: /* Procedure */

2018-07-27T23:53:29Z

‎Procedure

Kash: /* Procedure */

2014-03-14T02:00:46Z

‎Procedure

Kash at 01:58, 14 March 2014

2014-03-14T01:58:40Z

Kash: /* Procedure */

2014-03-14T01:57:07Z

‎Procedure

Kash at 21:51, 23 February 2014

2014-02-23T21:51:02Z

Kash at 21:48, 23 February 2014

2014-02-23T21:48:51Z

@@ Line 21: / Line 21: @@
 |Add 200ml toluene (or xylene) and mix for 10-15 minutes. Let the mixture settle and use a hot water bath to seperate the layers from the emulsion if necessary. Seperate the layers with a pipet, separatory funnel, or syringe. Save the toluene in another glass container and put basic aqueous cacti solution back in original container.
 |Repeat previous step atleast 4 times total. Discard basic aqueous layer after, saving the toluene extract which contains the alkaloids.
-|To the toluene extract add 100ml H2O. Add 0.5ml concentrated HCl to this and mix well for 5 minutes. Check the pH. If it is still basic (pH 9+) then add incriments of 0.5ml HCl with mixing and checking pH until it tests acidic (below pH 7). Continue mixing for 10 minutes after. Only one acid salting pull is necessary, but more can be performed and may be necessary for larger scale extraction.
+|To the toluene extract add 100ml H2O. Add 0.5ml concentrated HCl to this and mix well for 5 minutes. Check the pH. If it is still basic (pH 9+) then add incriments of 0.5ml HCl with mixing and checking pH until it tests acidic (below pH 7). Continue mixing for 10 minutes after. Only one acid salting pull is usually necessary, but more can be performed and may be necessary for larger scale extraction.
 |Seperate layers, hot water bath may be necessary to seperate emulsion quickly. Filter and save acidic H2O layer and discard/recycle toluene. Evaporate the aqueous layer on a dish with aid of a fan and/or hot water bath. Never use direct heat it will scorch your product. Scrape up the crystals.
 |Wash crystals with 50ml cold MEK (or anhydrous acetone, ethyl acetate). You will notice the solvent become discolored and the crystals become cleaner. Decant off the solvent carefully, leaving behind the cleaned crystals.

@@ Line 19: / Line 19: @@
 |Repeat step 3 atleast four to six times total until the liquid filtered out has very little color. Discard plant material after final time and reduce all the aqueous cacti extract to around 300 ml. This can be put in a glass pickle jar. Allow to sit overnight to precipitate unwanted fine particles, but this is optional.
 |Now it is time to basify. Mix 50g NaOH in 100ml H2O. It will get VERY hot, it is recommended to cool the mixing container while stirring with a cold water bath or under the faucet. Add the NaOH solution to the aqueous cacti extract.
-|Add 200ml toluene (or xylene) and mix for 10-15 minutes. Let the mixture settle and use a hot water bath to seperate the layers from the emulsion if necessary. The layers should seperate quickly. Seperate the layers with a pipet, separatory funnel, or syringe. Save the toluene in another glass container and put basic aqueous cacti solution back in original container.
+|Add 200ml toluene (or xylene) and mix for 10-15 minutes. Let the mixture settle and use a hot water bath to seperate the layers from the emulsion if necessary. Seperate the layers with a pipet, separatory funnel, or syringe. Save the toluene in another glass container and put basic aqueous cacti solution back in original container.
 |Repeat previous step atleast 4 times total. Discard basic aqueous layer after, saving the toluene extract which contains the alkaloids.
 |To the toluene extract add 100ml H2O. Add 0.5ml concentrated HCl to this and mix well for 5 minutes. Check the pH. If it is still basic (pH 9+) then add incriments of 0.5ml HCl with mixing and checking pH until it tests acidic (below pH 7). Continue mixing for 10 minutes after. Only one acid salting pull is necessary, but more can be performed and may be necessary for larger scale extraction.

@@ Line 21: / Line 21: @@
 |Add 200ml toluene (or xylene) and mix for 10-15 minutes. Let the mixture settle and use a hot water bath to seperate the layers from the emulsion if necessary. The layers should seperate quickly. Seperate the layers with a pipet, separatory funnel, or syringe. Save the toluene in another glass container and put basic aqueous cacti solution back in original container.
 |Repeat previous step atleast 4 times total. Discard basic aqueous layer after, saving the toluene extract which contains the alkaloids.
-|To the toluene extract add 100ml H2O. Add 0.5ml concentrated HCl to this and mix well for 5 minutes. Check the pH. If it is still basic (pH 9+) then add incriments of 0.5ml HCl with mixing and checking pH until it tests acidic (below pH 7). Continue mixing for 10 minutes after. Only one acid salting pull is necessary, still it is a good idea to do one more just to be safe.
+|To the toluene extract add 100ml H2O. Add 0.5ml concentrated HCl to this and mix well for 5 minutes. Check the pH. If it is still basic (pH 9+) then add incriments of 0.5ml HCl with mixing and checking pH until it tests acidic (below pH 7). Continue mixing for 10 minutes after. Only one acid salting pull is necessary, but more can be performed and may be necessary for larger scale extraction.
 |Seperate layers, hot water bath may be necessary to seperate emulsion quickly. Filter and save acidic H2O layer and discard/recycle toluene. Evaporate the aqueous layer on a dish with aid of a fan and/or hot water bath. Never use direct heat it will scorch your product. Scrape up the crystals.
 |Wash crystals with 50ml cold MEK (or anhydrous acetone, ethyl acetate). You will notice the solvent become discolored and the crystals become cleaner. Decant off the solvent carefully, leaving behind the cleaned crystals.

