https://wiki.dmt-nexus.me/w/api.php?action=feedcontributions&feedformat=atom&user=Trip 2026-04-07T17:21:30Z User contributions MediaWiki 1.22.1 https://wiki.dmt-nexus.me/Ethyl_Acetate_Approach_Harmala 2024-06-23T08:17:59Z

<p>Trip: /* Dissolve Goo */</p> <hr /> <div>= Introduction =<br /> <br /> ==Background &amp; acknowledgements==<br /> This Tek was inspired by Loveall's Cielo Tek, with the aim of cutting out Manske steps to aid in yields and substantially quicken the process while maintaining purity. The quickest run has been 2.5hours with decent yields and purity.<br /> <br /> Thanks to everyone who has contributed or helped experiment to aid in refining/ improving this process: Loveall, Benzyme, Downwardsfromzero, _Trip_, and others.<br /> <br /> This Tek is still a work in progress&lt;ref&gt;Forum Link[https://www.dmt-nexus.me/forum/default.aspx?g=posts&amp;t=93378]&lt;/ref&gt; however lab and test results have been confirmed and are very promising for a quick Tek. Feel free to contribute. More photo's to follow soon.<br /> <br /> Please take your time with your first extraction, although this is a quick and easy Tek you don't want to rush it and make a mistake.<br /> <br /> = Safety = <br /> Review ethyl acetate&lt;ref&gt;Ethyl acetate safety[https://www.msdsonline.com/2015/04/10/ethyl-acetate-a-sweet-smelling-safety-hazard/#:~:text=Ethyl%20acetate%20is%20highly%20flammable,with%20the%20eyes%20or%20skin.]&lt;/ref&gt; and citric acid&lt;ref&gt;Citric Acid Safety[https://wiki.dmt-nexus.me/Citric_Acid_Safety#Process_.F0.9F.A5.9E]&lt;/ref&gt; safety information. Verify solvent MSDS, plastic compatibility, and clean evaporation.<br /> <br /> This TEK is food safe if food grade materials are used.<br /> <br /> <br /> Following this advice does not guarantee safety. It is up to each adult individual to make their own personal decisions.<br /> <br /> <br /> ==Consumables==<br /> *300ml water/ 600-800ml of distilled water (tap water works fine too) <br /> *25g Ca(OH)<br /> *100g of Syrian Rue seeds (B. Caapi should work too but is yet to be tested).<br /> *1lt ethyl acetate (sometimes sold as &quot;MEK substitute&quot;)<br /> *10-15g of citric acid <br /> *Sodium Carbonate<br /> *1lt Jar<br /> <br /> ==Equipment==<br /> *Blender<br /> *French press <br /> *Kitchen scale <br /> *Coffee filters, support basket, and funnel Or lab filter and vacuum pump.<br /> *1lt mason glass jars with lids<br /> *Fridge <br /> *Milligram scale <br /> *Microwave<br /> <br /> <br /> <br /> = Detailed Process =<br /> <br /> <br /> == Base Water ==<br /> -Add 300ml of water to 25g of calcium hydroxide and mix to form 'base water'.<br /> Alternatively one can use sodium carbonate (this may negate the need for filtering later). <br /> Note: Sodium Carbonate has not been fully tested start to finish.<br /> <br /> == Powder ==<br /> -Get 100g of rue seeds and grind them up, mix with 'base water'. A glass blender is quickest.<br /> <br /> == Microwave ==<br /> -Microwave the rue/base mix until close to 2/3rd's of the water content is steamed off (use kitchen scales to measure this). As a guide a 750 watt microwave at 5-7min bursts should work fine. Mix between bursts. Several bursts will be required. <br /> <br /> If interested, see further investigations for microwaving below.<br /> <br /> == Water Bath ==<br /> -Prepare a warm water bath with boiling water and warm 1lt of EA. No open flames. (This step helps yields).<br /> <br /> == Pulling ==<br /> -Place ground up 'base paste rue seed mix' in a french press. Using the french press conduct 6 pulls with the 1lt of warm EA. So 6x 160ml pulls approx (keep in mind rue seeds will absorb a little bit of EA). Carefully decant into 1lt jar(6x warm pulls at 1-2 mins each). Decant from the french press after each pull. Keep rue base mix and fresh EA in the warm water bath to improve yield (obviously in their respective containers).<br /> <br /> == Recovery/ Filter ==<br /> -Approx just over 800ml of EA should be recovered and then filtered (filtering may not be necessary if one has used sodium carbonate as a base, this is still under investigation). Lab filter is recommended, coffee filters should work too.<br /> <br /> <br /> [[File:Download.jpeg-2.jpg]] [[File:Images.jpeg-6.jpg]] ‎<br /> <br /> <br /> <br /> <br /> <br /> Recovered vs Filtered<br /> <br /> == Salting ==<br /> -Add 15g of citirc acid to the combined EA pulls (the approx 800ml of EA) and shake for 5-10mins (red/orange/yellow oil should form very fast). Orange/red goo forms at the base of the jar and the rest of the jar gets covered with sticky yellow goo (making it easy to decant). (This goo should crystalize if left for 24hours+. This is not necessary though, the goo makes decanting easy so one can decant right away).<br /> <br /> [[File:Download.jpeg-1.jpg ]] (Initial clouding when adding citric acid).<br /> <br /> [[File:Images.jpeg-10.jpg]] <br /> (Don't let the photo deceive you the whole Jar is covered in sticky yellow harmala citrate residue).<br /> <br /> == Decant &amp; Reclaim ==<br /> -Decant EA (this can be cleaned and reused next extraction). One can also add a little bit of EA to the citrate stuck to the jar to clean it up a little bit but it is not necessary. Again decant this EA.<br /> <br /> == Dissolve Goo ==<br /> -After the tiny amount of EA still left in the jar evaporates off the goo, add minimum 850ml of warm water to the citrate goo, it will dissolve fairly quickly. <br /> <br /> (One can ratio it down if using less seeds). The more water used gives a cleaner product (in appearance anyway). One can use even more water 1lt-1.5lt to achieve a whiter end result (see further investigation notes on use of too much water in this step).<br /> <br /> <br /> <br /> [[File:20220415 182000.jpg]] <br /> <br /> <br /> <br /> Above is a photo comparing the final end result, more vs less water used in this step. (1lt vs 300ml). Yet purity still tested the same.<br /> <br /> == Base ==<br /> -Base slowly with sodium carbonate (you can shake up the jar to get excess sodium carbonate to dissolve once the acid is neutralized). Add enough sodium carbonate until the harmala starts to crash out then add a little bit more.<br /> <br /> [[File:Images.jpeg-9.jpg ]] Initial basing &amp; precipitation.<br /> <br /> == Crash/ Filter TEK Complete ==<br /> -Harmala will crash out quickly. Some of the FB harmala will float to the top, this needs to be left to cool.<br /> (Sticking the jar in a freezer '''appears''' to speed up the process and harmala crashes as it cools. The floating harmala should settle. This should not take long). <br /> <br /> [[File:Index1.jpg]] Crashing of Harmala (some will float to the top some settles to the bottom).<br /> <br /> [[File:Images.jpeg-8.jpg]] '''As a rule of thumb I wait for majority of the floating harmala to settle to the bottom'''. This rarely exceeds the 2 hour mark, again usually a lot quicker - as little as half an hour. However, one can filter straight away.<br /> <br /> <br /> <br /> Once it has finished crashing out filter and dry the product (lab filters or coffee filters should work fine). <br /> <br /> <br /> Well done this should have been a quick and easy run. '''3.7%+''' is usually the minimum percentage pulled on first run. The process can be repeated on spent material and re-pulled with hot EA to get over '''5%'''.<br /> Final product is usually off white almost greyish in color harmala. It doesn't necessarily represent purity in this Tek and color appears to be dependent on how much water was used during dissolving and basing step. If you <br /> look at lab sample B vs C, sample C had extra clean up steps added (and although the signals appear slightly clearer) sample C came out more of a tan color than off white/grey. <br /> If one is after a purer looking product you can do a 5% ammonia wash during the final filter before drying (this has reported to clean up harmala).<br /> <br /> [[File:Download.jpeg.jpg ‎]]<br /> <br /> <br /> No need to leave the product overnight to crash, if left for too long (say 24hrs+) some impurities appear to crash out with it. The final product in this step should crash out quick and should/ can be filtered within a hour or 2 (often quicker). <br /> Once filtered and dried you have the final product.<br /> <br /> (Keep the sodium carbonated water after filtering, more harmala may crash out overnight. It usually appears more impure by color and may contain impurities though an analysis has not been confirmed. It is likely still useable)<br /> <br /> == Lab Analysis ==<br /> [[File: A1.jpg]]<br /> <br /> Above is harmala lab analysis results.<br /> Figure A is the traditional 3x Manske, figure B &amp; C are from the EA approach (B &amp; C were conducted with slightly different variations). Figure B is the standard EA approach TEK as written above.<br /> The peaks indicate very clean harmine/harmaline. All main peaks can be attributed to harmala even 197 represent harmala with the loss -CH3 or and 169 is likely loss of -OCH3 functional groups during LC-MS. Results run in positive mode adds M 1+.<br /> <br /> == Further investigations ==<br /> -Sodium Carbonate should be usable as a base for this Tek but it's yet to be confirmed.<br /> <br /> -Chemical drying solvent after pulls only slightly changes the end result/ purity and is not necessary based of lab results..<br /> <br /> -A mini A/B at the end for clean up does not appear to change end result/ purity (it will likely make the harmala darker in appearance, reasons unknown).<br /> <br /> -Other acids are yet to be tested. Fumaric acid was briefly tested and should work. Phosphoric acid has been limitedly tested appears to behave like citric acid.<br /> <br /> -Microwave route may be unnecessary as eventually discovered with the Cielo Tek. If this is the case, water content in the first step may need to be reduced below 300ml. This may be like the Cielo Tek and require more water to facilitate efficient pulls, thus may need to be fine tuned. And like the Cielo tek may not need microwaving. However for now, those ratios and the microwave step should work fine so stick with these values and the use of a microwave.<br /> <br /> -Dissolving the goo in more water appears to give a purer looking product, using too little amount of water gives a very impure looking product. The ideal ratio is yet to be worked out. This may not affect purity to a great degree. Lab results have shown color doesn't necessarily equal purity in this tek. More water may lengthen the time needed to crash out harmala and or reduce yields. Note, this doesn't seem to be the case but further tests are needed.<br /> <br /> -This process will likely work with B. Caapi but has yet been tested but should work fine.<br /> <br /> -Butyl acetate does not appear to work effectively and harmala citrate will not crash out of BA.<br /> <br /> == Reuse ==<br /> Reusing solvents is encouraged&lt;ref&gt;On reusing non polar solvent[https://www.dmt-nexus.me/forum/default.aspx?g=posts&amp;t=31398]&lt;/ref&gt; at the DMT nexus.<br /> <br /> <br /> Wash spent extract with sodium carbonate saturated water (35% by weight). About 1/5 of the solvent volume as saturated water is enough. Shake vigorously (emulsions do not form). CO2 bubbles may be visible during citric acid neutralization. Keep an eye on any bubbles and release any pressure buildup regularly. Neutralization can be optionally verified with pH paper. Rest washed solution until clear (up to a day or more).<br /> <br /> <br /> Remove the water layer with a pipette or separatory funnel. Freezing the solvent and filtering the ice slush that forms with a metal strainer is also an option. Finally, decant off any excess solid sodium carbonate/citrate. CaCl2 (sold as deicer, calcium hardener for pools and sometimes is the only ingredient in moisture absorbers tubs) can be used to ensure there is no water still left in the EA.<br /> <br /> == References ==<br /> &lt;references/&gt;</div>

Trip https://wiki.dmt-nexus.me/Ethyl_Acetate_Approach_Harmala 2024-06-23T08:13:18Z

<p>Trip: /* Preliminary note */</p> <hr /> <div>= Introduction =<br /> <br /> ==Background &amp; acknowledgements==<br /> This Tek was inspired by Loveall's Cielo Tek, with the aim of cutting out Manske steps to aid in yields and substantially quicken the process while maintaining purity. The quickest run has been 2.5hours with decent yields and purity.<br /> <br /> Thanks to everyone who has contributed or helped experiment to aid in refining/ improving this process: Loveall, Benzyme, Downwardsfromzero, _Trip_, and others.<br /> <br /> This Tek is still a work in progress&lt;ref&gt;Forum Link[https://www.dmt-nexus.me/forum/default.aspx?g=posts&amp;t=93378]&lt;/ref&gt; however lab and test results have been confirmed and are very promising for a quick Tek. Feel free to contribute. More photo's to follow soon.<br /> <br /> Please take your time with your first extraction, although this is a quick and easy Tek you don't want to rush it and make a mistake.<br /> <br /> = Safety = <br /> Review ethyl acetate&lt;ref&gt;Ethyl acetate safety[https://www.msdsonline.com/2015/04/10/ethyl-acetate-a-sweet-smelling-safety-hazard/#:~:text=Ethyl%20acetate%20is%20highly%20flammable,with%20the%20eyes%20or%20skin.]&lt;/ref&gt; and citric acid&lt;ref&gt;Citric Acid Safety[https://wiki.dmt-nexus.me/Citric_Acid_Safety#Process_.F0.9F.A5.9E]&lt;/ref&gt; safety information. Verify solvent MSDS, plastic compatibility, and clean evaporation.<br /> <br /> This TEK is food safe if food grade materials are used.<br /> <br /> <br /> Following this advice does not guarantee safety. It is up to each adult individual to make their own personal decisions.<br /> <br /> <br /> ==Consumables==<br /> *300ml water/ 600-800ml of distilled water (tap water works fine too) <br /> *25g Ca(OH)<br /> *100g of Syrian Rue seeds (B. Caapi should work too but is yet to be tested).<br /> *1lt ethyl acetate (sometimes sold as &quot;MEK substitute&quot;)<br /> *10-15g of citric acid <br /> *Sodium Carbonate<br /> *1lt Jar<br /> <br /> ==Equipment==<br /> *Blender<br /> *French press <br /> *Kitchen scale <br /> *Coffee filters, support basket, and funnel Or lab filter and vacuum pump.<br /> *1lt mason glass jars with lids<br /> *Fridge <br /> *Milligram scale <br /> *Microwave<br /> <br /> <br /> <br /> = Detailed Process =<br /> <br /> <br /> == Base Water ==<br /> -Add 300ml of water to 25g of calcium hydroxide and mix to form 'base water'.<br /> Alternatively one can use sodium carbonate (this may negate the need for filtering later). <br /> Note: Sodium Carbonate has not been fully tested start to finish.<br /> <br /> == Powder ==<br /> -Get 100g of rue seeds and grind them up, mix with 'base water'. A glass blender is quickest.<br /> <br /> == Microwave ==<br /> -Microwave the rue/base mix until close to 2/3rd's of the water content is steamed off (use kitchen scales to measure this). As a guide a 750 watt microwave at 5-7min bursts should work fine. Mix between bursts. Several bursts will be required. <br /> <br /> If interested, see further investigations for microwaving below.<br /> <br /> == Water Bath ==<br /> -Prepare a warm water bath with boiling water and warm 1lt of EA. No open flames. (This step helps yields).<br /> <br /> == Pulling ==<br /> -Place ground up 'base paste rue seed mix' in a french press. Using the french press conduct 6 pulls with the 1lt of warm EA. So 6x 160ml pulls approx (keep in mind rue seeds will absorb a little bit of EA). Carefully decant into 1lt jar(6x warm pulls at 1-2 mins each). Decant from the french press after each pull. Keep rue base mix and fresh EA in the warm water bath to improve yield (obviously in their respective containers).<br /> <br /> == Recovery/ Filter ==<br /> -Approx just over 800ml of EA should be recovered and then filtered (filtering may not be necessary if one has used sodium carbonate as a base, this is still under investigation). Lab filter is recommended, coffee filters should work too.<br /> <br /> <br /> [[File:Download.jpeg-2.jpg]] [[File:Images.jpeg-6.jpg]] ‎<br /> <br /> <br /> <br /> <br /> <br /> Recovered vs Filtered<br /> <br /> == Salting ==<br /> -Add 15g of citirc acid to the combined EA pulls (the approx 800ml of EA) and shake for 5-10mins (red/orange/yellow oil should form very fast). Orange/red goo forms at the base of the jar and the rest of the jar gets covered with sticky yellow goo (making it easy to decant). (This goo should crystalize if left for 24hours+. This is not necessary though, the goo makes decanting easy so one can decant right away).<br /> <br /> [[File:Download.jpeg-1.jpg ]] (Initial clouding when adding citric acid).<br /> <br /> [[File:Images.jpeg-10.jpg]] <br /> (Don't let the photo deceive you the whole Jar is covered in sticky yellow harmala citrate residue).<br /> <br /> == Decant &amp; Reclaim ==<br /> -Decant EA (this can be cleaned and reused next extraction). One can also add a little bit of EA to the citrate stuck to the jar to clean it up a little bit but it is not necessary. Again decant this EA.<br /> <br /> == Dissolve Goo ==<br /> -After the tiny amount of EA still left in the jar evaporates off the goo, add minimum 850ml of warm water to the citrate goo, it will dissolve fairly quickly. <br /> <br /> (One can ratio it down if using less seeds). The more water used gives a cleaner product (in appearance anyway). One can use even more water 1lt-1.5lt to achieve a whiter end result (see further investigation notes on use of too much water in this step).<br /> <br /> <br /> <br /> [[File:20220415 182000.jpg]] <br /> <br /> <br /> <br /> Above is a photo comparing the final end result, more vs less water used in this step. (1lt vs 300ml)<br /> <br /> == Base ==<br /> -Base slowly with sodium carbonate (you can shake up the jar to get excess sodium carbonate to dissolve once the acid is neutralized). Add enough sodium carbonate until the harmala starts to crash out then add a little bit more.<br /> <br /> [[File:Images.jpeg-9.jpg ]] Initial basing &amp; precipitation.<br /> <br /> == Crash/ Filter TEK Complete ==<br /> -Harmala will crash out quickly. Some of the FB harmala will float to the top, this needs to be left to cool.<br /> (Sticking the jar in a freezer '''appears''' to speed up the process and harmala crashes as it cools. The floating harmala should settle. This should not take long). <br /> <br /> [[File:Index1.jpg]] Crashing of Harmala (some will float to the top some settles to the bottom).<br /> <br /> [[File:Images.jpeg-8.jpg]] '''As a rule of thumb I wait for majority of the floating harmala to settle to the bottom'''. This rarely exceeds the 2 hour mark, again usually a lot quicker - as little as half an hour. However, one can filter straight away.<br /> <br /> <br /> <br /> Once it has finished crashing out filter and dry the product (lab filters or coffee filters should work fine). <br /> <br /> <br /> Well done this should have been a quick and easy run. '''3.7%+''' is usually the minimum percentage pulled on first run. The process can be repeated on spent material and re-pulled with hot EA to get over '''5%'''.<br /> Final product is usually off white almost greyish in color harmala. It doesn't necessarily represent purity in this Tek and color appears to be dependent on how much water was used during dissolving and basing step. If you <br /> look at lab sample B vs C, sample C had extra clean up steps added (and although the signals appear slightly clearer) sample C came out more of a tan color than off white/grey. <br /> If one is after a purer looking product you can do a 5% ammonia wash during the final filter before drying (this has reported to clean up harmala).<br /> <br /> [[File:Download.jpeg.jpg ‎]]<br /> <br /> <br /> No need to leave the product overnight to crash, if left for too long (say 24hrs+) some impurities appear to crash out with it. The final product in this step should crash out quick and should/ can be filtered within a hour or 2 (often quicker). <br /> Once filtered and dried you have the final product.<br /> <br /> (Keep the sodium carbonated water after filtering, more harmala may crash out overnight. It usually appears more impure by color and may contain impurities though an analysis has not been confirmed. It is likely still useable)<br /> <br /> == Lab Analysis ==<br /> [[File: A1.jpg]]<br /> <br /> Above is harmala lab analysis results.<br /> Figure A is the traditional 3x Manske, figure B &amp; C are from the EA approach (B &amp; C were conducted with slightly different variations). Figure B is the standard EA approach TEK as written above.<br /> The peaks indicate very clean harmine/harmaline. All main peaks can be attributed to harmala even 197 represent harmala with the loss -CH3 or and 169 is likely loss of -OCH3 functional groups during LC-MS. Results run in positive mode adds M 1+.<br /> <br /> == Further investigations ==<br /> -Sodium Carbonate should be usable as a base for this Tek but it's yet to be confirmed.<br /> <br /> -Chemical drying solvent after pulls only slightly changes the end result/ purity and is not necessary based of lab results..<br /> <br /> -A mini A/B at the end for clean up does not appear to change end result/ purity (it will likely make the harmala darker in appearance, reasons unknown).<br /> <br /> -Other acids are yet to be tested. Fumaric acid was briefly tested and should work. Phosphoric acid has been limitedly tested appears to behave like citric acid.<br /> <br /> -Microwave route may be unnecessary as eventually discovered with the Cielo Tek. If this is the case, water content in the first step may need to be reduced below 300ml. This may be like the Cielo Tek and require more water to facilitate efficient pulls, thus may need to be fine tuned. And like the Cielo tek may not need microwaving. However for now, those ratios and the microwave step should work fine so stick with these values and the use of a microwave.<br /> <br /> -Dissolving the goo in more water appears to give a purer looking product, using too little amount of water gives a very impure looking product. The ideal ratio is yet to be worked out. This may not affect purity to a great degree. Lab results have shown color doesn't necessarily equal purity in this tek. More water may lengthen the time needed to crash out harmala and or reduce yields. Note, this doesn't seem to be the case but further tests are needed.<br /> <br /> -This process will likely work with B. Caapi but has yet been tested but should work fine.<br /> <br /> -Butyl acetate does not appear to work effectively and harmala citrate will not crash out of BA.<br /> <br /> == Reuse ==<br /> Reusing solvents is encouraged&lt;ref&gt;On reusing non polar solvent[https://www.dmt-nexus.me/forum/default.aspx?g=posts&amp;t=31398]&lt;/ref&gt; at the DMT nexus.<br /> <br /> <br /> Wash spent extract with sodium carbonate saturated water (35% by weight). About 1/5 of the solvent volume as saturated water is enough. Shake vigorously (emulsions do not form). CO2 bubbles may be visible during citric acid neutralization. Keep an eye on any bubbles and release any pressure buildup regularly. Neutralization can be optionally verified with pH paper. Rest washed solution until clear (up to a day or more).<br /> <br /> <br /> Remove the water layer with a pipette or separatory funnel. Freezing the solvent and filtering the ice slush that forms with a metal strainer is also an option. Finally, decant off any excess solid sodium carbonate/citrate. CaCl2 (sold as deicer, calcium hardener for pools and sometimes is the only ingredient in moisture absorbers tubs) can be used to ensure there is no water still left in the EA.<br /> <br /> == References ==<br /> &lt;references/&gt;</div>

