BW's Bufotenine Dry Tek - Revision history

Trip: /* Base */

2022-07-04T06:02:22Z

‎Base

Trip: /* Pull */

2022-07-04T06:01:55Z

‎Pull

Trip: /* Dissolve Goo */

2022-07-04T06:01:33Z

‎Dissolve Goo

Trip: /* Dissolve Goo */

2022-07-04T06:00:16Z

‎Dissolve Goo

Trip: /* Base */

2022-06-20T08:05:18Z

‎Base

Trip: /* Base */

2022-06-20T08:03:39Z

‎Base

Trip: /* Base */

2022-06-20T08:02:27Z

‎Base

Trip: /* Dissolve Goo */

2022-06-20T07:59:25Z

‎Dissolve Goo

Trip: /* Base */

2022-06-20T07:57:23Z

‎Base

Trip: /* Base */

2022-06-20T01:44:04Z

‎Base

@@ Line 94: / Line 94: @@
 <font color="green">  Alternatively (Experimental still-but works well):
-One can do a few pulls with Ethyl Acetate and then place it in a small glass dish with xylene 1:3 ratio (amount still being confirmed). And start to evaporate it.
+One can do a few pulls with ethyl acetate only and then place it in a small glass dish with xylene 1:3 ratio (amount still being confirmed). And start to evaporate it.
 So the idea here is to pull the freebase bufotenine with EA (EA may pick up some impurities) and place it with xylene. Bufotenine wont dissolve in room temp xylene (or even heated bufotenine <139 celcius).

@@ Line 66: / Line 66: @@
 Boiling the solvent should increase solubility
-so a hot water bath is recommended. You should be using glass jars, ensure glass containers have lids to minimize evaporation of solvent.
+so a hot water bath is recommended (no open flames near solvent). You should be using glass jars, ensure glass containers have lids to minimize evaporation of solvent.
 == Salting ==

← Older revision		Revision as of 06:01, 4 July 2022
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−	If the ratio's are off and a blob or crystals do not form you can evaporate the water with the freebase still in it and proceed to next step-Note if you evap results will be more impure.	+	If the ratio's are off and a blob or crystals do not form you can evaporate the water with the freebase still in it and proceed to next step. You will be left with a mix 'dry' of freebase alkaloids and sodium carbonate. Proceed to the next step and pull with EA/Naphtha.
		+
		+	Note if you evap results will be more impure.

	== Base ==		== Base ==

@@ Line 78: / Line 78: @@
 == Dissolve Goo ==
 - Dissolve the Alkaloid-Fumarate crystals (or citrate) in 25 ml hot water. Slowly pour another a solution of 1,85 g Na2CO3 (0,5:1 Na2CO3:Alkaloid-Fumarates) in 25 ml water. This will form impure freebase bufotenine (either as a blob or crystal if you defatted adequately enough). Decant water.
 If the ratio's are off and a blob or crystals do not form you can evaporate the water with the freebase still in it and proceed to next step-Note if you evap results will be more impure.

@@ Line 94: / Line 94: @@
 Since EA boils at 70 degrees and xylene at 140 degrees celcius, the idea is to let half the EA/ Xylene mix evaporate. At this point majority if not all the EA should have evaporated out leaving behind xylene only. Xylene won't hold bufotenine freebase so it crashes out as a white residue/ crystal. The majority of the impurities stay in the xylene as it is quite a large spectrum solvent. Once the bufotenine crashes out one can decant the xylene and dry the dish for bufo crystals. Crystals will be white but as you scrape it up it may become slightly brown (it will sometimes stay as white crystals). The browning that can occur is believed to do with over evaporating the xylene, xylene and EA ratios, and or depends on how well the de-fatting was performed.
-Keep decant xylene for the next run/ extraction, it may contain tiny amounts of EA and therefore bufo.
+Keep decanted xylene for the next run/ extraction, it may contain tiny amounts of EA and therefore bufo.
 Note: The alternative method is safer than boiling xylene and may pull more efficiently than EA/Naphtha mix. Note MS-LC data on this method has not be compiled.

@@ Line 92: / Line 92: @@
 So the idea here is to pull the freebase bufotenine with EA (EA may pick up some impurities) and place it with xylene. Bufotenine wont dissolve in room temp xylene (or even heated bufotenine <139 celcius).
-Since EA boils at 70 degrees and xylene at 140 degrees celcius, the idea is to let half the EA/ Xylene mix evaporate. At this point majority if not all the EA should have evaporated out leaving behind xylene only. Xylene won't hold bufotenine freebase so it crashes out as a white residue/ crystal. The majority of the impurities stay in the xylene as it is quite a large spectrum solvent. Once the bufotenine crashes out one can decant the xylene and dry the dish for bufo crystals. Crystals will be white but as you scrape can become slightly brown (it sometime stays white). The browning that can occur is believed to do with xylene and EA ratios as well as how well the de-fatting was performed.
+Since EA boils at 70 degrees and xylene at 140 degrees celcius, the idea is to let half the EA/ Xylene mix evaporate. At this point majority if not all the EA should have evaporated out leaving behind xylene only. Xylene won't hold bufotenine freebase so it crashes out as a white residue/ crystal. The majority of the impurities stay in the xylene as it is quite a large spectrum solvent. Once the bufotenine crashes out one can decant the xylene and dry the dish for bufo crystals. Crystals will be white but as you scrape it up it may become slightly brown (it will sometime stay as white crystals). The browning that can occur is believed to do with over evaporating the xylene, xylene and EA ratios, and or depend son how well the de-fatting was performed.
 Keep decant xylene for the next run/ extraction, it may contain tiny amounts of EA and therefore bufo.

@@ Line 79: / Line 79: @@
 - Dissolve the Alkaloid-Fumarate crystals (or citrate) in 25 ml hot water. Slowly pour another a solution of 1,85 g Na2CO3 (0,5:1 Na2CO3:Alkaloid-Fumarates) in 25 ml water. This will form impure freebase bufotenine (either as a blob or crystal if you defatted adequately enough). Decant water.
-If the ratio's are off and a blob or crystals do not form you can evaporate the water with the freebase and proceed to next step-Note if you evap results will be more impure.
+If the ratio's are off and a blob or crystals do not form you can evaporate the water with the freebase still in it and proceed to next step-Note if you evap results will be more impure.
 == Base ==

@@ Line 87: / Line 87: @@
-<font color="blue">  Alternatively (Experimental still-but works well):
+<font color="green">  Alternatively (Experimental still-but works well):
 One can do a few pulls with Ethyl Acetate and then place it in a small glass dish with xylene 1:3 ratio (amount still being confirmed). And start to evaporate it.
@@ Line 96: / Line 96: @@
 Note: The alternative method is safer than boiling xylene and may pull more efficiently than EA/Naphtha mix. Note MS-LC data on this method has not be compiled.
 <font color="white">
 == Crash/ Filter TEK Complete ==