@@ Line 21: / Line 21: @@
 |Add 200ml toluene (or xylene) and mix for 10-15 minutes. Let the mixture settle and use a hot water bath to seperate the layers from the emulsion if necessary. The layers should seperate quickly. Seperate the layers with a pipet, separatory funnel, or syringe. Save the toluene in another glass container and put basic aqueous cacti solution back in original container.
 |Repeat previous step atleast 4 times total. Discard basic aqueous layer after, saving the toluene extract which contains the alkaloids.
-|To the toluene extract add 100ml H2O. Add 0.5ml concentrated HCl to this and mix well for 5 minutes. Check the pH. If it is still basic (pH 9+) then add incriments of 0.5ml HCl with mixing and checking pH until it tests acidic (below pH 7). Continue mixing for 10 minutes after. Only one acid salting pull is necessary.
+|To the toluene extract add 100ml H2O. Add 0.5ml concentrated HCl to this and mix well for 5 minutes. Check the pH. If it is still basic (pH 9+) then add incriments of 0.5ml HCl with mixing and checking pH until it tests acidic (below pH 7). Continue mixing for 10 minutes after. Only one acid salting pull is necessary, still it is a good idea to do one more just to be safe.
 |Seperate layers, hot water bath may be necessary to seperate emulsion quickly. Filter and save acidic H2O layer and discard/recycle toluene. Evaporate the aqueous layer on a dish with aid of a fan and/or hot water bath. Never use direct heat it will scorch your product. Scrape up the crystals.
 |Wash crystals with 50ml cold MEK (or anhydrous acetone, ethyl acetate). You will notice the solvent become discolored and the crystals become cleaner. Decant off the solvent carefully, leaving behind the cleaned crystals.

@@ Line 17: / Line 17: @@
 |To this add 2L H2O and simmer for 2hrs. Mix occasionally. Any cacti snot will boil off eventually and the tea should become nonviscous and watery.
 |Filter out liquid from plant matter with a cloth filter and funnel, and add the liquid to another pot. Reduce this to a low volume by boiling. Add plant material back to original pot, cover with 2L H2O, and simmer for 1hr. Mix occasionally.
-|Repeat step 3 atleast four to six times total until the liquid filtered out has very little color. Discard plant material after final time and reduce all the aqueous cacti extract to around 500 ml. This can be put in a glass pickle jar. Allow to sit overnight to precipitate unwanted fine particles, but this is optional.
+|Repeat step 3 atleast four to six times total until the liquid filtered out has very little color. Discard plant material after final time and reduce all the aqueous cacti extract to around 300 ml. This can be put in a glass pickle jar. Allow to sit overnight to precipitate unwanted fine particles, but this is optional.
 |Now it is time to basify. Mix 50g NaOH in 100ml H2O. It will get VERY hot, it is recommended to cool the mixing container while stirring with a cold water bath or under the faucet. Add the NaOH solution to the aqueous cacti extract.
 |Add 200ml toluene (or xylene) and mix for 10-15 minutes. Let the mixture settle and use a hot water bath to seperate the layers from the emulsion if necessary. The layers should seperate quickly. Seperate the layers with a pipet, separatory funnel, or syringe. Save the toluene in another glass container and put basic aqueous cacti solution back in original container.

← Older revision		Revision as of 01:58, 14 March 2014
Line 1:		Line 1:
	{{ShowInfo\|[[Image:Note_error.png]]\|'''Note:'''\|This page is a transcription of Kash's A/B Mescaline Extraction <ref>Kash's A/B Mescaline Extraction		{{ShowInfo\|[[Image:Note_error.png]]\|'''Note:'''\|This page is a transcription of Kash's A/B Mescaline Extraction <ref>Kash's A/B Mescaline Extraction
−	Revision 1.2[https://www.dmt-nexus.me/forum/default.aspx?g=posts&t=43034]</ref>. The content is to remain accurate as such.}}	+	Revision 1.3[https://www.dmt-nexus.me/forum/default.aspx?g=posts&t=43034]</ref>. The content is to remain accurate as such.}}

@@ Line 72: / Line 72: @@
+|
 *30g Citric Acid or 200ml white vinegar (10ml glacial)
--->Citric Acid Has Appears More Likely To Cause Emulsions
+-->Citric Acid Appears More Likely To Cause Emulsions
 *50g NaOH (Lye)
 *Hcl (Muriatic Acid)