Trip https://wiki.dmt-nexus.me/Ethyl_Acetate_Approach_Harmala 2023-10-06T04:20:51Z

<p>Trip: /* Introduction */</p> <hr /> <div>= Introduction =<br /> <br /> ==Although this tek is a quick easy way to yield harmala, BW's latest lab results indicate that a traditional extraction without manske may be almost as quick tek with better yields. (Although the harmala will be more impure by color the lab results indicate very clean haramala and no signs of other quinasoline alkaloids such as vasicine etc)==<br /> This Tek was inspired by Loveall's Cielo Tek, with the aim of cutting out manske steps to aid in yields and substantially quicken the process while maintaining purity. The quickest run has been 2.5hours with decent yields and purity.<br /> <br /> Thanks to everyone who has contributed or helped experiment to aid in refining/ improving this process: Loveall, Benzyme, Downwardsfromzero, _Trip_, and others.<br /> <br /> This Tek is still a work in progress&lt;ref&gt;Forum Link[https://www.dmt-nexus.me/forum/default.aspx?g=posts&amp;t=93378]&lt;/ref&gt; however lab and test results have been confirmed and are very promising for a quick Tek. Feel free to contribute. More photo's to follow soon.<br /> <br /> Please take your time with your first extraction, although this is a quick and easy Tek you don't want to rush it and make a mistake.<br /> <br /> = Safety = <br /> Review ethyl acetate&lt;ref&gt;Ethyl acetate safety[https://www.msdsonline.com/2015/04/10/ethyl-acetate-a-sweet-smelling-safety-hazard/#:~:text=Ethyl%20acetate%20is%20highly%20flammable,with%20the%20eyes%20or%20skin.]&lt;/ref&gt; and citric acid&lt;ref&gt;Citric Acid Safety[https://wiki.dmt-nexus.me/Citric_Acid_Safety#Process_.F0.9F.A5.9E]&lt;/ref&gt; safety information. Verify solvent MSDS, plastic compatibility, and clean evaporation.<br /> <br /> This TEK is food safe if food grade materials are used.<br /> <br /> <br /> Following this advice does not guarantee safety. It is up to each adult individual to make their own personal decisions.<br /> <br /> <br /> ==Consumables==<br /> *300ml water/ 600-800ml of distilled water (tap water works fine too) <br /> *25g Ca(OH)<br /> *100g of Syrian Rue seeds (B. Caapi should work too but is yet to be tested).<br /> *1lt ethyl acetate (sometimes sold as &quot;MEK substitute&quot;)<br /> *10-15g of citric acid <br /> *Sodium Carbonate<br /> *1lt Jar<br /> <br /> ==Equipment==<br /> *Blender<br /> *French press <br /> *Kitchen scale <br /> *Coffee filters, support basket, and funnel Or lab filter and vacuum pump.<br /> *1lt mason glass jars with lids<br /> *Fridge <br /> *Milligram scale <br /> *Microwave<br /> <br /> <br /> <br /> = Detailed Process =<br /> <br /> <br /> == Base Water ==<br /> -Add 300ml of water to 25g of calcium hydroxide and mix to form 'base water'.<br /> Alternatively one can use sodium carbonate (this may negate the need for filtering later). <br /> Note: Sodium Carbonate has not been fully tested start to finish.<br /> <br /> == Powder ==<br /> -Get 100g of rue seeds and grind them up, mix with 'base water'. A glass bender is quickest.<br /> <br /> == Microwave ==<br /> -Microwave the rue/base mix until close to 2/3rd's of the water content is steamed off (use kitchen scales to measure this). As a guide a 750 watt microwave at 5-7min bursts should work fine. Mix between bursts. Several bursts will be required. <br /> <br /> If interested, see further investigations for microwaving below.<br /> <br /> == Water Bath ==<br /> -Prepare a warm water bath with boiling water and warm 1lt of EA. No open flames. (This step helps yields).<br /> <br /> == Pulling ==<br /> -Place ground up 'base paste rue seed mix' in a french press. Using the french press conduct 6 pulls with the 1lt of warm EA. So 6x 160ml pulls approx (keep in mind rue seeds will absorb a little bit of EA). Carefully decant into 1lt jar(6x warm pulls at 1-2 mins each). Decant from the french press after each pull. Keep rue base mix and fresh EA in the warm water bath to improve yield (obviously in their respective containers).<br /> <br /> == Recovery/ Filter ==<br /> -Approx just over 800ml of EA should be recovered and then filtered (filtering may not be necessary if one has used sodium carbonate as a base, this is still under investigation). Lab filter is recommended, coffee filters should work too.<br /> <br /> <br /> [[File:Download.jpeg-2.jpg]] [[File:Images.jpeg-6.jpg]] ‎<br /> <br /> <br /> <br /> <br /> <br /> Recovered vs Filtered<br /> <br /> == Salting ==<br /> -Add 15g of citirc acid to the combined EA pulls (the approx 800ml of EA) and shake for 5-10mins (red/orange/yellow oil should form very fast). Orange/red goo forms at the base of the jar and the rest of the jar gets covered with sticky yellow goo (making it easy to decant). (This goo should crystalize if left for 24hours+. This is not necessary though, the goo makes decanting easy so one can decant right away).<br /> <br /> [[File:Download.jpeg-1.jpg ]] (Initial clouding when adding citric acid).<br /> <br /> [[File:Images.jpeg-10.jpg]] <br /> (Don't let the photo deceive you the whole Jar is covered in sticky yellow harmala citrate residue).<br /> <br /> == Decant &amp; Reclaim ==<br /> -Decant EA (this can be cleaned and reused next extraction). One can also add a little bit of EA to the citrate stuck to the jar to clean it up a little bit but it is not necessary. Again decant this EA.<br /> <br /> == Dissolve Goo ==<br /> -After the tiny amount of EA still left in the jar evaporates off the goo, add minimum 850ml of warm water to the citrate goo, it will dissolve fairly quickly. <br /> <br /> (One can ratio it down if using less seeds). The more water used gives a cleaner product (in appearance anyway). One can use even more water 1lt-1.5lt to achieve a whiter end result (see further investigation notes on use of too much water in this step).<br /> <br /> <br /> <br /> [[File:20220415 182000.jpg]] <br /> <br /> <br /> <br /> Above is a photo comparing the final end result, more vs less water used in this step. (1lt vs 300ml)<br /> <br /> == Base ==<br /> -Base slowly with sodium carbonate (you can shake up the jar to get excess sodium carbonate to dissolve once the acid is neutralized). Add enough sodium carbonate until the harmala starts to crash out then add a little bit more.<br /> <br /> [[File:Images.jpeg-9.jpg ]] Initial basing &amp; precipitation.<br /> <br /> == Crash/ Filter TEK Complete ==<br /> -Harmala will crash out quickly. Some of the FB harmala will float to the top, this needs to be left to cool.<br /> (Sticking the jar in a freezer '''appears''' to speed up the process and harmala crashes as it cools. The floating harmala should settle. This should not take long). <br /> <br /> [[File:Index1.jpg]] Crashing of Harmala (some will float to the top some settles to the bottom).<br /> <br /> [[File:Images.jpeg-8.jpg]] '''As a rule of thumb I wait for majority of the floating harmala to settle to the bottom'''. This rarely exceeds the 2 hour mark, again usually a lot quicker - as little as half an hour. However, one can filter straight away.<br /> <br /> <br /> <br /> Once it has finished crashing out filter and dry the product (lab filters or coffee filters should work fine). <br /> <br /> <br /> Well done this should have been a quick and easy run. '''3.7%+''' is usually the minimum percentage pulled on first run. The process can be repeated on spent material and re-pulled with hot EA to get over '''5%'''.<br /> Final product is usually off white almost greyish in color harmala. It doesn't necessarily represent purity in this Tek and color appears to be dependent on how much water was used during dissolving and basing step. If you <br /> look at lab sample B vs C, sample C had extra clean up steps added (and although the signals appear slightly clearer) sample C came out more of a tan color than off white/grey. <br /> If one is after a purer looking product you can do a 5% ammonia wash during the final filter before drying (this has reported to clean up harmala).<br /> <br /> [[File:Download.jpeg.jpg ‎]]<br /> <br /> <br /> No need to leave the product overnight to crash, if left for too long (say 24hrs+) some impurities appear to crash out with it. The final product in this step should crash out quick and should/ can be filtered within a hour or 2 (often quicker). <br /> Once filtered and dried you have the final product.<br /> <br /> (Keep the sodium carbonated water after filtering, more harmala may crash out overnight. It usually appears more impure by color and may contain impurities though an analysis has not been confirmed. It is likely still useable)<br /> <br /> == Lab Analysis ==<br /> [[File: A1.jpg]]<br /> <br /> Above is harmala lab analysis results.<br /> Figure A is the traditional 3x Manske, figure B &amp; C are from the EA approach (B &amp; C were conducted with slightly different variations). Figure B is the standard EA approach TEK as written above.<br /> The peaks indicate very clean harmine/harmaline. All main peaks can be attributed to harmala even 197 represent harmala with the loss -CH3 or and 169 is likely loss of -OCH3 functional groups during LC-MS. Results run in positive mode adds M 1+.<br /> <br /> == Further investigations ==<br /> -Sodium Carbonate should be usable as a base for this Tek but it's yet to be confirmed.<br /> <br /> -Chemical drying solvent after pulls only slightly changes the end result/ purity and is not necessary based of lab results..<br /> <br /> -A mini A/B at the end for clean up does not appear to change end result/ purity (it will likely make the harmala darker in appearance, reasons unknown).<br /> <br /> -Other acids are yet to be tested. Fumaric acid was briefly tested and should work. Phosphoric acid has been limitedly tested appears to behave like citric acid.<br /> <br /> -Microwave route may be unnecessary as eventually discovered with the Cielo Tek. If this is the case, water content in the first step may need to be reduced below 300ml. This may be like the Cielo Tek and require more water to facilitate efficient pulls, thus may need to be fine tuned. And like the Cielo tek may not need microwaving. However for now, those ratios and the microwave step should work fine so stick with these values and the use of a microwave.<br /> <br /> -Dissolving the goo in more water appears to give a purer looking product, using too little amount of water gives a very impure looking product. The ideal ratio is yet to be worked out. This may not affect purity to a great degree. Lab results have shown color doesn't necessarily equal purity in this tek. More water may lengthen the time needed to crash out harmala and or reduce yields. Note, this doesn't seem to be the case but further tests are needed.<br /> <br /> -This process will likely work with B. Caapi but has yet been tested but should work fine.<br /> <br /> -Butyl acetate does not appear to work effectively and harmala citrate will not crash out of BA.<br /> <br /> == Reuse ==<br /> Reusing solvents is encouraged&lt;ref&gt;On reusing non polar solvent[https://www.dmt-nexus.me/forum/default.aspx?g=posts&amp;t=31398]&lt;/ref&gt; at the DMT nexus.<br /> <br /> <br /> Wash spent extract with sodium carbonate saturated water (35% by weight). About 1/5 of the solvent volume as saturated water is enough. Shake vigorously (emulsions do not form). CO2 bubbles may be visible during citric acid neutralization. Keep an eye on any bubbles and release any pressure buildup regularly. Neutralization can be optionally verified with pH paper. Rest washed solution until clear (up to a day or more).<br /> <br /> <br /> Remove the water layer with a pipette or separatory funnel. Freezing the solvent and filtering the ice slush that forms with a metal strainer is also an option. Finally, decant off any excess solid sodium carbonate/citrate. CaCl2 (sold as deicer, calcium hardener for pools and sometimes is the only ingredient in moisture absorbers tubs) can be used to ensure there is no water still left in the EA.<br /> <br /> == References ==<br /> &lt;references/&gt;</div>

Trip https://wiki.dmt-nexus.me/Category:Extraction_Tek 2023-10-06T04:02:04Z

<p>Trip: /* Dry tek */</p> <hr /> <div>An Extraction Tek is a manual to extract certain chemicals from a given source.<br /> <br /> To learn more about extractions in general and how they work, check the [http://wiki.dmt-nexus.me/FAQ#Where_to_start.3F FAQ], the [http://wiki.dmt-nexus.me/DMT_Extraction_Overview extraction overview], as well as read a few different teks, even if you don't plan on doing them, because many of them explain the processes and why each step is done.<br /> <br /> One does not need to be a chemist to perform an extraction. Don't worry about not understanding everything at first. Keep reading, inform yourself, take safety precautions, don't throw anything away before you're done with your extraction and don't consume anything you are not sure its clean.<br /> <br /> {{Main Page/Portal|[[Image:Information.png]]|'''[[:Category:Extraction_Tek|Extraction Teks]]'''|<br /> &lt;table&gt;<br /> &lt;tr&gt;<br /> &lt;td&gt;<br /> <br /> &lt;/td&gt;<br /> &lt;/tr&gt;<br /> &lt;/table&gt;<br /> }}<br /> <br /> ==DMT==<br /> ===A/B===<br /> <br /> * [[Lextek]]<br /> * [[Marsofold's tek]]<br /> * [[Shaggy's Jungle Tek]]<br /> * [[The DMT Handbook]]<br /> * [[Vovin's tek]]<br /> * [[ACRB Tek By Thick-Light]]<br /> * [https://www.dmt-nexus.me/forum/default.aspx?g=posts&amp;t=58064 ACRB TEK 100g &quot;PICS&quot; (Newbie Friendly)]<br /> * [[The Wanderer's Tek]]<br /> * [https://wiki.dmt-nexus.me/User_talk:Justamessenger SP's ACRB Extraction Tek]<br /> <br /> ===STB===<br /> <br /> * [[Jorkest's D-Limonene and Fumaric Acid Approach]]<br /> * [[Lazyman's tek]]<br /> * [[Noman's tek]]<br /> * [[STC - Dream Weaver's tek]]<br /> <br /> ===STB-A/B hybrid===<br /> <br /> * [[BLAB_-_The_Big_Leisurely_AB|BLAB]]<br /> * [[PanoraMIX European AB]]<br /> * [[Nontoxic_limonene_tek|SyZyGyPSy's Nontoxic Limomene Tek]]<br /> * [[Cyb's Hybrid ATB 'Salt' Tek]]<br /> * [https://www.dmt-nexus.me/forum/default.aspx?g=posts&amp;m=459391#post459391 Cyb's MAX ION Tek]<br /> <br /> ===Dry tek===<br /> <br /> * [[Amor fati's Nontoxic Approach to Spice Extraction]]<br /> * [[Q21Q21's Vinegar/Lime A/B Extraction Tek]]<br /> * [[HIELO]]<br /> <br /> ==MESCALINE==<br /> <br /> ===A/B===<br /> <br /> * [[Kash's A/B Mescaline Extraction]]<br /> <br /> ===STB===<br /> <br /> * [[LucidLemonade's sunflower oil mescaline extraction]]<br /> <br /> ===Crude extract===<br /> <br /> * [[House's cacti preparation tek]]<br /> <br /> ===Dry tek===<br /> <br /> * [[69ron's D-Limonene Mescaline Extraction]]<br /> * [[CIELO]]<br /> <br /> ==BUFOTENINE==<br /> <br /> ===Dry tek===<br /> <br /> * [[Jorkest's D-Limonene Bufotenine Extraction]]<br /> * [[http://www.dmt-nexus.me/forum/default.aspx?g=posts&amp;t=10071 No smell bufo extraction]]<br /> * [[BW's Bufotenine Dry Tek]]<br /> <br /> * [[https://wiki.dmt-nexus.me/Bufotenine_Benzoate Bufotenine Benzoate]]<br /> <br /> ===IPA extract===<br /> <br /> * [[Bufotenine IPA Extraction and Bufojam Changa Tek]]<br /> <br /> ==HARMALAS==<br /> <br /> ===A/B===<br /> <br /> * [[Harmalas Extraction and Separation Guide]]<br /> * [[EASY Harmaloid Freebase TEK]]<br /> * [[Easy Caapi Vine Alkaloid Extraction Guide]]<br /> * [[Enoons Cold Caapi Tek]]<br /> * [[The Tao of Rue Extraction]]<br /> <br /> ===Crude Manske (salt) Extract===<br /> <br /> * [[Harmine Crystals from Syrian Rue]]<br /> <br /> ===Dry Tek===<br /> * [[Ethyl Acetate Approach Harmala]]<br /> <br /> ==LSA==<br /> <br /> ===IPA extract===<br /> <br /> * [[PanoraMIX HBWR Extract]]<br /> <br /> ===Acetone extract===<br /> <br /> * [[Kash's Advanced LSA Extraction]]<br /> <br /> ==SALVIA==<br /> <br /> ===Acetone extract===<br /> <br /> * [[PanoraMIX salvia extact]]<br /> * [[Chilled Acetone with IPA and Naphtha re-X]]<br /> <br /> [[Category:Tek]]<br /> <br /> ==Conversion teks==<br /> <br /> [[DMT Fumarate to DMT Freebase]].<br /> <br /> [[THH_reduction]]</div>

Trip https://wiki.dmt-nexus.me/Bufotenine_Benzoate 2023-10-06T04:00:58Z

<p>Trip: /* Introduction= Bufotinine Benzoate (AKA 5-HO-DMT) */</p> <hr /> <div>==Introduction= Bufotinine Benzoate (AKA 5-HO-DMT)==<br /> '''THIS TEK LAB RESULTS STILL PENDING'''<br /> <br /> This Tek was written to be the quickest and easiest bufo extraction tek yet using cebil or yopo seeds. The final salt form is 5-HO-DMT benzoate which is smoother, easier to vape and appears more active per mg when compared to freebase 5-HO-DMT.<br /> <br /> Thanks to everyone who has contributed or helped experiment to aid in refining/ improving this process: Endlessness, Woolmer, Brennendes Wasser, _Trip_, and others.<br /> <br /> ==Safety==<br /> Review acetone safety information. Verify solvent MSDS, plastic compatibility, and clean evaporation.<br /> <br /> <br /> Following this advice does not guarantee safety. It is up to each adult individual to make their own personal decisions.<br /> <br /> ==Consumables==<br /> -100g of anadenanthera peregrina seeds or Anadenanthera colubrina seeds<br /> <br /> -25g Sodium Carbonate <br /> <br /> -150ml water <br /> <br /> -450ml Naphtha<br /> <br /> -100ml Xylene<br /> <br /> -450ml Acetone <br /> <br /> -5g-10g benzoic acid<br /> <br /> ==Equipment==<br /> Blender<br /> Frypan<br /> Spray bottle<br /> Jars<br /> Coffee or lab filters<br /> <br /> <br /> ==Detailed Process==<br /> Heat Seeds<br /> -Place seeds on minimal heat on fry pan, bring it up to heat until they start popping, lower the heat and turn it off once the seeds have stopped popping. (This step may be optional)<br /> <br /> ==Powder==<br /> -Get 100g seeds and 25g of sodium carbonate grind them with a glass blender into a powder. (Check weight on scales and take note).<br /> <br /> ==Add water==<br /> -Add 150ml of water by spraying the seeds/ sodium carbonate mix with a spray bottle. Do this until the paste becomes doughy. Mix well.<br /> <br /> ==Dry Paste==<br /> -Dry the paste with a fan and optionally low heat.<br /> <br /> ==Defatting==<br /> -When dry (check by comparing weight previously noted), defat with 3 x 150 ml boiling Naphtha, then decant.<br /> Repeat with 100ml of warm (not boiling) xylene (note: d-limo was originally used but xlyene should work better). Further defatting maybe required if solvent is not clean and is still pulling non polar material (fats).<br /> <br /> ==Pull==<br /> -Extract and pull with 3 x 150 ml DRY Acetone, filter store in jar. <br /> Add 5g-10g of Benzoic acid to acetone.<br /> <br /> ==Crystalisation==<br /> -5-HO-DMT will crystalise overtime this may take hours to a few days to happen be patient.<br /> <br /> [[File:Bufobenzoatefirstevermade.jpeg]]<br /> <br /> ==Decant &amp; Collect==<br /> -Decant and dry crystals for collection.<br /> <br /> [[File:1111112.jpg]]<br /> <br /> ==Lab results:==<br /> -Lab results to follow soon.</div>

Trip https://wiki.dmt-nexus.me/Bufotenine_Benzoate 2023-10-06T04:00:34Z

<p>Trip: /* Introduction= Bufotinine Benzoate (AKA 5-HO-DMT) */</p> <hr /> <div>==Introduction= Bufotinine Benzoate (AKA 5-HO-DMT)==<br /> '''THIS TEK LAB RESULTS STILL PENDING'''<br /> <br /> This Tek was written to be the quickest and easiest bufo extraction tek yet using cebil or yopo seeds. The final salt form is 5-HO-DMT benzoate which is smoother, easier to vape and appears more active per mg when compared to freebase 5-HO-DMT.<br /> <br /> Thanks to everyone who has contributed or helped experiment to aid in refining/ improving this process: Endlessness, Brennendes Wasser, _Trip_, and others.<br /> <br /> ==Safety==<br /> Review acetone safety information. Verify solvent MSDS, plastic compatibility, and clean evaporation.<br /> <br /> <br /> Following this advice does not guarantee safety. It is up to each adult individual to make their own personal decisions.<br /> <br /> ==Consumables==<br /> -100g of anadenanthera peregrina seeds or Anadenanthera colubrina seeds<br /> <br /> -25g Sodium Carbonate <br /> <br /> -150ml water <br /> <br /> -450ml Naphtha<br /> <br /> -100ml Xylene<br /> <br /> -450ml Acetone <br /> <br /> -5g-10g benzoic acid<br /> <br /> ==Equipment==<br /> Blender<br /> Frypan<br /> Spray bottle<br /> Jars<br /> Coffee or lab filters<br /> <br /> <br /> ==Detailed Process==<br /> Heat Seeds<br /> -Place seeds on minimal heat on fry pan, bring it up to heat until they start popping, lower the heat and turn it off once the seeds have stopped popping. (This step may be optional)<br /> <br /> ==Powder==<br /> -Get 100g seeds and 25g of sodium carbonate grind them with a glass blender into a powder. (Check weight on scales and take note).<br /> <br /> ==Add water==<br /> -Add 150ml of water by spraying the seeds/ sodium carbonate mix with a spray bottle. Do this until the paste becomes doughy. Mix well.<br /> <br /> ==Dry Paste==<br /> -Dry the paste with a fan and optionally low heat.<br /> <br /> ==Defatting==<br /> -When dry (check by comparing weight previously noted), defat with 3 x 150 ml boiling Naphtha, then decant.<br /> Repeat with 100ml of warm (not boiling) xylene (note: d-limo was originally used but xlyene should work better). Further defatting maybe required if solvent is not clean and is still pulling non polar material (fats).<br /> <br /> ==Pull==<br /> -Extract and pull with 3 x 150 ml DRY Acetone, filter store in jar. <br /> Add 5g-10g of Benzoic acid to acetone.<br /> <br /> ==Crystalisation==<br /> -5-HO-DMT will crystalise overtime this may take hours to a few days to happen be patient.<br /> <br /> [[File:Bufobenzoatefirstevermade.jpeg]]<br /> <br /> ==Decant &amp; Collect==<br /> -Decant and dry crystals for collection.<br /> <br /> [[File:1111112.jpg]]<br /> <br /> ==Lab results:==<br /> -Lab results to follow soon.</div>

Trip https://wiki.dmt-nexus.me/Category:Extraction_Tek 2023-10-06T04:00:13Z

<p>Trip: /* Dry tek */</p> <hr /> <div>An Extraction Tek is a manual to extract certain chemicals from a given source.<br /> <br /> To learn more about extractions in general and how they work, check the [http://wiki.dmt-nexus.me/FAQ#Where_to_start.3F FAQ], the [http://wiki.dmt-nexus.me/DMT_Extraction_Overview extraction overview], as well as read a few different teks, even if you don't plan on doing them, because many of them explain the processes and why each step is done.<br /> <br /> One does not need to be a chemist to perform an extraction. Don't worry about not understanding everything at first. Keep reading, inform yourself, take safety precautions, don't throw anything away before you're done with your extraction and don't consume anything you are not sure its clean.<br /> <br /> {{Main Page/Portal|[[Image:Information.png]]|'''[[:Category:Extraction_Tek|Extraction Teks]]'''|<br /> &lt;table&gt;<br /> &lt;tr&gt;<br /> &lt;td&gt;<br /> <br /> &lt;/td&gt;<br /> &lt;/tr&gt;<br /> &lt;/table&gt;<br /> }}<br /> <br /> ==DMT==<br /> ===A/B===<br /> <br /> * [[Lextek]]<br /> * [[Marsofold's tek]]<br /> * [[Shaggy's Jungle Tek]]<br /> * [[The DMT Handbook]]<br /> * [[Vovin's tek]]<br /> * [[ACRB Tek By Thick-Light]]<br /> * [https://www.dmt-nexus.me/forum/default.aspx?g=posts&amp;t=58064 ACRB TEK 100g &quot;PICS&quot; (Newbie Friendly)]<br /> * [[The Wanderer's Tek]]<br /> * [https://wiki.dmt-nexus.me/User_talk:Justamessenger SP's ACRB Extraction Tek]<br /> <br /> ===STB===<br /> <br /> * [[Jorkest's D-Limonene and Fumaric Acid Approach]]<br /> * [[Lazyman's tek]]<br /> * [[Noman's tek]]<br /> * [[STC - Dream Weaver's tek]]<br /> <br /> ===STB-A/B hybrid===<br /> <br /> * [[BLAB_-_The_Big_Leisurely_AB|BLAB]]<br /> * [[PanoraMIX European AB]]<br /> * [[Nontoxic_limonene_tek|SyZyGyPSy's Nontoxic Limomene Tek]]<br /> * [[Cyb's Hybrid ATB 'Salt' Tek]]<br /> * [https://www.dmt-nexus.me/forum/default.aspx?g=posts&amp;m=459391#post459391 Cyb's MAX ION Tek]<br /> <br /> ===Dry tek===<br /> <br /> * [[Amor fati's Nontoxic Approach to Spice Extraction]]<br /> * [[Q21Q21's Vinegar/Lime A/B Extraction Tek]]<br /> * [[HIELO]]<br /> <br /> ==MESCALINE==<br /> <br /> ===A/B===<br /> <br /> * [[Kash's A/B Mescaline Extraction]]<br /> <br /> ===STB===<br /> <br /> * [[LucidLemonade's sunflower oil mescaline extraction]]<br /> <br /> ===Crude extract===<br /> <br /> * [[House's cacti preparation tek]]<br /> <br /> ===Dry tek===<br /> <br /> * [[69ron's D-Limonene Mescaline Extraction]]<br /> * [[CIELO]]<br /> <br /> ==BUFOTENINE==<br /> <br /> ===Dry tek===<br /> <br /> * [[Jorkest's D-Limonene Bufotenine Extraction]]<br /> * [[http://www.dmt-nexus.me/forum/default.aspx?g=posts&amp;t=10071 No smell bufo extraction]]<br /> * [[BW's Bufotenine Dry Tek]]<br /> <br /> *[[https://wiki.dmt-nexus.me/Bufotenine_Benzoate Bufotenine Benzoate]]<br /> <br /> ===IPA extract===<br /> <br /> * [[Bufotenine IPA Extraction and Bufojam Changa Tek]]<br /> <br /> ==HARMALAS==<br /> <br /> ===A/B===<br /> <br /> * [[Harmalas Extraction and Separation Guide]]<br /> * [[EASY Harmaloid Freebase TEK]]<br /> * [[Easy Caapi Vine Alkaloid Extraction Guide]]<br /> * [[Enoons Cold Caapi Tek]]<br /> * [[The Tao of Rue Extraction]]<br /> <br /> ===Crude Manske (salt) Extract===<br /> <br /> * [[Harmine Crystals from Syrian Rue]]<br /> <br /> ===Dry Tek===<br /> * [[Ethyl Acetate Approach Harmala]]<br /> <br /> ==LSA==<br /> <br /> ===IPA extract===<br /> <br /> * [[PanoraMIX HBWR Extract]]<br /> <br /> ===Acetone extract===<br /> <br /> * [[Kash's Advanced LSA Extraction]]<br /> <br /> ==SALVIA==<br /> <br /> ===Acetone extract===<br /> <br /> * [[PanoraMIX salvia extact]]<br /> * [[Chilled Acetone with IPA and Naphtha re-X]]<br /> <br /> [[Category:Tek]]<br /> <br /> ==Conversion teks==<br /> <br /> [[DMT Fumarate to DMT Freebase]].<br /> <br /> [[THH_reduction]]</div>

Trip https://wiki.dmt-nexus.me/Category:Extraction_Tek 2023-10-06T03:59:43Z

<p>Trip: /* Dry tek */</p> <hr /> <div>An Extraction Tek is a manual to extract certain chemicals from a given source.<br /> <br /> To learn more about extractions in general and how they work, check the [http://wiki.dmt-nexus.me/FAQ#Where_to_start.3F FAQ], the [http://wiki.dmt-nexus.me/DMT_Extraction_Overview extraction overview], as well as read a few different teks, even if you don't plan on doing them, because many of them explain the processes and why each step is done.<br /> <br /> One does not need to be a chemist to perform an extraction. Don't worry about not understanding everything at first. Keep reading, inform yourself, take safety precautions, don't throw anything away before you're done with your extraction and don't consume anything you are not sure its clean.<br /> <br /> {{Main Page/Portal|[[Image:Information.png]]|'''[[:Category:Extraction_Tek|Extraction Teks]]'''|<br /> &lt;table&gt;<br /> &lt;tr&gt;<br /> &lt;td&gt;<br /> <br /> &lt;/td&gt;<br /> &lt;/tr&gt;<br /> &lt;/table&gt;<br /> }}<br /> <br /> ==DMT==<br /> ===A/B===<br /> <br /> * [[Lextek]]<br /> * [[Marsofold's tek]]<br /> * [[Shaggy's Jungle Tek]]<br /> * [[The DMT Handbook]]<br /> * [[Vovin's tek]]<br /> * [[ACRB Tek By Thick-Light]]<br /> * [https://www.dmt-nexus.me/forum/default.aspx?g=posts&amp;t=58064 ACRB TEK 100g &quot;PICS&quot; (Newbie Friendly)]<br /> * [[The Wanderer's Tek]]<br /> * [https://wiki.dmt-nexus.me/User_talk:Justamessenger SP's ACRB Extraction Tek]<br /> <br /> ===STB===<br /> <br /> * [[Jorkest's D-Limonene and Fumaric Acid Approach]]<br /> * [[Lazyman's tek]]<br /> * [[Noman's tek]]<br /> * [[STC - Dream Weaver's tek]]<br /> <br /> ===STB-A/B hybrid===<br /> <br /> * [[BLAB_-_The_Big_Leisurely_AB|BLAB]]<br /> * [[PanoraMIX European AB]]<br /> * [[Nontoxic_limonene_tek|SyZyGyPSy's Nontoxic Limomene Tek]]<br /> * [[Cyb's Hybrid ATB 'Salt' Tek]]<br /> * [https://www.dmt-nexus.me/forum/default.aspx?g=posts&amp;m=459391#post459391 Cyb's MAX ION Tek]<br /> <br /> ===Dry tek===<br /> <br /> * [[Amor fati's Nontoxic Approach to Spice Extraction]]<br /> * [[Q21Q21's Vinegar/Lime A/B Extraction Tek]]<br /> * [[HIELO]]<br /> <br /> ==MESCALINE==<br /> <br /> ===A/B===<br /> <br /> * [[Kash's A/B Mescaline Extraction]]<br /> <br /> ===STB===<br /> <br /> * [[LucidLemonade's sunflower oil mescaline extraction]]<br /> <br /> ===Crude extract===<br /> <br /> * [[House's cacti preparation tek]]<br /> <br /> ===Dry tek===<br /> <br /> * [[69ron's D-Limonene Mescaline Extraction]]<br /> * [[CIELO]]<br /> <br /> ==BUFOTENINE==<br /> <br /> ===Dry tek===<br /> <br /> * [[Jorkest's D-Limonene Bufotenine Extraction]]<br /> * [[http://www.dmt-nexus.me/forum/default.aspx?g=posts&amp;t=10071 No smell bufo extraction]]<br /> * [[BW's Bufotenine Dry Tek]]<br /> <br /> *[[https://wiki.dmt-nexus.me/Bufotenine_Benzoate]]<br /> <br /> ===IPA extract===<br /> <br /> * [[Bufotenine IPA Extraction and Bufojam Changa Tek]]<br /> <br /> ==HARMALAS==<br /> <br /> ===A/B===<br /> <br /> * [[Harmalas Extraction and Separation Guide]]<br /> * [[EASY Harmaloid Freebase TEK]]<br /> * [[Easy Caapi Vine Alkaloid Extraction Guide]]<br /> * [[Enoons Cold Caapi Tek]]<br /> * [[The Tao of Rue Extraction]]<br /> <br /> ===Crude Manske (salt) Extract===<br /> <br /> * [[Harmine Crystals from Syrian Rue]]<br /> <br /> ===Dry Tek===<br /> * [[Ethyl Acetate Approach Harmala]]<br /> <br /> ==LSA==<br /> <br /> ===IPA extract===<br /> <br /> * [[PanoraMIX HBWR Extract]]<br /> <br /> ===Acetone extract===<br /> <br /> * [[Kash's Advanced LSA Extraction]]<br /> <br /> ==SALVIA==<br /> <br /> ===Acetone extract===<br /> <br /> * [[PanoraMIX salvia extact]]<br /> * [[Chilled Acetone with IPA and Naphtha re-X]]<br /> <br /> [[Category:Tek]]<br /> <br /> ==Conversion teks==<br /> <br /> [[DMT Fumarate to DMT Freebase]].<br /> <br /> [[THH_reduction]]</div>

Trip https://wiki.dmt-nexus.me/Category:Extraction_Tek 2023-09-16T04:53:53Z

<p>Trip: </p> <hr /> <div>An Extraction Tek is a manual to extract certain chemicals from a given source.<br /> <br /> To learn more about extractions in general and how they work, check the [http://wiki.dmt-nexus.me/FAQ#Where_to_start.3F FAQ], the [http://wiki.dmt-nexus.me/DMT_Extraction_Overview extraction overview], as well as read a few different teks, even if you don't plan on doing them, because many of them explain the processes and why each step is done.<br /> <br /> One does not need to be a chemist to perform an extraction. Don't worry about not understanding everything at first. Keep reading, inform yourself, take safety precautions, don't throw anything away before you're done with your extraction and don't consume anything you are not sure its clean.<br /> <br /> {{Main Page/Portal|[[Image:Information.png]]|'''[[:Category:Extraction_Tek|Extraction Teks]]'''|<br /> &lt;table&gt;<br /> &lt;tr&gt;<br /> &lt;td&gt;<br /> <br /> &lt;/td&gt;<br /> &lt;/tr&gt;<br /> &lt;/table&gt;<br /> }}<br /> <br /> ==DMT==<br /> ===A/B===<br /> <br /> * [[Lextek]]<br /> * [[Marsofold's tek]]<br /> * [[Shaggy's Jungle Tek]]<br /> * [[The DMT Handbook]]<br /> * [[Vovin's tek]]<br /> * [[ACRB Tek By Thick-Light]]<br /> * [https://www.dmt-nexus.me/forum/default.aspx?g=posts&amp;t=58064 ACRB TEK 100g &quot;PICS&quot; (Newbie Friendly)]<br /> * [[The Wanderer's Tek]]<br /> * [https://wiki.dmt-nexus.me/User_talk:Justamessenger SP's ACRB Extraction Tek]<br /> <br /> ===STB===<br /> <br /> * [[Jorkest's D-Limonene and Fumaric Acid Approach]]<br /> * [[Lazyman's tek]]<br /> * [[Noman's tek]]<br /> * [[STC - Dream Weaver's tek]]<br /> <br /> ===STB-A/B hybrid===<br /> <br /> * [[BLAB_-_The_Big_Leisurely_AB|BLAB]]<br /> * [[PanoraMIX European AB]]<br /> * [[Nontoxic_limonene_tek|SyZyGyPSy's Nontoxic Limomene Tek]]<br /> * [[Cyb's Hybrid ATB 'Salt' Tek]]<br /> * [https://www.dmt-nexus.me/forum/default.aspx?g=posts&amp;m=459391#post459391 Cyb's MAX ION Tek]<br /> <br /> ===Dry tek===<br /> <br /> * [[Amor fati's Nontoxic Approach to Spice Extraction]]<br /> * [[Q21Q21's Vinegar/Lime A/B Extraction Tek]]<br /> * [[HIELO]]<br /> <br /> ==MESCALINE==<br /> <br /> ===A/B===<br /> <br /> * [[Kash's A/B Mescaline Extraction]]<br /> <br /> ===STB===<br /> <br /> * [[LucidLemonade's sunflower oil mescaline extraction]]<br /> <br /> ===Crude extract===<br /> <br /> * [[House's cacti preparation tek]]<br /> <br /> ===Dry tek===<br /> <br /> * [[69ron's D-Limonene Mescaline Extraction]]<br /> * [[CIELO]]<br /> <br /> ==BUFOTENINE==<br /> <br /> ===Dry tek===<br /> <br /> * [[Jorkest's D-Limonene Bufotenine Extraction]]<br /> * [[http://www.dmt-nexus.me/forum/default.aspx?g=posts&amp;t=10071 No smell bufo extraction]]<br /> * [[BW's Bufotenine Dry Tek]]<br /> <br /> <br /> ===IPA extract===<br /> <br /> * [[Bufotenine IPA Extraction and Bufojam Changa Tek]]<br /> <br /> ==HARMALAS==<br /> <br /> ===A/B===<br /> <br /> * [[Harmalas Extraction and Separation Guide]]<br /> * [[EASY Harmaloid Freebase TEK]]<br /> * [[Easy Caapi Vine Alkaloid Extraction Guide]]<br /> * [[Enoons Cold Caapi Tek]]<br /> * [[The Tao of Rue Extraction]]<br /> <br /> ===Crude Manske (salt) Extract===<br /> <br /> * [[Harmine Crystals from Syrian Rue]]<br /> <br /> ===Dry Tek===<br /> * [[Ethyl Acetate Approach Harmala]]<br /> <br /> ==LSA==<br /> <br /> ===IPA extract===<br /> <br /> * [[PanoraMIX HBWR Extract]]<br /> <br /> ===Acetone extract===<br /> <br /> * [[Kash's Advanced LSA Extraction]]<br /> <br /> ==SALVIA==<br /> <br /> ===Acetone extract===<br /> <br /> * [[PanoraMIX salvia extact]]<br /> * [[Chilled Acetone with IPA and Naphtha re-X]]<br /> <br /> [[Category:Tek]]<br /> <br /> ==Conversion teks==<br /> <br /> [[DMT Fumarate to DMT Freebase]].<br /> <br /> [[THH_reduction]]</div>

Trip https://wiki.dmt-nexus.me/Bufotenine_Benzoate 2023-07-08T15:24:02Z

<p>Trip: /* Introduction= Bufotinine Benzoate (AKA 5-HO-DMT) */</p> <hr /> <div>==Introduction= Bufotinine Benzoate (AKA 5-HO-DMT)==<br /> '''PLEASE DO NOT USE THIS TEK LAB RESULTS STILL PENDING'''<br /> <br /> This Tek was written to be the quickest and easiest bufo extraction tek yet using cebil or yopo seeds. The final salt form is 5-HO-DMT benzoate which is smoother, easier to vape and appears more active per mg when compared to freebase 5-HO-DMT.<br /> <br /> Thanks to everyone who has contributed or helped experiment to aid in refining/ improving this process: Endlessness, Brennendes Wasser, _Trip_, and others.<br /> <br /> ==Safety==<br /> Review acetone safety information. Verify solvent MSDS, plastic compatibility, and clean evaporation.<br /> <br /> <br /> Following this advice does not guarantee safety. It is up to each adult individual to make their own personal decisions.<br /> <br /> ==Consumables==<br /> -100g of anadenanthera peregrina seeds or Anadenanthera colubrina seeds<br /> <br /> -25g Sodium Carbonate <br /> <br /> -150ml water <br /> <br /> -450ml Naphtha<br /> <br /> -100ml Xylene<br /> <br /> -450ml Acetone <br /> <br /> -5g-10g benzoic acid<br /> <br /> ==Equipment==<br /> Blender<br /> Frypan<br /> Spray bottle<br /> Jars<br /> Coffee or lab filters<br /> <br /> <br /> ==Detailed Process==<br /> Heat Seeds<br /> -Place seeds on minimal heat on fry pan, bring it up to heat until they start popping, lower the heat and turn it off once the seeds have stopped popping. (This step may be optional)<br /> <br /> ==Powder==<br /> -Get 100g seeds and 25g of sodium carbonate grind them with a glass blender into a powder. (Check weight on scales and take note).<br /> <br /> ==Add water==<br /> -Add 150ml of water by spraying the seeds/ sodium carbonate mix with a spray bottle. Do this until the paste becomes doughy. Mix well.<br /> <br /> ==Dry Paste==<br /> -Dry the paste with a fan and optionally low heat.<br /> <br /> ==Defatting==<br /> -When dry (check by comparing weight previously noted), defat with 3 x 150 ml boiling Naphtha, then decant.<br /> Repeat with 100ml of warm (not boiling) xylene (note: d-limo was originally used but xlyene should work better). Further defatting maybe required if solvent is not clean and is still pulling non polar material (fats).<br /> <br /> ==Pull==<br /> -Extract and pull with 3 x 150 ml DRY Acetone, filter store in jar. <br /> Add 5g-10g of Benzoic acid to acetone.<br /> <br /> ==Crystalisation==<br /> -5-HO-DMT will crystalise overtime this may take hours to a few days to happen be patient.<br /> <br /> [[File:Bufobenzoatefirstevermade.jpeg]]<br /> <br /> ==Decant &amp; Collect==<br /> -Decant and dry crystals for collection.<br /> <br /> [[File:1111112.jpg]]<br /> <br /> ==Lab results:==<br /> -Lab results to follow soon.</div>

Trip https://wiki.dmt-nexus.me/Bufotenine_Benzoate 2023-06-02T06:00:46Z

<p>Trip: /* Consumables */</p> <hr /> <div>==Introduction= Bufotinine Benzoate (AKA 5-HO-DMT)==<br /> This Tek was written to be the quickest and easiest bufo extraction tek yet using cebil or yopo seeds. The final salt form is 5-HO-DMT benzoate which is smoother, easier to vape and appears more active per mg when compared to freebase 5-HO-DMT.<br /> <br /> Thanks to everyone who has contributed or helped experiment to aid in refining/ improving this process: Endlessness, Brennendes Wasser, _Trip_, and others.<br /> <br /> ==Safety==<br /> Review acetone safety information. Verify solvent MSDS, plastic compatibility, and clean evaporation.<br /> <br /> <br /> Following this advice does not guarantee safety. It is up to each adult individual to make their own personal decisions.<br /> <br /> ==Consumables==<br /> -100g of anadenanthera peregrina seeds or Anadenanthera colubrina seeds<br /> <br /> -25g Sodium Carboante<br /> <br /> -150ml water <br /> <br /> -450ml Naphtha<br /> <br /> -100ml Xylene<br /> <br /> -450ml Acetone <br /> <br /> -5g-10g benzoic acid<br /> <br /> ==Equipment==<br /> Blender<br /> Frypan<br /> Spray bottle<br /> Jars<br /> Coffee or lab filters<br /> <br /> <br /> ==Detailed Process==<br /> Heat Seeds<br /> -Place seeds on minimal heat on fry pan, bring it up to heat until they start popping, lower the heat and turn it off once the seeds have stopped popping. (This step may be optional)<br /> <br /> ==Powder==<br /> -Get 100g seeds and 25g of sodium carbonate grind them with a glass blender into a powder. (Check weight on scales and take note).<br /> <br /> ==Add water==<br /> -Add 150ml of water by spraying the seeds/ sodium carbonate mix with a spray bottle. Do this until the paste becomes doughy. Mix well.<br /> <br /> ==Dry Paste==<br /> -Dry the paste with a fan and optionally low heat.<br /> <br /> ==Defatting==<br /> -When dry (check by comparing weight previously noted), defat with 3 x 150 ml boiling Naphtha, then decant.<br /> Repeat with 100ml of warm (not boiling) xylene (note: d-limo was originally used but xlyene should work better). Further defatting maybe required if solvent is not clean and is still pulling non polar material (fats).<br /> <br /> ==Pull==<br /> -Extract and pull with 3 x 450 ml DRY Acetone, filter store in jar. <br /> Add 5g-10g of Benzoic acid to acetone.<br /> <br /> ==Crystalisation==<br /> -5-HO-DMT will crystalise overtime this may take hours to a few days to happen be patient.<br /> <br /> [[File:Bufobenzoatefirstevermade.jpeg]]<br /> <br /> ==Decant &amp; Collect==<br /> -Decant and dry crystals for collection.<br /> <br /> [[File:1111112.jpg]]<br /> <br /> ==Lab results:==<br /> -Lab results to follow soon.</div>

Trip https://wiki.dmt-nexus.me/Bufotenine_Benzoate 2023-06-02T06:00:06Z

<p>Trip: /* Consumables */</p> <hr /> <div>==Introduction= Bufotinine Benzoate (AKA 5-HO-DMT)==<br /> This Tek was written to be the quickest and easiest bufo extraction tek yet using cebil or yopo seeds. The final salt form is 5-HO-DMT benzoate which is smoother, easier to vape and appears more active per mg when compared to freebase 5-HO-DMT.<br /> <br /> Thanks to everyone who has contributed or helped experiment to aid in refining/ improving this process: Endlessness, Brennendes Wasser, _Trip_, and others.<br /> <br /> ==Safety==<br /> Review acetone safety information. Verify solvent MSDS, plastic compatibility, and clean evaporation.<br /> <br /> <br /> Following this advice does not guarantee safety. It is up to each adult individual to make their own personal decisions.<br /> <br /> ==Consumables==<br /> -100g of anadenanthera peregrina seeds or ---Anadenanthera colubrina<br /> -25g Sodium Carboante<br /> -150ml water <br /> -450ml Naphtha<br /> -100ml Xylene<br /> -450ml Acetone <br /> -5g-10g benzoic acid<br /> <br /> ==Equipment==<br /> Blender<br /> Frypan<br /> Spray bottle<br /> Jars<br /> Coffee or lab filters<br /> <br /> <br /> ==Detailed Process==<br /> Heat Seeds<br /> -Place seeds on minimal heat on fry pan, bring it up to heat until they start popping, lower the heat and turn it off once the seeds have stopped popping. (This step may be optional)<br /> <br /> ==Powder==<br /> -Get 100g seeds and 25g of sodium carbonate grind them with a glass blender into a powder. (Check weight on scales and take note).<br /> <br /> ==Add water==<br /> -Add 150ml of water by spraying the seeds/ sodium carbonate mix with a spray bottle. Do this until the paste becomes doughy. Mix well.<br /> <br /> ==Dry Paste==<br /> -Dry the paste with a fan and optionally low heat.<br /> <br /> ==Defatting==<br /> -When dry (check by comparing weight previously noted), defat with 3 x 150 ml boiling Naphtha, then decant.<br /> Repeat with 100ml of warm (not boiling) xylene (note: d-limo was originally used but xlyene should work better). Further defatting maybe required if solvent is not clean and is still pulling non polar material (fats).<br /> <br /> ==Pull==<br /> -Extract and pull with 3 x 450 ml DRY Acetone, filter store in jar. <br /> Add 5g-10g of Benzoic acid to acetone.<br /> <br /> ==Crystalisation==<br /> -5-HO-DMT will crystalise overtime this may take hours to a few days to happen be patient.<br /> <br /> [[File:Bufobenzoatefirstevermade.jpeg]]<br /> <br /> ==Decant &amp; Collect==<br /> -Decant and dry crystals for collection.<br /> <br /> [[File:1111112.jpg]]<br /> <br /> ==Lab results:==<br /> -Lab results to follow soon.</div>

Trip https://wiki.dmt-nexus.me/Bufotenine_Benzoate 2023-06-02T05:59:05Z

<p>Trip: /* Safety */</p> <hr /> <div>==Introduction= Bufotinine Benzoate (AKA 5-HO-DMT)==<br /> This Tek was written to be the quickest and easiest bufo extraction tek yet using cebil or yopo seeds. The final salt form is 5-HO-DMT benzoate which is smoother, easier to vape and appears more active per mg when compared to freebase 5-HO-DMT.<br /> <br /> Thanks to everyone who has contributed or helped experiment to aid in refining/ improving this process: Endlessness, Brennendes Wasser, _Trip_, and others.<br /> <br /> ==Safety==<br /> Review acetone safety information. Verify solvent MSDS, plastic compatibility, and clean evaporation.<br /> <br /> <br /> Following this advice does not guarantee safety. It is up to each adult individual to make their own personal decisions.<br /> <br /> ==Consumables==<br /> 100g of anadenanthera peregrina seeds or Anadenanthera colubrina<br /> 25g Sodium Carboante<br /> 150ml water <br /> 450ml Naphtha<br /> 100ml Xylene<br /> 450ml Acetone <br /> 5g-10g benzoic acid<br /> <br /> ==Equipment==<br /> Blender<br /> Frypan<br /> Spray bottle<br /> Jars<br /> Coffee or lab filters<br /> <br /> <br /> ==Detailed Process==<br /> Heat Seeds<br /> -Place seeds on minimal heat on fry pan, bring it up to heat until they start popping, lower the heat and turn it off once the seeds have stopped popping. (This step may be optional)<br /> <br /> ==Powder==<br /> -Get 100g seeds and 25g of sodium carbonate grind them with a glass blender into a powder. (Check weight on scales and take note).<br /> <br /> ==Add water==<br /> -Add 150ml of water by spraying the seeds/ sodium carbonate mix with a spray bottle. Do this until the paste becomes doughy. Mix well.<br /> <br /> ==Dry Paste==<br /> -Dry the paste with a fan and optionally low heat.<br /> <br /> ==Defatting==<br /> -When dry (check by comparing weight previously noted), defat with 3 x 150 ml boiling Naphtha, then decant.<br /> Repeat with 100ml of warm (not boiling) xylene (note: d-limo was originally used but xlyene should work better). Further defatting maybe required if solvent is not clean and is still pulling non polar material (fats).<br /> <br /> ==Pull==<br /> -Extract and pull with 3 x 450 ml DRY Acetone, filter store in jar. <br /> Add 5g-10g of Benzoic acid to acetone.<br /> <br /> ==Crystalisation==<br /> -5-HO-DMT will crystalise overtime this may take hours to a few days to happen be patient.<br /> <br /> [[File:Bufobenzoatefirstevermade.jpeg]]<br /> <br /> ==Decant &amp; Collect==<br /> -Decant and dry crystals for collection.<br /> <br /> [[File:1111112.jpg]]<br /> <br /> ==Lab results:==<br /> -Lab results to follow soon.</div>

Trip https://wiki.dmt-nexus.me/Bufotenine_Benzoate 2023-05-31T12:16:25Z

<p>Trip: /* Decant &amp; Collect */</p> <hr /> <div>==Introduction= Bufotinine Benzoate (AKA 5-HO-DMT)==<br /> This Tek was written to be the quickest and easiest bufo extraction tek yet using cebil or yopo seeds. The final salt form is 5-HO-DMT benzoate which is smoother, easier to vape and appears more active per mg when compared to freebase 5-HO-DMT.<br /> <br /> Thanks to everyone who has contributed or helped experiment to aid in refining/ improving this process: Endlessness, Brennendes Wasser, _Trip_, and others.<br /> <br /> ==Safety==<br /> Review ethyl acetate safety information. Verify solvent MSDS, plastic compatibility, and clean evaporation.<br /> <br /> <br /> Following this advice does not guarantee safety. It is up to each adult individual to make their own personal decisions.<br /> <br /> <br /> ==Consumables==<br /> 100g of anadenanthera peregrina seeds or Anadenanthera colubrina<br /> 25g Sodium Carboante<br /> 150ml water <br /> 450ml Naphtha<br /> 100ml Xylene<br /> 450ml Acetone <br /> 5g-10g benzoic acid<br /> <br /> ==Equipment==<br /> Blender<br /> Frypan<br /> Spray bottle<br /> Jars<br /> Coffee or lab filters<br /> <br /> <br /> ==Detailed Process==<br /> Heat Seeds<br /> -Place seeds on minimal heat on fry pan, bring it up to heat until they start popping, lower the heat and turn it off once the seeds have stopped popping. (This step may be optional)<br /> <br /> ==Powder==<br /> -Get 100g seeds and 25g of sodium carbonate grind them with a glass blender into a powder. (Check weight on scales and take note).<br /> <br /> ==Add water==<br /> -Add 150ml of water by spraying the seeds/ sodium carbonate mix with a spray bottle. Do this until the paste becomes doughy. Mix well.<br /> <br /> ==Dry Paste==<br /> -Dry the paste with a fan and optionally low heat.<br /> <br /> ==Defatting==<br /> -When dry (check by comparing weight previously noted), defat with 3 x 150 ml boiling Naphtha, then decant.<br /> Repeat with 100ml of warm (not boiling) xylene (note: d-limo was originally used but xlyene should work better). Further defatting maybe required if solvent is not clean and is still pulling non polar material (fats).<br /> <br /> ==Pull==<br /> -Extract and pull with 3 x 450 ml DRY Acetone, filter store in jar. <br /> Add 5g-10g of Benzoic acid to acetone.<br /> <br /> ==Crystalisation==<br /> -5-HO-DMT will crystalise overtime this may take hours to a few days to happen be patient.<br /> <br /> [[File:Bufobenzoatefirstevermade.jpeg]]<br /> <br /> ==Decant &amp; Collect==<br /> -Decant and dry crystals for collection.<br /> <br /> [[File:1111112.jpg]]<br /> <br /> ==Lab results:==<br /> -Lab results to follow soon.</div>

Trip https://wiki.dmt-nexus.me/Bufotenine_Benzoate 2023-05-31T12:16:14Z

<p>Trip: /* Decant &amp; Collect */</p> <hr /> <div>==Introduction= Bufotinine Benzoate (AKA 5-HO-DMT)==<br /> This Tek was written to be the quickest and easiest bufo extraction tek yet using cebil or yopo seeds. The final salt form is 5-HO-DMT benzoate which is smoother, easier to vape and appears more active per mg when compared to freebase 5-HO-DMT.<br /> <br /> Thanks to everyone who has contributed or helped experiment to aid in refining/ improving this process: Endlessness, Brennendes Wasser, _Trip_, and others.<br /> <br /> ==Safety==<br /> Review ethyl acetate safety information. Verify solvent MSDS, plastic compatibility, and clean evaporation.<br /> <br /> <br /> Following this advice does not guarantee safety. It is up to each adult individual to make their own personal decisions.<br /> <br /> <br /> ==Consumables==<br /> 100g of anadenanthera peregrina seeds or Anadenanthera colubrina<br /> 25g Sodium Carboante<br /> 150ml water <br /> 450ml Naphtha<br /> 100ml Xylene<br /> 450ml Acetone <br /> 5g-10g benzoic acid<br /> <br /> ==Equipment==<br /> Blender<br /> Frypan<br /> Spray bottle<br /> Jars<br /> Coffee or lab filters<br /> <br /> <br /> ==Detailed Process==<br /> Heat Seeds<br /> -Place seeds on minimal heat on fry pan, bring it up to heat until they start popping, lower the heat and turn it off once the seeds have stopped popping. (This step may be optional)<br /> <br /> ==Powder==<br /> -Get 100g seeds and 25g of sodium carbonate grind them with a glass blender into a powder. (Check weight on scales and take note).<br /> <br /> ==Add water==<br /> -Add 150ml of water by spraying the seeds/ sodium carbonate mix with a spray bottle. Do this until the paste becomes doughy. Mix well.<br /> <br /> ==Dry Paste==<br /> -Dry the paste with a fan and optionally low heat.<br /> <br /> ==Defatting==<br /> -When dry (check by comparing weight previously noted), defat with 3 x 150 ml boiling Naphtha, then decant.<br /> Repeat with 100ml of warm (not boiling) xylene (note: d-limo was originally used but xlyene should work better). Further defatting maybe required if solvent is not clean and is still pulling non polar material (fats).<br /> <br /> ==Pull==<br /> -Extract and pull with 3 x 450 ml DRY Acetone, filter store in jar. <br /> Add 5g-10g of Benzoic acid to acetone.<br /> <br /> ==Crystalisation==<br /> -5-HO-DMT will crystalise overtime this may take hours to a few days to happen be patient.<br /> <br /> [[File:Bufobenzoatefirstevermade.jpeg]]<br /> <br /> ==Decant &amp; Collect==<br /> -Decant and dry crystals for collection.<br /> <br /> [[File:File:1111112.jpg]]<br /> <br /> ==Lab results:==<br /> -Lab results to follow soon.</div>

Trip https://wiki.dmt-nexus.me/File:1111112.jpg 2023-05-31T12:15:53Z

<p>Trip: </p> <hr /> <div></div>

Trip https://wiki.dmt-nexus.me/Bufotenine_Benzoate 2023-05-31T12:12:33Z

<p>Trip: /* Crystalisation */</p> <hr /> <div>==Introduction= Bufotinine Benzoate (AKA 5-HO-DMT)==<br /> This Tek was written to be the quickest and easiest bufo extraction tek yet using cebil or yopo seeds. The final salt form is 5-HO-DMT benzoate which is smoother, easier to vape and appears more active per mg when compared to freebase 5-HO-DMT.<br /> <br /> Thanks to everyone who has contributed or helped experiment to aid in refining/ improving this process: Endlessness, Brennendes Wasser, _Trip_, and others.<br /> <br /> ==Safety==<br /> Review ethyl acetate safety information. Verify solvent MSDS, plastic compatibility, and clean evaporation.<br /> <br /> <br /> Following this advice does not guarantee safety. It is up to each adult individual to make their own personal decisions.<br /> <br /> <br /> ==Consumables==<br /> 100g of anadenanthera peregrina seeds or Anadenanthera colubrina<br /> 25g Sodium Carboante<br /> 150ml water <br /> 450ml Naphtha<br /> 100ml Xylene<br /> 450ml Acetone <br /> 5g-10g benzoic acid<br /> <br /> ==Equipment==<br /> Blender<br /> Frypan<br /> Spray bottle<br /> Jars<br /> Coffee or lab filters<br /> <br /> <br /> ==Detailed Process==<br /> Heat Seeds<br /> -Place seeds on minimal heat on fry pan, bring it up to heat until they start popping, lower the heat and turn it off once the seeds have stopped popping. (This step may be optional)<br /> <br /> ==Powder==<br /> -Get 100g seeds and 25g of sodium carbonate grind them with a glass blender into a powder. (Check weight on scales and take note).<br /> <br /> ==Add water==<br /> -Add 150ml of water by spraying the seeds/ sodium carbonate mix with a spray bottle. Do this until the paste becomes doughy. Mix well.<br /> <br /> ==Dry Paste==<br /> -Dry the paste with a fan and optionally low heat.<br /> <br /> ==Defatting==<br /> -When dry (check by comparing weight previously noted), defat with 3 x 150 ml boiling Naphtha, then decant.<br /> Repeat with 100ml of warm (not boiling) xylene (note: d-limo was originally used but xlyene should work better). Further defatting maybe required if solvent is not clean and is still pulling non polar material (fats).<br /> <br /> ==Pull==<br /> -Extract and pull with 3 x 450 ml DRY Acetone, filter store in jar. <br /> Add 5g-10g of Benzoic acid to acetone.<br /> <br /> ==Crystalisation==<br /> -5-HO-DMT will crystalise overtime this may take hours to a few days to happen be patient.<br /> <br /> [[File:Bufobenzoatefirstevermade.jpeg]]<br /> <br /> ==Decant &amp; Collect==<br /> -Decant and dry crystals for collection.<br /> <br /> ==Lab results:==<br /> -Lab results to follow soon.</div>

Trip https://wiki.dmt-nexus.me/Bufotenine_Benzoate 2023-05-31T12:12:13Z

<p>Trip: /* Crystalisation */</p> <hr /> <div>==Introduction= Bufotinine Benzoate (AKA 5-HO-DMT)==<br /> This Tek was written to be the quickest and easiest bufo extraction tek yet using cebil or yopo seeds. The final salt form is 5-HO-DMT benzoate which is smoother, easier to vape and appears more active per mg when compared to freebase 5-HO-DMT.<br /> <br /> Thanks to everyone who has contributed or helped experiment to aid in refining/ improving this process: Endlessness, Brennendes Wasser, _Trip_, and others.<br /> <br /> ==Safety==<br /> Review ethyl acetate safety information. Verify solvent MSDS, plastic compatibility, and clean evaporation.<br /> <br /> <br /> Following this advice does not guarantee safety. It is up to each adult individual to make their own personal decisions.<br /> <br /> <br /> ==Consumables==<br /> 100g of anadenanthera peregrina seeds or Anadenanthera colubrina<br /> 25g Sodium Carboante<br /> 150ml water <br /> 450ml Naphtha<br /> 100ml Xylene<br /> 450ml Acetone <br /> 5g-10g benzoic acid<br /> <br /> ==Equipment==<br /> Blender<br /> Frypan<br /> Spray bottle<br /> Jars<br /> Coffee or lab filters<br /> <br /> <br /> ==Detailed Process==<br /> Heat Seeds<br /> -Place seeds on minimal heat on fry pan, bring it up to heat until they start popping, lower the heat and turn it off once the seeds have stopped popping. (This step may be optional)<br /> <br /> ==Powder==<br /> -Get 100g seeds and 25g of sodium carbonate grind them with a glass blender into a powder. (Check weight on scales and take note).<br /> <br /> ==Add water==<br /> -Add 150ml of water by spraying the seeds/ sodium carbonate mix with a spray bottle. Do this until the paste becomes doughy. Mix well.<br /> <br /> ==Dry Paste==<br /> -Dry the paste with a fan and optionally low heat.<br /> <br /> ==Defatting==<br /> -When dry (check by comparing weight previously noted), defat with 3 x 150 ml boiling Naphtha, then decant.<br /> Repeat with 100ml of warm (not boiling) xylene (note: d-limo was originally used but xlyene should work better). Further defatting maybe required if solvent is not clean and is still pulling non polar material (fats).<br /> <br /> ==Pull==<br /> -Extract and pull with 3 x 450 ml DRY Acetone, filter store in jar. <br /> Add 5g-10g of Benzoic acid to acetone.<br /> <br /> ==Crystalisation==<br /> -5-HO-DMT will crystalise overtime this may take hours to a few days to happen be patient.<br /> <br /> <br /> [IMG]File:Bufobenzoatefirstevermade.jpeg[/IMG]<br /> <br /> ==Decant &amp; Collect==<br /> -Decant and dry crystals for collection.<br /> <br /> ==Lab results:==<br /> -Lab results to follow soon.</div>

Trip https://wiki.dmt-nexus.me/File:Bufobenzoatefirstevermade.jpeg 2023-05-31T12:11:59Z

<p>Trip: </p> <hr /> <div></div>

Trip https://wiki.dmt-nexus.me/Bufotenine_Benzoate 2023-05-31T12:10:20Z

<p>Trip: /* Defatting */</p> <hr /> <div>==Introduction= Bufotinine Benzoate (AKA 5-HO-DMT)==<br /> This Tek was written to be the quickest and easiest bufo extraction tek yet using cebil or yopo seeds. The final salt form is 5-HO-DMT benzoate which is smoother, easier to vape and appears more active per mg when compared to freebase 5-HO-DMT.<br /> <br /> Thanks to everyone who has contributed or helped experiment to aid in refining/ improving this process: Endlessness, Brennendes Wasser, _Trip_, and others.<br /> <br /> ==Safety==<br /> Review ethyl acetate safety information. Verify solvent MSDS, plastic compatibility, and clean evaporation.<br /> <br /> <br /> Following this advice does not guarantee safety. It is up to each adult individual to make their own personal decisions.<br /> <br /> <br /> ==Consumables==<br /> 100g of anadenanthera peregrina seeds or Anadenanthera colubrina<br /> 25g Sodium Carboante<br /> 150ml water <br /> 450ml Naphtha<br /> 100ml Xylene<br /> 450ml Acetone <br /> 5g-10g benzoic acid<br /> <br /> ==Equipment==<br /> Blender<br /> Frypan<br /> Spray bottle<br /> Jars<br /> Coffee or lab filters<br /> <br /> <br /> ==Detailed Process==<br /> Heat Seeds<br /> -Place seeds on minimal heat on fry pan, bring it up to heat until they start popping, lower the heat and turn it off once the seeds have stopped popping. (This step may be optional)<br /> <br /> ==Powder==<br /> -Get 100g seeds and 25g of sodium carbonate grind them with a glass blender into a powder. (Check weight on scales and take note).<br /> <br /> ==Add water==<br /> -Add 150ml of water by spraying the seeds/ sodium carbonate mix with a spray bottle. Do this until the paste becomes doughy. Mix well.<br /> <br /> ==Dry Paste==<br /> -Dry the paste with a fan and optionally low heat.<br /> <br /> ==Defatting==<br /> -When dry (check by comparing weight previously noted), defat with 3 x 150 ml boiling Naphtha, then decant.<br /> Repeat with 100ml of warm (not boiling) xylene (note: d-limo was originally used but xlyene should work better). Further defatting maybe required if solvent is not clean and is still pulling non polar material (fats).<br /> <br /> ==Pull==<br /> -Extract and pull with 3 x 450 ml DRY Acetone, filter store in jar. <br /> Add 5g-10g of Benzoic acid to acetone.<br /> <br /> ==Crystalisation==<br /> -5-HO-DMT will crystalise overtime this may take hours to a few days to happen be patient.<br /> <br /> <br /> [IMG]https://www.dmt-nexus.me/forum/resource.ashx?a=58372&amp;nc=1[/IMG]<br /> <br /> ==Decant &amp; Collect==<br /> -Decant and dry crystals for collection.<br /> <br /> ==Lab results:==<br /> -Lab results to follow soon.</div>

Trip https://wiki.dmt-nexus.me/Bufotenine_Benzoate 2023-05-31T12:08:14Z

<p>Trip: /* Crystalisation */</p> <hr /> <div>==Introduction= Bufotinine Benzoate (AKA 5-HO-DMT)==<br /> This Tek was written to be the quickest and easiest bufo extraction tek yet using cebil or yopo seeds. The final salt form is 5-HO-DMT benzoate which is smoother, easier to vape and appears more active per mg when compared to freebase 5-HO-DMT.<br /> <br /> Thanks to everyone who has contributed or helped experiment to aid in refining/ improving this process: Endlessness, Brennendes Wasser, _Trip_, and others.<br /> <br /> ==Safety==<br /> Review ethyl acetate safety information. Verify solvent MSDS, plastic compatibility, and clean evaporation.<br /> <br /> <br /> Following this advice does not guarantee safety. It is up to each adult individual to make their own personal decisions.<br /> <br /> <br /> ==Consumables==<br /> 100g of anadenanthera peregrina seeds or Anadenanthera colubrina<br /> 25g Sodium Carboante<br /> 150ml water <br /> 450ml Naphtha<br /> 100ml Xylene<br /> 450ml Acetone <br /> 5g-10g benzoic acid<br /> <br /> ==Equipment==<br /> Blender<br /> Frypan<br /> Spray bottle<br /> Jars<br /> Coffee or lab filters<br /> <br /> <br /> ==Detailed Process==<br /> Heat Seeds<br /> -Place seeds on minimal heat on fry pan, bring it up to heat until they start popping, lower the heat and turn it off once the seeds have stopped popping. (This step may be optional)<br /> <br /> ==Powder==<br /> -Get 100g seeds and 25g of sodium carbonate grind them with a glass blender into a powder. (Check weight on scales and take note).<br /> <br /> ==Add water==<br /> -Add 150ml of water by spraying the seeds/ sodium carbonate mix with a spray bottle. Do this until the paste becomes doughy. Mix well.<br /> <br /> ==Dry Paste==<br /> -Dry the paste with a fan and optionally low heat.<br /> <br /> ==Defatting==<br /> -When dry (check by comparing weight previously noted), defat with 3 x 150 ml boiling Naphtha, then decant.<br /> Repeat with 100ml of warm (not boiling) xylene. Further defatting maybe required if solvent is not clean and is still pulling non polar material (fats).<br /> <br /> ==Pull==<br /> -Extract and pull with 3 x 450 ml DRY Acetone, filter store in jar. <br /> Add 5g-10g of Benzoic acid to acetone.<br /> <br /> ==Crystalisation==<br /> -5-HO-DMT will crystalise overtime this may take hours to a few days to happen be patient.<br /> <br /> <br /> [IMG]https://www.dmt-nexus.me/forum/resource.ashx?a=58372&amp;nc=1[/IMG]<br /> <br /> ==Decant &amp; Collect==<br /> -Decant and dry crystals for collection.<br /> <br /> ==Lab results:==<br /> -Lab results to follow soon.</div>

Trip https://wiki.dmt-nexus.me/Bufotenine_Benzoate 2023-05-31T12:07:52Z

<p>Trip: /* Crystalisation */</p> <hr /> <div>==Introduction= Bufotinine Benzoate (AKA 5-HO-DMT)==<br /> This Tek was written to be the quickest and easiest bufo extraction tek yet using cebil or yopo seeds. The final salt form is 5-HO-DMT benzoate which is smoother, easier to vape and appears more active per mg when compared to freebase 5-HO-DMT.<br /> <br /> Thanks to everyone who has contributed or helped experiment to aid in refining/ improving this process: Endlessness, Brennendes Wasser, _Trip_, and others.<br /> <br /> ==Safety==<br /> Review ethyl acetate safety information. Verify solvent MSDS, plastic compatibility, and clean evaporation.<br /> <br /> <br /> Following this advice does not guarantee safety. It is up to each adult individual to make their own personal decisions.<br /> <br /> <br /> ==Consumables==<br /> 100g of anadenanthera peregrina seeds or Anadenanthera colubrina<br /> 25g Sodium Carboante<br /> 150ml water <br /> 450ml Naphtha<br /> 100ml Xylene<br /> 450ml Acetone <br /> 5g-10g benzoic acid<br /> <br /> ==Equipment==<br /> Blender<br /> Frypan<br /> Spray bottle<br /> Jars<br /> Coffee or lab filters<br /> <br /> <br /> ==Detailed Process==<br /> Heat Seeds<br /> -Place seeds on minimal heat on fry pan, bring it up to heat until they start popping, lower the heat and turn it off once the seeds have stopped popping. (This step may be optional)<br /> <br /> ==Powder==<br /> -Get 100g seeds and 25g of sodium carbonate grind them with a glass blender into a powder. (Check weight on scales and take note).<br /> <br /> ==Add water==<br /> -Add 150ml of water by spraying the seeds/ sodium carbonate mix with a spray bottle. Do this until the paste becomes doughy. Mix well.<br /> <br /> ==Dry Paste==<br /> -Dry the paste with a fan and optionally low heat.<br /> <br /> ==Defatting==<br /> -When dry (check by comparing weight previously noted), defat with 3 x 150 ml boiling Naphtha, then decant.<br /> Repeat with 100ml of warm (not boiling) xylene. Further defatting maybe required if solvent is not clean and is still pulling non polar material (fats).<br /> <br /> ==Pull==<br /> -Extract and pull with 3 x 450 ml DRY Acetone, filter store in jar. <br /> Add 5g-10g of Benzoic acid to acetone.<br /> <br /> ==Crystalisation==<br /> -5-HO-DMT will crystalise overtime this may take hours to a few days to happen be patient.<br /> <br /> <br /> [IMG]--https://www.dmt-nexus.me/forum/resource.ashx?a=58372&amp;nc=1--[/IMG]<br /> <br /> ==Decant &amp; Collect==<br /> -Decant and dry crystals for collection.<br /> <br /> ==Lab results:==<br /> -Lab results to follow soon.</div>

Trip https://wiki.dmt-nexus.me/Bufotenine_Benzoate 2023-05-31T12:06:08Z

<p>Trip: /* Crystalisation */</p> <hr /> <div>==Introduction= Bufotinine Benzoate (AKA 5-HO-DMT)==<br /> This Tek was written to be the quickest and easiest bufo extraction tek yet using cebil or yopo seeds. The final salt form is 5-HO-DMT benzoate which is smoother, easier to vape and appears more active per mg when compared to freebase 5-HO-DMT.<br /> <br /> Thanks to everyone who has contributed or helped experiment to aid in refining/ improving this process: Endlessness, Brennendes Wasser, _Trip_, and others.<br /> <br /> ==Safety==<br /> Review ethyl acetate safety information. Verify solvent MSDS, plastic compatibility, and clean evaporation.<br /> <br /> <br /> Following this advice does not guarantee safety. It is up to each adult individual to make their own personal decisions.<br /> <br /> <br /> ==Consumables==<br /> 100g of anadenanthera peregrina seeds or Anadenanthera colubrina<br /> 25g Sodium Carboante<br /> 150ml water <br /> 450ml Naphtha<br /> 100ml Xylene<br /> 450ml Acetone <br /> 5g-10g benzoic acid<br /> <br /> ==Equipment==<br /> Blender<br /> Frypan<br /> Spray bottle<br /> Jars<br /> Coffee or lab filters<br /> <br /> <br /> ==Detailed Process==<br /> Heat Seeds<br /> -Place seeds on minimal heat on fry pan, bring it up to heat until they start popping, lower the heat and turn it off once the seeds have stopped popping. (This step may be optional)<br /> <br /> ==Powder==<br /> -Get 100g seeds and 25g of sodium carbonate grind them with a glass blender into a powder. (Check weight on scales and take note).<br /> <br /> ==Add water==<br /> -Add 150ml of water by spraying the seeds/ sodium carbonate mix with a spray bottle. Do this until the paste becomes doughy. Mix well.<br /> <br /> ==Dry Paste==<br /> -Dry the paste with a fan and optionally low heat.<br /> <br /> ==Defatting==<br /> -When dry (check by comparing weight previously noted), defat with 3 x 150 ml boiling Naphtha, then decant.<br /> Repeat with 100ml of warm (not boiling) xylene. Further defatting maybe required if solvent is not clean and is still pulling non polar material (fats).<br /> <br /> ==Pull==<br /> -Extract and pull with 3 x 450 ml DRY Acetone, filter store in jar. <br /> Add 5g-10g of Benzoic acid to acetone.<br /> <br /> ==Crystalisation==<br /> -5-HO-DMT will crystalise overtime this may take hours to a few days to happen be patient.<br /> <br /> [[File:Untitled - Copy.png]]<br /> <br /> ==Decant &amp; Collect==<br /> -Decant and dry crystals for collection.<br /> <br /> ==Lab results:==<br /> -Lab results to follow soon.</div>

Trip https://wiki.dmt-nexus.me/Bufotenine_Benzoate 2023-05-31T12:05:29Z

<p>Trip: /* Crystalisation */</p> <hr /> <div>==Introduction= Bufotinine Benzoate (AKA 5-HO-DMT)==<br /> This Tek was written to be the quickest and easiest bufo extraction tek yet using cebil or yopo seeds. The final salt form is 5-HO-DMT benzoate which is smoother, easier to vape and appears more active per mg when compared to freebase 5-HO-DMT.<br /> <br /> Thanks to everyone who has contributed or helped experiment to aid in refining/ improving this process: Endlessness, Brennendes Wasser, _Trip_, and others.<br /> <br /> ==Safety==<br /> Review ethyl acetate safety information. Verify solvent MSDS, plastic compatibility, and clean evaporation.<br /> <br /> <br /> Following this advice does not guarantee safety. It is up to each adult individual to make their own personal decisions.<br /> <br /> <br /> ==Consumables==<br /> 100g of anadenanthera peregrina seeds or Anadenanthera colubrina<br /> 25g Sodium Carboante<br /> 150ml water <br /> 450ml Naphtha<br /> 100ml Xylene<br /> 450ml Acetone <br /> 5g-10g benzoic acid<br /> <br /> ==Equipment==<br /> Blender<br /> Frypan<br /> Spray bottle<br /> Jars<br /> Coffee or lab filters<br /> <br /> <br /> ==Detailed Process==<br /> Heat Seeds<br /> -Place seeds on minimal heat on fry pan, bring it up to heat until they start popping, lower the heat and turn it off once the seeds have stopped popping. (This step may be optional)<br /> <br /> ==Powder==<br /> -Get 100g seeds and 25g of sodium carbonate grind them with a glass blender into a powder. (Check weight on scales and take note).<br /> <br /> ==Add water==<br /> -Add 150ml of water by spraying the seeds/ sodium carbonate mix with a spray bottle. Do this until the paste becomes doughy. Mix well.<br /> <br /> ==Dry Paste==<br /> -Dry the paste with a fan and optionally low heat.<br /> <br /> ==Defatting==<br /> -When dry (check by comparing weight previously noted), defat with 3 x 150 ml boiling Naphtha, then decant.<br /> Repeat with 100ml of warm (not boiling) xylene. Further defatting maybe required if solvent is not clean and is still pulling non polar material (fats).<br /> <br /> ==Pull==<br /> -Extract and pull with 3 x 450 ml DRY Acetone, filter store in jar. <br /> Add 5g-10g of Benzoic acid to acetone.<br /> <br /> ==Crystalisation==<br /> -5-HO-DMT will crystalise overtime this may take hours to a few days to happen be patient.<br /> <br /> https://www.dmt-nexus.me/forum/resource.ashx?a=58372<br /> <br /> ==Decant &amp; Collect==<br /> -Decant and dry crystals for collection.<br /> <br /> ==Lab results:==<br /> -Lab results to follow soon.</div>

Trip https://wiki.dmt-nexus.me/Bufotenine_Benzoate 2023-05-31T12:04:38Z

<p>Trip: /* Introduction= Bufotinine Benzoate (AKA 5-HO-DMT) */</p> <hr /> <div>==Introduction= Bufotinine Benzoate (AKA 5-HO-DMT)==<br /> This Tek was written to be the quickest and easiest bufo extraction tek yet using cebil or yopo seeds. The final salt form is 5-HO-DMT benzoate which is smoother, easier to vape and appears more active per mg when compared to freebase 5-HO-DMT.<br /> <br /> Thanks to everyone who has contributed or helped experiment to aid in refining/ improving this process: Endlessness, Brennendes Wasser, _Trip_, and others.<br /> <br /> ==Safety==<br /> Review ethyl acetate safety information. Verify solvent MSDS, plastic compatibility, and clean evaporation.<br /> <br /> <br /> Following this advice does not guarantee safety. It is up to each adult individual to make their own personal decisions.<br /> <br /> <br /> ==Consumables==<br /> 100g of anadenanthera peregrina seeds or Anadenanthera colubrina<br /> 25g Sodium Carboante<br /> 150ml water <br /> 450ml Naphtha<br /> 100ml Xylene<br /> 450ml Acetone <br /> 5g-10g benzoic acid<br /> <br /> ==Equipment==<br /> Blender<br /> Frypan<br /> Spray bottle<br /> Jars<br /> Coffee or lab filters<br /> <br /> <br /> ==Detailed Process==<br /> Heat Seeds<br /> -Place seeds on minimal heat on fry pan, bring it up to heat until they start popping, lower the heat and turn it off once the seeds have stopped popping. (This step may be optional)<br /> <br /> ==Powder==<br /> -Get 100g seeds and 25g of sodium carbonate grind them with a glass blender into a powder. (Check weight on scales and take note).<br /> <br /> ==Add water==<br /> -Add 150ml of water by spraying the seeds/ sodium carbonate mix with a spray bottle. Do this until the paste becomes doughy. Mix well.<br /> <br /> ==Dry Paste==<br /> -Dry the paste with a fan and optionally low heat.<br /> <br /> ==Defatting==<br /> -When dry (check by comparing weight previously noted), defat with 3 x 150 ml boiling Naphtha, then decant.<br /> Repeat with 100ml of warm (not boiling) xylene. Further defatting maybe required if solvent is not clean and is still pulling non polar material (fats).<br /> <br /> ==Pull==<br /> -Extract and pull with 3 x 450 ml DRY Acetone, filter store in jar. <br /> Add 5g-10g of Benzoic acid to acetone.<br /> <br /> ==Crystalisation==<br /> -5-HO-DMT will crystalise overtime this may take hours to a few days to happen be patient.<br /> <br /> ==Decant &amp; Collect==<br /> -Decant and dry crystals for collection.<br /> <br /> ==Lab results:==<br /> -Lab results to follow soon.</div>

Trip https://wiki.dmt-nexus.me/Bufotenine_Benzoate 2023-05-31T11:59:34Z

<p>Trip: </p> <hr /> <div>==Introduction= Bufotinine Benzoate (AKA 5-HO-DMT)==<br /> This Tek was written to be the quickest and easiest bufo extraction tek yet using cebil or yopo seeds. The final salt form is 5-HO-DMT benzoate which is smoother, easier to vape and appears more active per mg when compared to freebase 5-HO-DMT.<br /> <br /> Thanks to everyone who has contributed or helped experiment to aid in refining/ improving this process: Endlessness, BW, _Trip_, and others.<br /> <br /> <br /> ==Safety==<br /> Review ethyl acetate safety information. Verify solvent MSDS, plastic compatibility, and clean evaporation.<br /> <br /> <br /> Following this advice does not guarantee safety. It is up to each adult individual to make their own personal decisions.<br /> <br /> <br /> ==Consumables==<br /> 100g of anadenanthera peregrina seeds or Anadenanthera colubrina<br /> 25g Sodium Carboante<br /> 150ml water <br /> 450ml Naphtha<br /> 100ml Xylene<br /> 450ml Acetone <br /> 5g-10g benzoic acid<br /> <br /> ==Equipment==<br /> Blender<br /> Frypan<br /> Spray bottle<br /> Jars<br /> Coffee or lab filters<br /> <br /> <br /> ==Detailed Process==<br /> Heat Seeds<br /> -Place seeds on minimal heat on fry pan, bring it up to heat until they start popping, lower the heat and turn it off once the seeds have stopped popping. (This step may be optional)<br /> <br /> ==Powder==<br /> -Get 100g seeds and 25g of sodium carbonate grind them with a glass blender into a powder. (Check weight on scales and take note).<br /> <br /> ==Add water==<br /> -Add 150ml of water by spraying the seeds/ sodium carbonate mix with a spray bottle. Do this until the paste becomes doughy. Mix well.<br /> <br /> ==Dry Paste==<br /> -Dry the paste with a fan and optionally low heat.<br /> <br /> ==Defatting==<br /> -When dry (check by comparing weight previously noted), defat with 3 x 150 ml boiling Naphtha, then decant.<br /> Repeat with 100ml of warm (not boiling) xylene. Further defatting maybe required if solvent is not clean and is still pulling non polar material (fats).<br /> <br /> ==Pull==<br /> -Extract and pull with 3 x 450 ml DRY Acetone, filter store in jar. <br /> Add 5g-10g of Benzoic acid to acetone.<br /> <br /> ==Crystalisation==<br /> -5-HO-DMT will crystalise overtime this may take hours to a few days to happen be patient.<br /> <br /> ==Decant &amp; Collect==<br /> -Decant and dry crystals for collection.<br /> <br /> ==Lab results:==<br /> -Lab results to follow soon.</div>

Trip https://wiki.dmt-nexus.me/Bufotenine_Benzoate 2023-05-31T11:58:35Z

<p>Trip: </p> <hr /> <div>Introduction Bufotinine Benzoate (AKA 5-HO-DMT)<br /> This Tek was written to be the quickest and easiest bufo extraction tek yet using cebil or yopo seeds. The final salt form is 5-HO-DMT benzoate which is smoother, easier to vape and appears more active per mg when compared to freebase 5-HO-DMT.<br /> <br /> Thanks to everyone who has contributed or helped experiment to aid in refining/ improving this process: Endlessness, BW, _Trip_, and others.<br /> <br /> <br /> Safety<br /> Review ethyl acetate safety information. Verify solvent MSDS, plastic compatibility, and clean evaporation.<br /> <br /> <br /> Following this advice does not guarantee safety. It is up to each adult individual to make their own personal decisions.<br /> <br /> <br /> Consumables<br /> 100g of anadenanthera peregrina seeds or Anadenanthera colubrina<br /> 25g Sodium Carboante<br /> 150ml water <br /> 450ml Naphtha<br /> 100ml Xylene<br /> 450ml Acetone <br /> 5g-10g benzoic acid<br /> <br /> Equipment<br /> Blender<br /> Frypan<br /> Spray bottle<br /> Jars<br /> Coffee or lab filters<br /> <br /> <br /> Detailed Process<br /> Heat Seeds<br /> -Place seeds on minimal heat on fry pan, bring it up to heat until they start popping, lower the heat and turn it off once the seeds have stopped popping. (This step may be optional)<br /> <br /> Powder<br /> -Get 100g seeds and 25g of sodium carbonate grind them with a glass blender into a powder. (Check weight on scales and take note).<br /> <br /> Add water<br /> -Add 150ml of water by spraying the seeds/ sodium carbonate mix with a spray bottle. Do this until the paste becomes doughy. Mix well.<br /> <br /> Dry Paste<br /> -Dry the paste with a fan and optionally low heat.<br /> <br /> Defatting<br /> -When dry (check by comparing weight previously noted), defat with 3 x 150 ml boiling Naphtha, then decant.<br /> Repeat with 100ml of warm (not boiling) xylene. Further defatting maybe required if solvent is not clean and is still pulling non polar material (fats).<br /> <br /> Pull<br /> -Extract and pull with 3 x 450 ml DRY Acetone, filter store in jar. <br /> Add 5g-10g of Benzoic acid to acetone.<br /> <br /> Crystalisation<br /> -5-HO-DMT will crystalise overtime this may take hours to a few days to happen be patient.<br /> <br /> Decant &amp; Collect<br /> -Decant and dry crystals for collection.<br /> <br /> Lab results:<br /> -Lab results to follow soon.</div>

Trip https://wiki.dmt-nexus.me/Bufotenine_Benzoate 2023-05-31T11:35:50Z

<p>Trip: Created page with &quot;Bufotenine Benzoate Tek&quot;</p> <hr /> <div>Bufotenine Benzoate Tek</div>

Trip https://wiki.dmt-nexus.me/Category:Extraction_Tek 2023-05-31T11:35:31Z

<p>Trip: /* BUFOTENINE */</p> <hr /> <div>An Extraction Tek is a manual to extract certain chemicals from a given source.<br /> <br /> To learn more about extractions in general and how they work, check the [http://wiki.dmt-nexus.me/FAQ#Where_to_start.3F FAQ], the [http://wiki.dmt-nexus.me/DMT_Extraction_Overview extraction overview], as well as read a few different teks, even if you don't plan on doing them, because many of them explain the processes and why each step is done.<br /> <br /> One does not need to be a chemist to perform an extraction. Don't worry about not understanding everything at first. Keep reading, inform yourself, take safety precautions, don't throw anything away before you're done with your extraction and don't consume anything you are not sure its clean.<br /> <br /> {{Main Page/Portal|[[Image:Information.png]]|'''[[:Category:Extraction_Tek|Extraction Teks]]'''|<br /> &lt;table&gt;<br /> &lt;tr&gt;<br /> &lt;td&gt;<br /> <br /> &lt;/td&gt;<br /> &lt;/tr&gt;<br /> &lt;/table&gt;<br /> }}<br /> <br /> ==DMT==<br /> ===A/B===<br /> <br /> * [[Lextek]]<br /> * [[Marsofold's tek]]<br /> * [[Shaggy's Jungle Tek]]<br /> * [[The DMT Handbook]]<br /> * [[Vovin's tek]]<br /> * [[ACRB Tek By Thick-Light]]<br /> * [https://www.dmt-nexus.me/forum/default.aspx?g=posts&amp;t=58064 ACRB TEK 100g &quot;PICS&quot; (Newbie Friendly)]<br /> * [[The Wanderer's Tek]]<br /> * [https://wiki.dmt-nexus.me/User_talk:Justamessenger SP's ACRB Extraction Tek]<br /> <br /> ===STB===<br /> <br /> * [[Jorkest's D-Limonene and Fumaric Acid Approach]]<br /> * [[Lazyman's tek]]<br /> * [[Noman's tek]]<br /> * [[STC - Dream Weaver's tek]]<br /> <br /> ===STB-A/B hybrid===<br /> <br /> * [[BLAB_-_The_Big_Leisurely_AB|BLAB]]<br /> * [[PanoraMIX European AB]]<br /> * [[Nontoxic_limonene_tek|SyZyGyPSy's Nontoxic Limomene Tek]]<br /> * [[Cyb's Hybrid ATB 'Salt' Tek]]<br /> * [https://www.dmt-nexus.me/forum/default.aspx?g=posts&amp;m=459391#post459391 Cyb's MAX ION Tek]<br /> <br /> ===Dry tek===<br /> <br /> * [[Amor fati's Nontoxic Approach to Spice Extraction]]<br /> * [[Q21Q21's Vinegar/Lime A/B Extraction Tek]]<br /> * [[HIELO]]<br /> <br /> ==MESCALINE==<br /> <br /> ===A/B===<br /> <br /> * [[Kash's A/B Mescaline Extraction]]<br /> <br /> ===STB===<br /> <br /> * [[LucidLemonade's sunflower oil mescaline extraction]]<br /> <br /> ===Crude extract===<br /> <br /> * [[House's cacti preparation tek]]<br /> <br /> ===Dry tek===<br /> <br /> * [[69ron's D-Limonene Mescaline Extraction]]<br /> * [[CIELO]]<br /> <br /> ==BUFOTENINE==<br /> <br /> ===Dry tek===<br /> <br /> * [[Jorkest's D-Limonene Bufotenine Extraction]]<br /> * [[http://www.dmt-nexus.me/forum/default.aspx?g=posts&amp;t=10071 No smell bufo extraction]]<br /> * [[BW's Bufotenine Dry Tek]]<br /> * [[Bufotenine Benzoate]]<br /> <br /> ===IPA extract===<br /> <br /> * [[Bufotenine IPA Extraction and Bufojam Changa Tek]]<br /> <br /> ==HARMALAS==<br /> <br /> ===A/B===<br /> <br /> * [[Harmalas Extraction and Separation Guide]]<br /> * [[EASY Harmaloid Freebase TEK]]<br /> * [[Easy Caapi Vine Alkaloid Extraction Guide]]<br /> * [[Enoons Cold Caapi Tek]]<br /> * [[The Tao of Rue Extraction]]<br /> <br /> ===Crude Manske (salt) Extract===<br /> <br /> * [[Harmine Crystals from Syrian Rue]]<br /> <br /> ===Dry Tek===<br /> * [[Ethyl Acetate Approach Harmala]]<br /> <br /> ==LSA==<br /> <br /> ===IPA extract===<br /> <br /> * [[PanoraMIX HBWR Extract]]<br /> <br /> ===Acetone extract===<br /> <br /> * [[Kash's Advanced LSA Extraction]]<br /> <br /> ==SALVIA==<br /> <br /> ===Acetone extract===<br /> <br /> * [[PanoraMIX salvia extact]]<br /> * [[Chilled Acetone with IPA and Naphtha re-X]]<br /> <br /> [[Category:Tek]]<br /> <br /> ==Conversion teks==<br /> <br /> [[DMT Fumarate to DMT Freebase]].<br /> <br /> [[THH_reduction]]</div>

Trip https://wiki.dmt-nexus.me/Ethyl_Acetate_Approach_Harmala 2023-03-29T11:41:42Z

<p>Trip: /* Crash/ Filter TEK Complete */</p> <hr /> <div>= Introduction =<br /> This Tek was inspired by Loveall's Cielo Tek, with the aim of cutting out manske steps to aid in yields and substantially quicken the process while maintaining purity. The quickest run has been 2.5hours with decent yields and purity.<br /> <br /> Thanks to everyone who has contributed or helped experiment to aid in refining/ improving this process: Loveall, Benzyme, Downwardsfromzero, _Trip_, and others.<br /> <br /> This Tek is still a work in progress&lt;ref&gt;Forum Link[https://www.dmt-nexus.me/forum/default.aspx?g=posts&amp;t=93378]&lt;/ref&gt; however lab and test results have been confirmed and are very promising for a quick Tek. Feel free to contribute. More photo's to follow soon.<br /> <br /> Please take your time with your first extraction, although this is a quick and easy Tek you don't want to rush it and make a mistake.<br /> <br /> = Safety = <br /> Review ethyl acetate&lt;ref&gt;Ethyl acetate safety[https://www.msdsonline.com/2015/04/10/ethyl-acetate-a-sweet-smelling-safety-hazard/#:~:text=Ethyl%20acetate%20is%20highly%20flammable,with%20the%20eyes%20or%20skin.]&lt;/ref&gt; and citric acid&lt;ref&gt;Citric Acid Safety[https://wiki.dmt-nexus.me/Citric_Acid_Safety#Process_.F0.9F.A5.9E]&lt;/ref&gt; safety information. Verify solvent MSDS, plastic compatibility, and clean evaporation.<br /> <br /> This TEK is food safe if food grade materials are used.<br /> <br /> <br /> Following this advice does not guarantee safety. It is up to each adult individual to make their own personal decisions.<br /> <br /> <br /> ==Consumables==<br /> *300ml water/ 600-800ml of distilled water (tap water works fine too) <br /> *25g Ca(OH)<br /> *100g of Syrian Rue seeds (B. Caapi should work too but is yet to be tested).<br /> *1lt ethyl acetate (sometimes sold as &quot;MEK substitute&quot;)<br /> *10-15g of citric acid <br /> *Sodium Carbonate<br /> *1lt Jar<br /> <br /> ==Equipment==<br /> *Blender<br /> *French press <br /> *Kitchen scale <br /> *Coffee filters, support basket, and funnel Or lab filter and vacuum pump.<br /> *1lt mason glass jars with lids<br /> *Fridge <br /> *Milligram scale <br /> *Microwave<br /> <br /> <br /> <br /> = Detailed Process =<br /> <br /> <br /> == Base Water ==<br /> -Add 300ml of water to 25g of calcium hydroxide and mix to form 'base water'.<br /> Alternatively one can use sodium carbonate (this may negate the need for filtering later). <br /> Note: Sodium Carbonate has not been fully tested start to finish.<br /> <br /> == Powder ==<br /> -Get 100g of rue seeds and grind them up, mix with 'base water'. A glass bender is quickest.<br /> <br /> == Microwave ==<br /> -Microwave the rue/base mix until close to 2/3rd's of the water content is steamed off (use kitchen scales to measure this). As a guide a 750 watt microwave at 5-7min bursts should work fine. Mix between bursts. Several bursts will be required. <br /> <br /> If interested, see further investigations for microwaving below.<br /> <br /> == Water Bath ==<br /> -Prepare a warm water bath with boiling water and warm 1lt of EA. No open flames. (This step helps yields).<br /> <br /> == Pulling ==<br /> -Place ground up 'base paste rue seed mix' in a french press. Using the french press conduct 6 pulls with the 1lt of warm EA. So 6x 160ml pulls approx (keep in mind rue seeds will absorb a little bit of EA). Carefully decant into 1lt jar(6x warm pulls at 1-2 mins each). Decant from the french press after each pull. Keep rue base mix and fresh EA in the warm water bath to improve yield (obviously in their respective containers).<br /> <br /> == Recovery/ Filter ==<br /> -Approx just over 800ml of EA should be recovered and then filtered (filtering may not be necessary if one has used sodium carbonate as a base, this is still under investigation). Lab filter is recommended, coffee filters should work too.<br /> <br /> <br /> [[File:Download.jpeg-2.jpg]] [[File:Images.jpeg-6.jpg]] ‎<br /> <br /> <br /> <br /> <br /> <br /> Recovered vs Filtered<br /> <br /> == Salting ==<br /> -Add 15g of citirc acid to the combined EA pulls (the approx 800ml of EA) and shake for 5-10mins (red/orange/yellow oil should form very fast). Orange/red goo forms at the base of the jar and the rest of the jar gets covered with sticky yellow goo (making it easy to decant). (This goo should crystalize if left for 24hours+. This is not necessary though, the goo makes decanting easy so one can decant right away).<br /> <br /> [[File:Download.jpeg-1.jpg ]] (Initial clouding when adding citric acid).<br /> <br /> [[File:Images.jpeg-10.jpg]] <br /> (Don't let the photo deceive you the whole Jar is covered in sticky yellow harmala citrate residue).<br /> <br /> == Decant &amp; Reclaim ==<br /> -Decant EA (this can be cleaned and reused next extraction). One can also add a little bit of EA to the citrate stuck to the jar to clean it up a little bit but it is not necessary. Again decant this EA.<br /> <br /> == Dissolve Goo ==<br /> -After the tiny amount of EA still left in the jar evaporates off the goo, add minimum 850ml of warm water to the citrate goo, it will dissolve fairly quickly. <br /> <br /> (One can ratio it down if using less seeds). The more water used gives a cleaner product (in appearance anyway). One can use even more water 1lt-1.5lt to achieve a whiter end result (see further investigation notes on use of too much water in this step).<br /> <br /> <br /> <br /> [[File:20220415 182000.jpg]] <br /> <br /> <br /> <br /> Above is a photo comparing the final end result, more vs less water used in this step. (1lt vs 300ml)<br /> <br /> == Base ==<br /> -Base slowly with sodium carbonate (you can shake up the jar to get excess sodium carbonate to dissolve once the acid is neutralized). Add enough sodium carbonate until the harmala starts to crash out then add a little bit more.<br /> <br /> [[File:Images.jpeg-9.jpg ]] Initial basing &amp; precipitation.<br /> <br /> == Crash/ Filter TEK Complete ==<br /> -Harmala will crash out quickly. Some of the FB harmala will float to the top, this needs to be left to cool.<br /> (Sticking the jar in a freezer '''appears''' to speed up the process and harmala crashes as it cools. The floating harmala should settle. This should not take long). <br /> <br /> [[File:Index1.jpg]] Crashing of Harmala (some will float to the top some settles to the bottom).<br /> <br /> [[File:Images.jpeg-8.jpg]] '''As a rule of thumb I wait for majority of the floating harmala to settle to the bottom'''. This rarely exceeds the 2 hour mark, again usually a lot quicker - as little as half an hour. However, one can filter straight away.<br /> <br /> <br /> <br /> Once it has finished crashing out filter and dry the product (lab filters or coffee filters should work fine). <br /> <br /> <br /> Well done this should have been a quick and easy run. '''3.7%+''' is usually the minimum percentage pulled on first run. The process can be repeated on spent material and re-pulled with hot EA to get over '''5%'''.<br /> Final product is usually off white almost greyish in color harmala. It doesn't necessarily represent purity in this Tek and color appears to be dependent on how much water was used during dissolving and basing step. If you <br /> look at lab sample B vs C, sample C had extra clean up steps added (and although the signals appear slightly clearer) sample C came out more of a tan color than off white/grey. <br /> If one is after a purer looking product you can do a 5% ammonia wash during the final filter before drying (this has reported to clean up harmala).<br /> <br /> [[File:Download.jpeg.jpg ‎]]<br /> <br /> <br /> No need to leave the product overnight to crash, if left for too long (say 24hrs+) some impurities appear to crash out with it. The final product in this step should crash out quick and should/ can be filtered within a hour or 2 (often quicker). <br /> Once filtered and dried you have the final product.<br /> <br /> (Keep the sodium carbonated water after filtering, more harmala may crash out overnight. It usually appears more impure by color and may contain impurities though an analysis has not been confirmed. It is likely still useable)<br /> <br /> == Lab Analysis ==<br /> [[File: A1.jpg]]<br /> <br /> Above is harmala lab analysis results.<br /> Figure A is the traditional 3x Manske, figure B &amp; C are from the EA approach (B &amp; C were conducted with slightly different variations). Figure B is the standard EA approach TEK as written above.<br /> The peaks indicate very clean harmine/harmaline. All main peaks can be attributed to harmala even 197 represent harmala with the loss -CH3 or and 169 is likely loss of -OCH3 functional groups during LC-MS. Results run in positive mode adds M 1+.<br /> <br /> == Further investigations ==<br /> -Sodium Carbonate should be usable as a base for this Tek but it's yet to be confirmed.<br /> <br /> -Chemical drying solvent after pulls only slightly changes the end result/ purity and is not necessary based of lab results..<br /> <br /> -A mini A/B at the end for clean up does not appear to change end result/ purity (it will likely make the harmala darker in appearance, reasons unknown).<br /> <br /> -Other acids are yet to be tested. Fumaric acid was briefly tested and should work. Phosphoric acid has been limitedly tested appears to behave like citric acid.<br /> <br /> -Microwave route may be unnecessary as eventually discovered with the Cielo Tek. If this is the case, water content in the first step may need to be reduced below 300ml. This may be like the Cielo Tek and require more water to facilitate efficient pulls, thus may need to be fine tuned. And like the Cielo tek may not need microwaving. However for now, those ratios and the microwave step should work fine so stick with these values and the use of a microwave.<br /> <br /> -Dissolving the goo in more water appears to give a purer looking product, using too little amount of water gives a very impure looking product. The ideal ratio is yet to be worked out. This may not affect purity to a great degree. Lab results have shown color doesn't necessarily equal purity in this tek. More water may lengthen the time needed to crash out harmala and or reduce yields. Note, this doesn't seem to be the case but further tests are needed.<br /> <br /> -This process will likely work with B. Caapi but has yet been tested but should work fine.<br /> <br /> -Butyl acetate does not appear to work effectively and harmala citrate will not crash out of BA.<br /> <br /> == Reuse ==<br /> Reusing solvents is encouraged&lt;ref&gt;On reusing non polar solvent[https://www.dmt-nexus.me/forum/default.aspx?g=posts&amp;t=31398]&lt;/ref&gt; at the DMT nexus.<br /> <br /> <br /> Wash spent extract with sodium carbonate saturated water (35% by weight). About 1/5 of the solvent volume as saturated water is enough. Shake vigorously (emulsions do not form). CO2 bubbles may be visible during citric acid neutralization. Keep an eye on any bubbles and release any pressure buildup regularly. Neutralization can be optionally verified with pH paper. Rest washed solution until clear (up to a day or more).<br /> <br /> <br /> Remove the water layer with a pipette or separatory funnel. Freezing the solvent and filtering the ice slush that forms with a metal strainer is also an option. Finally, decant off any excess solid sodium carbonate/citrate. CaCl2 (sold as deicer, calcium hardener for pools and sometimes is the only ingredient in moisture absorbers tubs) can be used to ensure there is no water still left in the EA.<br /> <br /> == References ==<br /> &lt;references/&gt;</div>

Trip https://wiki.dmt-nexus.me/Ethyl_Acetate_Approach_Harmala 2023-03-29T11:41:15Z

<p>Trip: /* Crash/ Filter TEK Complete */</p> <hr /> <div>= Introduction =<br /> This Tek was inspired by Loveall's Cielo Tek, with the aim of cutting out manske steps to aid in yields and substantially quicken the process while maintaining purity. The quickest run has been 2.5hours with decent yields and purity.<br /> <br /> Thanks to everyone who has contributed or helped experiment to aid in refining/ improving this process: Loveall, Benzyme, Downwardsfromzero, _Trip_, and others.<br /> <br /> This Tek is still a work in progress&lt;ref&gt;Forum Link[https://www.dmt-nexus.me/forum/default.aspx?g=posts&amp;t=93378]&lt;/ref&gt; however lab and test results have been confirmed and are very promising for a quick Tek. Feel free to contribute. More photo's to follow soon.<br /> <br /> Please take your time with your first extraction, although this is a quick and easy Tek you don't want to rush it and make a mistake.<br /> <br /> = Safety = <br /> Review ethyl acetate&lt;ref&gt;Ethyl acetate safety[https://www.msdsonline.com/2015/04/10/ethyl-acetate-a-sweet-smelling-safety-hazard/#:~:text=Ethyl%20acetate%20is%20highly%20flammable,with%20the%20eyes%20or%20skin.]&lt;/ref&gt; and citric acid&lt;ref&gt;Citric Acid Safety[https://wiki.dmt-nexus.me/Citric_Acid_Safety#Process_.F0.9F.A5.9E]&lt;/ref&gt; safety information. Verify solvent MSDS, plastic compatibility, and clean evaporation.<br /> <br /> This TEK is food safe if food grade materials are used.<br /> <br /> <br /> Following this advice does not guarantee safety. It is up to each adult individual to make their own personal decisions.<br /> <br /> <br /> ==Consumables==<br /> *300ml water/ 600-800ml of distilled water (tap water works fine too) <br /> *25g Ca(OH)<br /> *100g of Syrian Rue seeds (B. Caapi should work too but is yet to be tested).<br /> *1lt ethyl acetate (sometimes sold as &quot;MEK substitute&quot;)<br /> *10-15g of citric acid <br /> *Sodium Carbonate<br /> *1lt Jar<br /> <br /> ==Equipment==<br /> *Blender<br /> *French press <br /> *Kitchen scale <br /> *Coffee filters, support basket, and funnel Or lab filter and vacuum pump.<br /> *1lt mason glass jars with lids<br /> *Fridge <br /> *Milligram scale <br /> *Microwave<br /> <br /> <br /> <br /> = Detailed Process =<br /> <br /> <br /> == Base Water ==<br /> -Add 300ml of water to 25g of calcium hydroxide and mix to form 'base water'.<br /> Alternatively one can use sodium carbonate (this may negate the need for filtering later). <br /> Note: Sodium Carbonate has not been fully tested start to finish.<br /> <br /> == Powder ==<br /> -Get 100g of rue seeds and grind them up, mix with 'base water'. A glass bender is quickest.<br /> <br /> == Microwave ==<br /> -Microwave the rue/base mix until close to 2/3rd's of the water content is steamed off (use kitchen scales to measure this). As a guide a 750 watt microwave at 5-7min bursts should work fine. Mix between bursts. Several bursts will be required. <br /> <br /> If interested, see further investigations for microwaving below.<br /> <br /> == Water Bath ==<br /> -Prepare a warm water bath with boiling water and warm 1lt of EA. No open flames. (This step helps yields).<br /> <br /> == Pulling ==<br /> -Place ground up 'base paste rue seed mix' in a french press. Using the french press conduct 6 pulls with the 1lt of warm EA. So 6x 160ml pulls approx (keep in mind rue seeds will absorb a little bit of EA). Carefully decant into 1lt jar(6x warm pulls at 1-2 mins each). Decant from the french press after each pull. Keep rue base mix and fresh EA in the warm water bath to improve yield (obviously in their respective containers).<br /> <br /> == Recovery/ Filter ==<br /> -Approx just over 800ml of EA should be recovered and then filtered (filtering may not be necessary if one has used sodium carbonate as a base, this is still under investigation). Lab filter is recommended, coffee filters should work too.<br /> <br /> <br /> [[File:Download.jpeg-2.jpg]] [[File:Images.jpeg-6.jpg]] ‎<br /> <br /> <br /> <br /> <br /> <br /> Recovered vs Filtered<br /> <br /> == Salting ==<br /> -Add 15g of citirc acid to the combined EA pulls (the approx 800ml of EA) and shake for 5-10mins (red/orange/yellow oil should form very fast). Orange/red goo forms at the base of the jar and the rest of the jar gets covered with sticky yellow goo (making it easy to decant). (This goo should crystalize if left for 24hours+. This is not necessary though, the goo makes decanting easy so one can decant right away).<br /> <br /> [[File:Download.jpeg-1.jpg ]] (Initial clouding when adding citric acid).<br /> <br /> [[File:Images.jpeg-10.jpg]] <br /> (Don't let the photo deceive you the whole Jar is covered in sticky yellow harmala citrate residue).<br /> <br /> == Decant &amp; Reclaim ==<br /> -Decant EA (this can be cleaned and reused next extraction). One can also add a little bit of EA to the citrate stuck to the jar to clean it up a little bit but it is not necessary. Again decant this EA.<br /> <br /> == Dissolve Goo ==<br /> -After the tiny amount of EA still left in the jar evaporates off the goo, add minimum 850ml of warm water to the citrate goo, it will dissolve fairly quickly. <br /> <br /> (One can ratio it down if using less seeds). The more water used gives a cleaner product (in appearance anyway). One can use even more water 1lt-1.5lt to achieve a whiter end result (see further investigation notes on use of too much water in this step).<br /> <br /> <br /> <br /> [[File:20220415 182000.jpg]] <br /> <br /> <br /> <br /> Above is a photo comparing the final end result, more vs less water used in this step. (1lt vs 300ml)<br /> <br /> == Base ==<br /> -Base slowly with sodium carbonate (you can shake up the jar to get excess sodium carbonate to dissolve once the acid is neutralized). Add enough sodium carbonate until the harmala starts to crash out then add a little bit more.<br /> <br /> [[File:Images.jpeg-9.jpg ]] Initial basing &amp; precipitation.<br /> <br /> == Crash/ Filter TEK Complete ==<br /> -Harmala will crash out quickly. Some of the FB harmala will float to the top, this needs to be left to cool.<br /> (Sticking the jar in a freezer '''appears''' to speed up the process and harmala crashes as it cools. The floating harmala should settle. This should not take long). <br /> <br /> [[File:Index1.jpg]] Crashing of Harmala (some will float to the top some settles to the bottom).<br /> <br /> [[File:Images.jpeg-8.jpg]] '''As a rule of thumb I wait for majority of the floating harmala to settle to the bottom'''. This rarely exceeds the 2 hour mark, again usually a lot quicker - as little as half an hour. However, one can decant straight away.<br /> <br /> <br /> <br /> Once it has finished crashing out filter and dry the product (lab filters or coffee filters should work fine). <br /> <br /> <br /> Well done this should have been a quick and easy run. '''3.7%+''' is usually the minimum percentage pulled on first run. The process can be repeated on spent material and re-pulled with hot EA to get over '''5%'''.<br /> Final product is usually off white almost greyish in color harmala. It doesn't necessarily represent purity in this Tek and color appears to be dependent on how much water was used during dissolving and basing step. If you <br /> look at lab sample B vs C, sample C had extra clean up steps added (and although the signals appear slightly clearer) sample C came out more of a tan color than off white/grey. <br /> If one is after a purer looking product you can do a 5% ammonia wash during the final filter before drying (this has reported to clean up harmala).<br /> <br /> [[File:Download.jpeg.jpg ‎]]<br /> <br /> <br /> No need to leave the product overnight to crash, if left for too long (say 24hrs+) some impurities appear to crash out with it. The final product in this step should crash out quick and should/ can be filtered within a hour or 2 (often quicker). <br /> Once filtered and dried you have the final product.<br /> <br /> (Keep the sodium carbonated water after filtering, more harmala may crash out overnight. It usually appears more impure by color and may contain impurities though an analysis has not been confirmed. It is likely still useable)<br /> <br /> == Lab Analysis ==<br /> [[File: A1.jpg]]<br /> <br /> Above is harmala lab analysis results.<br /> Figure A is the traditional 3x Manske, figure B &amp; C are from the EA approach (B &amp; C were conducted with slightly different variations). Figure B is the standard EA approach TEK as written above.<br /> The peaks indicate very clean harmine/harmaline. All main peaks can be attributed to harmala even 197 represent harmala with the loss -CH3 or and 169 is likely loss of -OCH3 functional groups during LC-MS. Results run in positive mode adds M 1+.<br /> <br /> == Further investigations ==<br /> -Sodium Carbonate should be usable as a base for this Tek but it's yet to be confirmed.<br /> <br /> -Chemical drying solvent after pulls only slightly changes the end result/ purity and is not necessary based of lab results..<br /> <br /> -A mini A/B at the end for clean up does not appear to change end result/ purity (it will likely make the harmala darker in appearance, reasons unknown).<br /> <br /> -Other acids are yet to be tested. Fumaric acid was briefly tested and should work. Phosphoric acid has been limitedly tested appears to behave like citric acid.<br /> <br /> -Microwave route may be unnecessary as eventually discovered with the Cielo Tek. If this is the case, water content in the first step may need to be reduced below 300ml. This may be like the Cielo Tek and require more water to facilitate efficient pulls, thus may need to be fine tuned. And like the Cielo tek may not need microwaving. However for now, those ratios and the microwave step should work fine so stick with these values and the use of a microwave.<br /> <br /> -Dissolving the goo in more water appears to give a purer looking product, using too little amount of water gives a very impure looking product. The ideal ratio is yet to be worked out. This may not affect purity to a great degree. Lab results have shown color doesn't necessarily equal purity in this tek. More water may lengthen the time needed to crash out harmala and or reduce yields. Note, this doesn't seem to be the case but further tests are needed.<br /> <br /> -This process will likely work with B. Caapi but has yet been tested but should work fine.<br /> <br /> -Butyl acetate does not appear to work effectively and harmala citrate will not crash out of BA.<br /> <br /> == Reuse ==<br /> Reusing solvents is encouraged&lt;ref&gt;On reusing non polar solvent[https://www.dmt-nexus.me/forum/default.aspx?g=posts&amp;t=31398]&lt;/ref&gt; at the DMT nexus.<br /> <br /> <br /> Wash spent extract with sodium carbonate saturated water (35% by weight). About 1/5 of the solvent volume as saturated water is enough. Shake vigorously (emulsions do not form). CO2 bubbles may be visible during citric acid neutralization. Keep an eye on any bubbles and release any pressure buildup regularly. Neutralization can be optionally verified with pH paper. Rest washed solution until clear (up to a day or more).<br /> <br /> <br /> Remove the water layer with a pipette or separatory funnel. Freezing the solvent and filtering the ice slush that forms with a metal strainer is also an option. Finally, decant off any excess solid sodium carbonate/citrate. CaCl2 (sold as deicer, calcium hardener for pools and sometimes is the only ingredient in moisture absorbers tubs) can be used to ensure there is no water still left in the EA.<br /> <br /> == References ==<br /> &lt;references/&gt;</div>

Trip https://wiki.dmt-nexus.me/Ethyl_Acetate_Approach_Harmala 2023-03-29T11:39:53Z

<p>Trip: /* Convert FB Harmala to Harmala Citrate for Pharmahuasca */</p> <hr /> <div>= Introduction =<br /> This Tek was inspired by Loveall's Cielo Tek, with the aim of cutting out manske steps to aid in yields and substantially quicken the process while maintaining purity. The quickest run has been 2.5hours with decent yields and purity.<br /> <br /> Thanks to everyone who has contributed or helped experiment to aid in refining/ improving this process: Loveall, Benzyme, Downwardsfromzero, _Trip_, and others.<br /> <br /> This Tek is still a work in progress&lt;ref&gt;Forum Link[https://www.dmt-nexus.me/forum/default.aspx?g=posts&amp;t=93378]&lt;/ref&gt; however lab and test results have been confirmed and are very promising for a quick Tek. Feel free to contribute. More photo's to follow soon.<br /> <br /> Please take your time with your first extraction, although this is a quick and easy Tek you don't want to rush it and make a mistake.<br /> <br /> = Safety = <br /> Review ethyl acetate&lt;ref&gt;Ethyl acetate safety[https://www.msdsonline.com/2015/04/10/ethyl-acetate-a-sweet-smelling-safety-hazard/#:~:text=Ethyl%20acetate%20is%20highly%20flammable,with%20the%20eyes%20or%20skin.]&lt;/ref&gt; and citric acid&lt;ref&gt;Citric Acid Safety[https://wiki.dmt-nexus.me/Citric_Acid_Safety#Process_.F0.9F.A5.9E]&lt;/ref&gt; safety information. Verify solvent MSDS, plastic compatibility, and clean evaporation.<br /> <br /> This TEK is food safe if food grade materials are used.<br /> <br /> <br /> Following this advice does not guarantee safety. It is up to each adult individual to make their own personal decisions.<br /> <br /> <br /> ==Consumables==<br /> *300ml water/ 600-800ml of distilled water (tap water works fine too) <br /> *25g Ca(OH)<br /> *100g of Syrian Rue seeds (B. Caapi should work too but is yet to be tested).<br /> *1lt ethyl acetate (sometimes sold as &quot;MEK substitute&quot;)<br /> *10-15g of citric acid <br /> *Sodium Carbonate<br /> *1lt Jar<br /> <br /> ==Equipment==<br /> *Blender<br /> *French press <br /> *Kitchen scale <br /> *Coffee filters, support basket, and funnel Or lab filter and vacuum pump.<br /> *1lt mason glass jars with lids<br /> *Fridge <br /> *Milligram scale <br /> *Microwave<br /> <br /> <br /> <br /> = Detailed Process =<br /> <br /> <br /> == Base Water ==<br /> -Add 300ml of water to 25g of calcium hydroxide and mix to form 'base water'.<br /> Alternatively one can use sodium carbonate (this may negate the need for filtering later). <br /> Note: Sodium Carbonate has not been fully tested start to finish.<br /> <br /> == Powder ==<br /> -Get 100g of rue seeds and grind them up, mix with 'base water'. A glass bender is quickest.<br /> <br /> == Microwave ==<br /> -Microwave the rue/base mix until close to 2/3rd's of the water content is steamed off (use kitchen scales to measure this). As a guide a 750 watt microwave at 5-7min bursts should work fine. Mix between bursts. Several bursts will be required. <br /> <br /> If interested, see further investigations for microwaving below.<br /> <br /> == Water Bath ==<br /> -Prepare a warm water bath with boiling water and warm 1lt of EA. No open flames. (This step helps yields).<br /> <br /> == Pulling ==<br /> -Place ground up 'base paste rue seed mix' in a french press. Using the french press conduct 6 pulls with the 1lt of warm EA. So 6x 160ml pulls approx (keep in mind rue seeds will absorb a little bit of EA). Carefully decant into 1lt jar(6x warm pulls at 1-2 mins each). Decant from the french press after each pull. Keep rue base mix and fresh EA in the warm water bath to improve yield (obviously in their respective containers).<br /> <br /> == Recovery/ Filter ==<br /> -Approx just over 800ml of EA should be recovered and then filtered (filtering may not be necessary if one has used sodium carbonate as a base, this is still under investigation). Lab filter is recommended, coffee filters should work too.<br /> <br /> <br /> [[File:Download.jpeg-2.jpg]] [[File:Images.jpeg-6.jpg]] ‎<br /> <br /> <br /> <br /> <br /> <br /> Recovered vs Filtered<br /> <br /> == Salting ==<br /> -Add 15g of citirc acid to the combined EA pulls (the approx 800ml of EA) and shake for 5-10mins (red/orange/yellow oil should form very fast). Orange/red goo forms at the base of the jar and the rest of the jar gets covered with sticky yellow goo (making it easy to decant). (This goo should crystalize if left for 24hours+. This is not necessary though, the goo makes decanting easy so one can decant right away).<br /> <br /> [[File:Download.jpeg-1.jpg ]] (Initial clouding when adding citric acid).<br /> <br /> [[File:Images.jpeg-10.jpg]] <br /> (Don't let the photo deceive you the whole Jar is covered in sticky yellow harmala citrate residue).<br /> <br /> == Decant &amp; Reclaim ==<br /> -Decant EA (this can be cleaned and reused next extraction). One can also add a little bit of EA to the citrate stuck to the jar to clean it up a little bit but it is not necessary. Again decant this EA.<br /> <br /> == Dissolve Goo ==<br /> -After the tiny amount of EA still left in the jar evaporates off the goo, add minimum 850ml of warm water to the citrate goo, it will dissolve fairly quickly. <br /> <br /> (One can ratio it down if using less seeds). The more water used gives a cleaner product (in appearance anyway). One can use even more water 1lt-1.5lt to achieve a whiter end result (see further investigation notes on use of too much water in this step).<br /> <br /> <br /> <br /> [[File:20220415 182000.jpg]] <br /> <br /> <br /> <br /> Above is a photo comparing the final end result, more vs less water used in this step. (1lt vs 300ml)<br /> <br /> == Base ==<br /> -Base slowly with sodium carbonate (you can shake up the jar to get excess sodium carbonate to dissolve once the acid is neutralized). Add enough sodium carbonate until the harmala starts to crash out then add a little bit more.<br /> <br /> [[File:Images.jpeg-9.jpg ]] Initial basing &amp; precipitation.<br /> <br /> == Crash/ Filter TEK Complete ==<br /> -Harmala will crash out quickly. Some of the FB harmala will float to the top, this needs to be left to cool.<br /> (Sticking the jar in a freezer '''appears''' to speed up the process and harmala crashes as it cools. The floating harmala should settle. This should not take long). <br /> <br /> [[File:Index1.jpg]] Crashing of Harmala (some will float to the top some settles to the bottom).<br /> <br /> [[File:Images.jpeg-8.jpg]] '''As a rule of thumb I wait for majority of the floating harmala to settle to the bottom'''. This rarely exceeds the 2 hour mark, again usually a lot quicker - as little as half an hour. <br /> <br /> <br /> <br /> Once it has finished crashing out filter and dry the product (lab filters or coffee filters should work fine). <br /> <br /> <br /> Well done this should have been a quick and easy run. '''3.7%+''' is usually the minimum percentage pulled on first run. The process can be repeated on spent material and re-pulled with hot EA to get over '''5%'''.<br /> Final product is usually off white almost greyish in color harmala. It doesn't necessarily represent purity in this Tek and color appears to be dependent on how much water was used during dissolving and basing step. If you <br /> look at lab sample B vs C, sample C had extra clean up steps added (and although the signals appear slightly clearer) sample C came out more of a tan color than off white/grey. <br /> If one is after a purer looking product you can do a 5% ammonia wash during the final filter before drying (this has reported to clean up harmala).<br /> <br /> [[File:Download.jpeg.jpg ‎]]<br /> <br /> <br /> No need to leave the product overnight to crash, if left for too long (say 24hrs+) some impurities appear to crash out with it. The final product in this step should crash out quick and should/ can be filtered within a hour or 2 (often quicker). <br /> Once filtered and dried you have the final product.<br /> <br /> (Keep the sodium carbonated water after filtering, more harmala may crash out overnight. It usually appears more impure by color and may contain impurities though an analysis has not been confirmed. It is likely still useable)<br /> <br /> == Lab Analysis ==<br /> [[File: A1.jpg]]<br /> <br /> Above is harmala lab analysis results.<br /> Figure A is the traditional 3x Manske, figure B &amp; C are from the EA approach (B &amp; C were conducted with slightly different variations). Figure B is the standard EA approach TEK as written above.<br /> The peaks indicate very clean harmine/harmaline. All main peaks can be attributed to harmala even 197 represent harmala with the loss -CH3 or and 169 is likely loss of -OCH3 functional groups during LC-MS. Results run in positive mode adds M 1+.<br /> <br /> == Further investigations ==<br /> -Sodium Carbonate should be usable as a base for this Tek but it's yet to be confirmed.<br /> <br /> -Chemical drying solvent after pulls only slightly changes the end result/ purity and is not necessary based of lab results..<br /> <br /> -A mini A/B at the end for clean up does not appear to change end result/ purity (it will likely make the harmala darker in appearance, reasons unknown).<br /> <br /> -Other acids are yet to be tested. Fumaric acid was briefly tested and should work. Phosphoric acid has been limitedly tested appears to behave like citric acid.<br /> <br /> -Microwave route may be unnecessary as eventually discovered with the Cielo Tek. If this is the case, water content in the first step may need to be reduced below 300ml. This may be like the Cielo Tek and require more water to facilitate efficient pulls, thus may need to be fine tuned. And like the Cielo tek may not need microwaving. However for now, those ratios and the microwave step should work fine so stick with these values and the use of a microwave.<br /> <br /> -Dissolving the goo in more water appears to give a purer looking product, using too little amount of water gives a very impure looking product. The ideal ratio is yet to be worked out. This may not affect purity to a great degree. Lab results have shown color doesn't necessarily equal purity in this tek. More water may lengthen the time needed to crash out harmala and or reduce yields. Note, this doesn't seem to be the case but further tests are needed.<br /> <br /> -This process will likely work with B. Caapi but has yet been tested but should work fine.<br /> <br /> -Butyl acetate does not appear to work effectively and harmala citrate will not crash out of BA.<br /> <br /> == Reuse ==<br /> Reusing solvents is encouraged&lt;ref&gt;On reusing non polar solvent[https://www.dmt-nexus.me/forum/default.aspx?g=posts&amp;t=31398]&lt;/ref&gt; at the DMT nexus.<br /> <br /> <br /> Wash spent extract with sodium carbonate saturated water (35% by weight). About 1/5 of the solvent volume as saturated water is enough. Shake vigorously (emulsions do not form). CO2 bubbles may be visible during citric acid neutralization. Keep an eye on any bubbles and release any pressure buildup regularly. Neutralization can be optionally verified with pH paper. Rest washed solution until clear (up to a day or more).<br /> <br /> <br /> Remove the water layer with a pipette or separatory funnel. Freezing the solvent and filtering the ice slush that forms with a metal strainer is also an option. Finally, decant off any excess solid sodium carbonate/citrate. CaCl2 (sold as deicer, calcium hardener for pools and sometimes is the only ingredient in moisture absorbers tubs) can be used to ensure there is no water still left in the EA.<br /> <br /> == References ==<br /> &lt;references/&gt;</div>

Trip https://wiki.dmt-nexus.me/Ethyl_Acetate_Approach_Harmala 2023-03-29T11:38:44Z

<p>Trip: /* Further investigations */</p> <hr /> <div>= Introduction =<br /> This Tek was inspired by Loveall's Cielo Tek, with the aim of cutting out manske steps to aid in yields and substantially quicken the process while maintaining purity. The quickest run has been 2.5hours with decent yields and purity.<br /> <br /> Thanks to everyone who has contributed or helped experiment to aid in refining/ improving this process: Loveall, Benzyme, Downwardsfromzero, _Trip_, and others.<br /> <br /> This Tek is still a work in progress&lt;ref&gt;Forum Link[https://www.dmt-nexus.me/forum/default.aspx?g=posts&amp;t=93378]&lt;/ref&gt; however lab and test results have been confirmed and are very promising for a quick Tek. Feel free to contribute. More photo's to follow soon.<br /> <br /> Please take your time with your first extraction, although this is a quick and easy Tek you don't want to rush it and make a mistake.<br /> <br /> = Safety = <br /> Review ethyl acetate&lt;ref&gt;Ethyl acetate safety[https://www.msdsonline.com/2015/04/10/ethyl-acetate-a-sweet-smelling-safety-hazard/#:~:text=Ethyl%20acetate%20is%20highly%20flammable,with%20the%20eyes%20or%20skin.]&lt;/ref&gt; and citric acid&lt;ref&gt;Citric Acid Safety[https://wiki.dmt-nexus.me/Citric_Acid_Safety#Process_.F0.9F.A5.9E]&lt;/ref&gt; safety information. Verify solvent MSDS, plastic compatibility, and clean evaporation.<br /> <br /> This TEK is food safe if food grade materials are used.<br /> <br /> <br /> Following this advice does not guarantee safety. It is up to each adult individual to make their own personal decisions.<br /> <br /> <br /> ==Consumables==<br /> *300ml water/ 600-800ml of distilled water (tap water works fine too) <br /> *25g Ca(OH)<br /> *100g of Syrian Rue seeds (B. Caapi should work too but is yet to be tested).<br /> *1lt ethyl acetate (sometimes sold as &quot;MEK substitute&quot;)<br /> *10-15g of citric acid <br /> *Sodium Carbonate<br /> *1lt Jar<br /> <br /> ==Equipment==<br /> *Blender<br /> *French press <br /> *Kitchen scale <br /> *Coffee filters, support basket, and funnel Or lab filter and vacuum pump.<br /> *1lt mason glass jars with lids<br /> *Fridge <br /> *Milligram scale <br /> *Microwave<br /> <br /> <br /> <br /> = Detailed Process =<br /> <br /> <br /> == Base Water ==<br /> -Add 300ml of water to 25g of calcium hydroxide and mix to form 'base water'.<br /> Alternatively one can use sodium carbonate (this may negate the need for filtering later). <br /> Note: Sodium Carbonate has not been fully tested start to finish.<br /> <br /> == Powder ==<br /> -Get 100g of rue seeds and grind them up, mix with 'base water'. A glass bender is quickest.<br /> <br /> == Microwave ==<br /> -Microwave the rue/base mix until close to 2/3rd's of the water content is steamed off (use kitchen scales to measure this). As a guide a 750 watt microwave at 5-7min bursts should work fine. Mix between bursts. Several bursts will be required. <br /> <br /> If interested, see further investigations for microwaving below.<br /> <br /> == Water Bath ==<br /> -Prepare a warm water bath with boiling water and warm 1lt of EA. No open flames. (This step helps yields).<br /> <br /> == Pulling ==<br /> -Place ground up 'base paste rue seed mix' in a french press. Using the french press conduct 6 pulls with the 1lt of warm EA. So 6x 160ml pulls approx (keep in mind rue seeds will absorb a little bit of EA). Carefully decant into 1lt jar(6x warm pulls at 1-2 mins each). Decant from the french press after each pull. Keep rue base mix and fresh EA in the warm water bath to improve yield (obviously in their respective containers).<br /> <br /> == Recovery/ Filter ==<br /> -Approx just over 800ml of EA should be recovered and then filtered (filtering may not be necessary if one has used sodium carbonate as a base, this is still under investigation). Lab filter is recommended, coffee filters should work too.<br /> <br /> <br /> [[File:Download.jpeg-2.jpg]] [[File:Images.jpeg-6.jpg]] ‎<br /> <br /> <br /> <br /> <br /> <br /> Recovered vs Filtered<br /> <br /> == Salting ==<br /> -Add 15g of citirc acid to the combined EA pulls (the approx 800ml of EA) and shake for 5-10mins (red/orange/yellow oil should form very fast). Orange/red goo forms at the base of the jar and the rest of the jar gets covered with sticky yellow goo (making it easy to decant). (This goo should crystalize if left for 24hours+. This is not necessary though, the goo makes decanting easy so one can decant right away).<br /> <br /> [[File:Download.jpeg-1.jpg ]] (Initial clouding when adding citric acid).<br /> <br /> [[File:Images.jpeg-10.jpg]] <br /> (Don't let the photo deceive you the whole Jar is covered in sticky yellow harmala citrate residue).<br /> <br /> == Decant &amp; Reclaim ==<br /> -Decant EA (this can be cleaned and reused next extraction). One can also add a little bit of EA to the citrate stuck to the jar to clean it up a little bit but it is not necessary. Again decant this EA.<br /> <br /> == Dissolve Goo ==<br /> -After the tiny amount of EA still left in the jar evaporates off the goo, add minimum 850ml of warm water to the citrate goo, it will dissolve fairly quickly. <br /> <br /> (One can ratio it down if using less seeds). The more water used gives a cleaner product (in appearance anyway). One can use even more water 1lt-1.5lt to achieve a whiter end result (see further investigation notes on use of too much water in this step).<br /> <br /> <br /> <br /> [[File:20220415 182000.jpg]] <br /> <br /> <br /> <br /> Above is a photo comparing the final end result, more vs less water used in this step. (1lt vs 300ml)<br /> <br /> == Base ==<br /> -Base slowly with sodium carbonate (you can shake up the jar to get excess sodium carbonate to dissolve once the acid is neutralized). Add enough sodium carbonate until the harmala starts to crash out then add a little bit more.<br /> <br /> [[File:Images.jpeg-9.jpg ]] Initial basing &amp; precipitation.<br /> <br /> == Crash/ Filter TEK Complete ==<br /> -Harmala will crash out quickly. Some of the FB harmala will float to the top, this needs to be left to cool.<br /> (Sticking the jar in a freezer '''appears''' to speed up the process and harmala crashes as it cools. The floating harmala should settle. This should not take long). <br /> <br /> [[File:Index1.jpg]] Crashing of Harmala (some will float to the top some settles to the bottom).<br /> <br /> [[File:Images.jpeg-8.jpg]] '''As a rule of thumb I wait for majority of the floating harmala to settle to the bottom'''. This rarely exceeds the 2 hour mark, again usually a lot quicker - as little as half an hour. <br /> <br /> <br /> <br /> Once it has finished crashing out filter and dry the product (lab filters or coffee filters should work fine). <br /> <br /> <br /> Well done this should have been a quick and easy run. '''3.7%+''' is usually the minimum percentage pulled on first run. The process can be repeated on spent material and re-pulled with hot EA to get over '''5%'''.<br /> Final product is usually off white almost greyish in color harmala. It doesn't necessarily represent purity in this Tek and color appears to be dependent on how much water was used during dissolving and basing step. If you <br /> look at lab sample B vs C, sample C had extra clean up steps added (and although the signals appear slightly clearer) sample C came out more of a tan color than off white/grey. <br /> If one is after a purer looking product you can do a 5% ammonia wash during the final filter before drying (this has reported to clean up harmala).<br /> <br /> [[File:Download.jpeg.jpg ‎]]<br /> <br /> <br /> No need to leave the product overnight to crash, if left for too long (say 24hrs+) some impurities appear to crash out with it. The final product in this step should crash out quick and should/ can be filtered within a hour or 2 (often quicker). <br /> Once filtered and dried you have the final product.<br /> <br /> (Keep the sodium carbonated water after filtering, more harmala may crash out overnight. It usually appears more impure by color and may contain impurities though an analysis has not been confirmed. It is likely still useable)<br /> <br /> == Convert FB Harmala to Harmala Citrate for Pharmahuasca ==<br /> Initially the citric acid crashes out a goo. However, once clean freebase (FB) Haramla is obtained one can dissolve it in hot EA (with the help of a few shakes of the jar) and then add citirc acid at about 20mg per ml of EA. This should give you nice clean yellowish harmala citrate crystals. They may be slightly sticky.<br /> <br /> 200mg FB harmala is a good dose to convert for pharmahuasca (for full MAO-inhibition).<br /> FB harmala can also be used for pharmahuasca depending on your stomachs sensitivity (however, it all gets converted to HCL in your stomach anyway). How the dose is taken varies from person to person and Nexus forums have discussed this extensively, please check the forum and or experiment to see what works for you.<br /> <br /> == Lab Analysis ==<br /> [[File: A1.jpg]]<br /> <br /> Above is harmala lab analysis results.<br /> Figure A is the traditional 3x Manske, figure B &amp; C are from the EA approach (B &amp; C were conducted with slightly different variations). Figure B is the standard EA approach TEK as written above.<br /> The peaks indicate very clean harmine/harmaline. All main peaks can be attributed to harmala even 197 represent harmala with the loss -CH3 or and 169 is likely loss of -OCH3 functional groups during LC-MS. Results run in positive mode adds M 1+.<br /> <br /> == Further investigations ==<br /> -Sodium Carbonate should be usable as a base for this Tek but it's yet to be confirmed.<br /> <br /> -Chemical drying solvent after pulls only slightly changes the end result/ purity and is not necessary based of lab results..<br /> <br /> -A mini A/B at the end for clean up does not appear to change end result/ purity (it will likely make the harmala darker in appearance, reasons unknown).<br /> <br /> -Other acids are yet to be tested. Fumaric acid was briefly tested and should work. Phosphoric acid has been limitedly tested appears to behave like citric acid.<br /> <br /> -Microwave route may be unnecessary as eventually discovered with the Cielo Tek. If this is the case, water content in the first step may need to be reduced below 300ml. This may be like the Cielo Tek and require more water to facilitate efficient pulls, thus may need to be fine tuned. And like the Cielo tek may not need microwaving. However for now, those ratios and the microwave step should work fine so stick with these values and the use of a microwave.<br /> <br /> -Dissolving the goo in more water appears to give a purer looking product, using too little amount of water gives a very impure looking product. The ideal ratio is yet to be worked out. This may not affect purity to a great degree. Lab results have shown color doesn't necessarily equal purity in this tek. More water may lengthen the time needed to crash out harmala and or reduce yields. Note, this doesn't seem to be the case but further tests are needed.<br /> <br /> -This process will likely work with B. Caapi but has yet been tested but should work fine.<br /> <br /> -Butyl acetate does not appear to work effectively and harmala citrate will not crash out of BA.<br /> <br /> == Reuse ==<br /> Reusing solvents is encouraged&lt;ref&gt;On reusing non polar solvent[https://www.dmt-nexus.me/forum/default.aspx?g=posts&amp;t=31398]&lt;/ref&gt; at the DMT nexus.<br /> <br /> <br /> Wash spent extract with sodium carbonate saturated water (35% by weight). About 1/5 of the solvent volume as saturated water is enough. Shake vigorously (emulsions do not form). CO2 bubbles may be visible during citric acid neutralization. Keep an eye on any bubbles and release any pressure buildup regularly. Neutralization can be optionally verified with pH paper. Rest washed solution until clear (up to a day or more).<br /> <br /> <br /> Remove the water layer with a pipette or separatory funnel. Freezing the solvent and filtering the ice slush that forms with a metal strainer is also an option. Finally, decant off any excess solid sodium carbonate/citrate. CaCl2 (sold as deicer, calcium hardener for pools and sometimes is the only ingredient in moisture absorbers tubs) can be used to ensure there is no water still left in the EA.<br /> <br /> == References ==<br /> &lt;references/&gt;</div>

Trip https://wiki.dmt-nexus.me/Ethyl_Acetate_Approach_Harmala 2023-03-29T11:37:46Z

<p>Trip: /* Further investigations */</p> <hr /> <div>= Introduction =<br /> This Tek was inspired by Loveall's Cielo Tek, with the aim of cutting out manske steps to aid in yields and substantially quicken the process while maintaining purity. The quickest run has been 2.5hours with decent yields and purity.<br /> <br /> Thanks to everyone who has contributed or helped experiment to aid in refining/ improving this process: Loveall, Benzyme, Downwardsfromzero, _Trip_, and others.<br /> <br /> This Tek is still a work in progress&lt;ref&gt;Forum Link[https://www.dmt-nexus.me/forum/default.aspx?g=posts&amp;t=93378]&lt;/ref&gt; however lab and test results have been confirmed and are very promising for a quick Tek. Feel free to contribute. More photo's to follow soon.<br /> <br /> Please take your time with your first extraction, although this is a quick and easy Tek you don't want to rush it and make a mistake.<br /> <br /> = Safety = <br /> Review ethyl acetate&lt;ref&gt;Ethyl acetate safety[https://www.msdsonline.com/2015/04/10/ethyl-acetate-a-sweet-smelling-safety-hazard/#:~:text=Ethyl%20acetate%20is%20highly%20flammable,with%20the%20eyes%20or%20skin.]&lt;/ref&gt; and citric acid&lt;ref&gt;Citric Acid Safety[https://wiki.dmt-nexus.me/Citric_Acid_Safety#Process_.F0.9F.A5.9E]&lt;/ref&gt; safety information. Verify solvent MSDS, plastic compatibility, and clean evaporation.<br /> <br /> This TEK is food safe if food grade materials are used.<br /> <br /> <br /> Following this advice does not guarantee safety. It is up to each adult individual to make their own personal decisions.<br /> <br /> <br /> ==Consumables==<br /> *300ml water/ 600-800ml of distilled water (tap water works fine too) <br /> *25g Ca(OH)<br /> *100g of Syrian Rue seeds (B. Caapi should work too but is yet to be tested).<br /> *1lt ethyl acetate (sometimes sold as &quot;MEK substitute&quot;)<br /> *10-15g of citric acid <br /> *Sodium Carbonate<br /> *1lt Jar<br /> <br /> ==Equipment==<br /> *Blender<br /> *French press <br /> *Kitchen scale <br /> *Coffee filters, support basket, and funnel Or lab filter and vacuum pump.<br /> *1lt mason glass jars with lids<br /> *Fridge <br /> *Milligram scale <br /> *Microwave<br /> <br /> <br /> <br /> = Detailed Process =<br /> <br /> <br /> == Base Water ==<br /> -Add 300ml of water to 25g of calcium hydroxide and mix to form 'base water'.<br /> Alternatively one can use sodium carbonate (this may negate the need for filtering later). <br /> Note: Sodium Carbonate has not been fully tested start to finish.<br /> <br /> == Powder ==<br /> -Get 100g of rue seeds and grind them up, mix with 'base water'. A glass bender is quickest.<br /> <br /> == Microwave ==<br /> -Microwave the rue/base mix until close to 2/3rd's of the water content is steamed off (use kitchen scales to measure this). As a guide a 750 watt microwave at 5-7min bursts should work fine. Mix between bursts. Several bursts will be required. <br /> <br /> If interested, see further investigations for microwaving below.<br /> <br /> == Water Bath ==<br /> -Prepare a warm water bath with boiling water and warm 1lt of EA. No open flames. (This step helps yields).<br /> <br /> == Pulling ==<br /> -Place ground up 'base paste rue seed mix' in a french press. Using the french press conduct 6 pulls with the 1lt of warm EA. So 6x 160ml pulls approx (keep in mind rue seeds will absorb a little bit of EA). Carefully decant into 1lt jar(6x warm pulls at 1-2 mins each). Decant from the french press after each pull. Keep rue base mix and fresh EA in the warm water bath to improve yield (obviously in their respective containers).<br /> <br /> == Recovery/ Filter ==<br /> -Approx just over 800ml of EA should be recovered and then filtered (filtering may not be necessary if one has used sodium carbonate as a base, this is still under investigation). Lab filter is recommended, coffee filters should work too.<br /> <br /> <br /> [[File:Download.jpeg-2.jpg]] [[File:Images.jpeg-6.jpg]] ‎<br /> <br /> <br /> <br /> <br /> <br /> Recovered vs Filtered<br /> <br /> == Salting ==<br /> -Add 15g of citirc acid to the combined EA pulls (the approx 800ml of EA) and shake for 5-10mins (red/orange/yellow oil should form very fast). Orange/red goo forms at the base of the jar and the rest of the jar gets covered with sticky yellow goo (making it easy to decant). (This goo should crystalize if left for 24hours+. This is not necessary though, the goo makes decanting easy so one can decant right away).<br /> <br /> [[File:Download.jpeg-1.jpg ]] (Initial clouding when adding citric acid).<br /> <br /> [[File:Images.jpeg-10.jpg]] <br /> (Don't let the photo deceive you the whole Jar is covered in sticky yellow harmala citrate residue).<br /> <br /> == Decant &amp; Reclaim ==<br /> -Decant EA (this can be cleaned and reused next extraction). One can also add a little bit of EA to the citrate stuck to the jar to clean it up a little bit but it is not necessary. Again decant this EA.<br /> <br /> == Dissolve Goo ==<br /> -After the tiny amount of EA still left in the jar evaporates off the goo, add minimum 850ml of warm water to the citrate goo, it will dissolve fairly quickly. <br /> <br /> (One can ratio it down if using less seeds). The more water used gives a cleaner product (in appearance anyway). One can use even more water 1lt-1.5lt to achieve a whiter end result (see further investigation notes on use of too much water in this step).<br /> <br /> <br /> <br /> [[File:20220415 182000.jpg]] <br /> <br /> <br /> <br /> Above is a photo comparing the final end result, more vs less water used in this step. (1lt vs 300ml)<br /> <br /> == Base ==<br /> -Base slowly with sodium carbonate (you can shake up the jar to get excess sodium carbonate to dissolve once the acid is neutralized). Add enough sodium carbonate until the harmala starts to crash out then add a little bit more.<br /> <br /> [[File:Images.jpeg-9.jpg ]] Initial basing &amp; precipitation.<br /> <br /> == Crash/ Filter TEK Complete ==<br /> -Harmala will crash out quickly. Some of the FB harmala will float to the top, this needs to be left to cool.<br /> (Sticking the jar in a freezer '''appears''' to speed up the process and harmala crashes as it cools. The floating harmala should settle. This should not take long). <br /> <br /> [[File:Index1.jpg]] Crashing of Harmala (some will float to the top some settles to the bottom).<br /> <br /> [[File:Images.jpeg-8.jpg]] '''As a rule of thumb I wait for majority of the floating harmala to settle to the bottom'''. This rarely exceeds the 2 hour mark, again usually a lot quicker - as little as half an hour. <br /> <br /> <br /> <br /> Once it has finished crashing out filter and dry the product (lab filters or coffee filters should work fine). <br /> <br /> <br /> Well done this should have been a quick and easy run. '''3.7%+''' is usually the minimum percentage pulled on first run. The process can be repeated on spent material and re-pulled with hot EA to get over '''5%'''.<br /> Final product is usually off white almost greyish in color harmala. It doesn't necessarily represent purity in this Tek and color appears to be dependent on how much water was used during dissolving and basing step. If you <br /> look at lab sample B vs C, sample C had extra clean up steps added (and although the signals appear slightly clearer) sample C came out more of a tan color than off white/grey. <br /> If one is after a purer looking product you can do a 5% ammonia wash during the final filter before drying (this has reported to clean up harmala).<br /> <br /> [[File:Download.jpeg.jpg ‎]]<br /> <br /> <br /> No need to leave the product overnight to crash, if left for too long (say 24hrs+) some impurities appear to crash out with it. The final product in this step should crash out quick and should/ can be filtered within a hour or 2 (often quicker). <br /> Once filtered and dried you have the final product.<br /> <br /> (Keep the sodium carbonated water after filtering, more harmala may crash out overnight. It usually appears more impure by color and may contain impurities though an analysis has not been confirmed. It is likely still useable)<br /> <br /> == Convert FB Harmala to Harmala Citrate for Pharmahuasca ==<br /> Initially the citric acid crashes out a goo. However, once clean freebase (FB) Haramla is obtained one can dissolve it in hot EA (with the help of a few shakes of the jar) and then add citirc acid at about 20mg per ml of EA. This should give you nice clean yellowish harmala citrate crystals. They may be slightly sticky.<br /> <br /> 200mg FB harmala is a good dose to convert for pharmahuasca (for full MAO-inhibition).<br /> FB harmala can also be used for pharmahuasca depending on your stomachs sensitivity (however, it all gets converted to HCL in your stomach anyway). How the dose is taken varies from person to person and Nexus forums have discussed this extensively, please check the forum and or experiment to see what works for you.<br /> <br /> == Lab Analysis ==<br /> [[File: A1.jpg]]<br /> <br /> Above is harmala lab analysis results.<br /> Figure A is the traditional 3x Manske, figure B &amp; C are from the EA approach (B &amp; C were conducted with slightly different variations). Figure B is the standard EA approach TEK as written above.<br /> The peaks indicate very clean harmine/harmaline. All main peaks can be attributed to harmala even 197 represent harmala with the loss -CH3 or and 169 is likely loss of -OCH3 functional groups during LC-MS. Results run in positive mode adds M 1+.<br /> <br /> == Further investigations ==<br /> -Sodium Carbonate should be usable as a base for this Tek but it's yet to be confirmed.<br /> <br /> -Chemical drying solvent after pulls only slightly changes the end result/ purity and is not necessary based of lab results..<br /> <br /> -A mini A/B at the end for clean up does not appear to change end result/ purity (it will likely make the harmala darker in appearance, reasons unknown).<br /> <br /> -Other acids are yet to be tested. Fumaric acid was briefly tested and should work. Phosphoric acid has been limitedly tested appears to behave like citric acid.<br /> <br /> -Microwave route may be unnecessary as eventually discovered with the Cielo Tek. If this is the case, water content in the first step may need to be reduced below 300ml. This may be like the Cielo Tek and require more water to facilitate efficient pulls, thus may need to be fine tuned. And like the Cielo tek may not need microwaving. However for now, those ratios and the microwave step should work fine so stick with these values and the use of a microwave.<br /> <br /> -Dissolving the goo in more water appears to give a purer looking product, using too little amount of water gives a very impure looking product. The ideal ratio is yet to be worked out. This may not affect purity to a great degree. Lab results have shown color doesn't necessarily equal purity in this tek. More water may lengthen the time needed to crash out harmala and or reduce yields. Note, this doesn't seem to be the case but further tests are needed.<br /> <br /> -This process will likely work with B. Caapi but has yet been tested.<br /> <br /> -Butyl acetate does not appear to work effectively and harmala citrate will not crash out of BA.<br /> <br /> == Reuse ==<br /> Reusing solvents is encouraged&lt;ref&gt;On reusing non polar solvent[https://www.dmt-nexus.me/forum/default.aspx?g=posts&amp;t=31398]&lt;/ref&gt; at the DMT nexus.<br /> <br /> <br /> Wash spent extract with sodium carbonate saturated water (35% by weight). About 1/5 of the solvent volume as saturated water is enough. Shake vigorously (emulsions do not form). CO2 bubbles may be visible during citric acid neutralization. Keep an eye on any bubbles and release any pressure buildup regularly. Neutralization can be optionally verified with pH paper. Rest washed solution until clear (up to a day or more).<br /> <br /> <br /> Remove the water layer with a pipette or separatory funnel. Freezing the solvent and filtering the ice slush that forms with a metal strainer is also an option. Finally, decant off any excess solid sodium carbonate/citrate. CaCl2 (sold as deicer, calcium hardener for pools and sometimes is the only ingredient in moisture absorbers tubs) can be used to ensure there is no water still left in the EA.<br /> <br /> == References ==<br /> &lt;references/&gt;</div>

Trip https://wiki.dmt-nexus.me/Ethyl_Acetate_Approach_Harmala 2023-03-29T11:37:11Z

<p>Trip: /* Further investigations */</p> <hr /> <div>= Introduction =<br /> This Tek was inspired by Loveall's Cielo Tek, with the aim of cutting out manske steps to aid in yields and substantially quicken the process while maintaining purity. The quickest run has been 2.5hours with decent yields and purity.<br /> <br /> Thanks to everyone who has contributed or helped experiment to aid in refining/ improving this process: Loveall, Benzyme, Downwardsfromzero, _Trip_, and others.<br /> <br /> This Tek is still a work in progress&lt;ref&gt;Forum Link[https://www.dmt-nexus.me/forum/default.aspx?g=posts&amp;t=93378]&lt;/ref&gt; however lab and test results have been confirmed and are very promising for a quick Tek. Feel free to contribute. More photo's to follow soon.<br /> <br /> Please take your time with your first extraction, although this is a quick and easy Tek you don't want to rush it and make a mistake.<br /> <br /> = Safety = <br /> Review ethyl acetate&lt;ref&gt;Ethyl acetate safety[https://www.msdsonline.com/2015/04/10/ethyl-acetate-a-sweet-smelling-safety-hazard/#:~:text=Ethyl%20acetate%20is%20highly%20flammable,with%20the%20eyes%20or%20skin.]&lt;/ref&gt; and citric acid&lt;ref&gt;Citric Acid Safety[https://wiki.dmt-nexus.me/Citric_Acid_Safety#Process_.F0.9F.A5.9E]&lt;/ref&gt; safety information. Verify solvent MSDS, plastic compatibility, and clean evaporation.<br /> <br /> This TEK is food safe if food grade materials are used.<br /> <br /> <br /> Following this advice does not guarantee safety. It is up to each adult individual to make their own personal decisions.<br /> <br /> <br /> ==Consumables==<br /> *300ml water/ 600-800ml of distilled water (tap water works fine too) <br /> *25g Ca(OH)<br /> *100g of Syrian Rue seeds (B. Caapi should work too but is yet to be tested).<br /> *1lt ethyl acetate (sometimes sold as &quot;MEK substitute&quot;)<br /> *10-15g of citric acid <br /> *Sodium Carbonate<br /> *1lt Jar<br /> <br /> ==Equipment==<br /> *Blender<br /> *French press <br /> *Kitchen scale <br /> *Coffee filters, support basket, and funnel Or lab filter and vacuum pump.<br /> *1lt mason glass jars with lids<br /> *Fridge <br /> *Milligram scale <br /> *Microwave<br /> <br /> <br /> <br /> = Detailed Process =<br /> <br /> <br /> == Base Water ==<br /> -Add 300ml of water to 25g of calcium hydroxide and mix to form 'base water'.<br /> Alternatively one can use sodium carbonate (this may negate the need for filtering later). <br /> Note: Sodium Carbonate has not been fully tested start to finish.<br /> <br /> == Powder ==<br /> -Get 100g of rue seeds and grind them up, mix with 'base water'. A glass bender is quickest.<br /> <br /> == Microwave ==<br /> -Microwave the rue/base mix until close to 2/3rd's of the water content is steamed off (use kitchen scales to measure this). As a guide a 750 watt microwave at 5-7min bursts should work fine. Mix between bursts. Several bursts will be required. <br /> <br /> If interested, see further investigations for microwaving below.<br /> <br /> == Water Bath ==<br /> -Prepare a warm water bath with boiling water and warm 1lt of EA. No open flames. (This step helps yields).<br /> <br /> == Pulling ==<br /> -Place ground up 'base paste rue seed mix' in a french press. Using the french press conduct 6 pulls with the 1lt of warm EA. So 6x 160ml pulls approx (keep in mind rue seeds will absorb a little bit of EA). Carefully decant into 1lt jar(6x warm pulls at 1-2 mins each). Decant from the french press after each pull. Keep rue base mix and fresh EA in the warm water bath to improve yield (obviously in their respective containers).<br /> <br /> == Recovery/ Filter ==<br /> -Approx just over 800ml of EA should be recovered and then filtered (filtering may not be necessary if one has used sodium carbonate as a base, this is still under investigation). Lab filter is recommended, coffee filters should work too.<br /> <br /> <br /> [[File:Download.jpeg-2.jpg]] [[File:Images.jpeg-6.jpg]] ‎<br /> <br /> <br /> <br /> <br /> <br /> Recovered vs Filtered<br /> <br /> == Salting ==<br /> -Add 15g of citirc acid to the combined EA pulls (the approx 800ml of EA) and shake for 5-10mins (red/orange/yellow oil should form very fast). Orange/red goo forms at the base of the jar and the rest of the jar gets covered with sticky yellow goo (making it easy to decant). (This goo should crystalize if left for 24hours+. This is not necessary though, the goo makes decanting easy so one can decant right away).<br /> <br /> [[File:Download.jpeg-1.jpg ]] (Initial clouding when adding citric acid).<br /> <br /> [[File:Images.jpeg-10.jpg]] <br /> (Don't let the photo deceive you the whole Jar is covered in sticky yellow harmala citrate residue).<br /> <br /> == Decant &amp; Reclaim ==<br /> -Decant EA (this can be cleaned and reused next extraction). One can also add a little bit of EA to the citrate stuck to the jar to clean it up a little bit but it is not necessary. Again decant this EA.<br /> <br /> == Dissolve Goo ==<br /> -After the tiny amount of EA still left in the jar evaporates off the goo, add minimum 850ml of warm water to the citrate goo, it will dissolve fairly quickly. <br /> <br /> (One can ratio it down if using less seeds). The more water used gives a cleaner product (in appearance anyway). One can use even more water 1lt-1.5lt to achieve a whiter end result (see further investigation notes on use of too much water in this step).<br /> <br /> <br /> <br /> [[File:20220415 182000.jpg]] <br /> <br /> <br /> <br /> Above is a photo comparing the final end result, more vs less water used in this step. (1lt vs 300ml)<br /> <br /> == Base ==<br /> -Base slowly with sodium carbonate (you can shake up the jar to get excess sodium carbonate to dissolve once the acid is neutralized). Add enough sodium carbonate until the harmala starts to crash out then add a little bit more.<br /> <br /> [[File:Images.jpeg-9.jpg ]] Initial basing &amp; precipitation.<br /> <br /> == Crash/ Filter TEK Complete ==<br /> -Harmala will crash out quickly. Some of the FB harmala will float to the top, this needs to be left to cool.<br /> (Sticking the jar in a freezer '''appears''' to speed up the process and harmala crashes as it cools. The floating harmala should settle. This should not take long). <br /> <br /> [[File:Index1.jpg]] Crashing of Harmala (some will float to the top some settles to the bottom).<br /> <br /> [[File:Images.jpeg-8.jpg]] '''As a rule of thumb I wait for majority of the floating harmala to settle to the bottom'''. This rarely exceeds the 2 hour mark, again usually a lot quicker - as little as half an hour. <br /> <br /> <br /> <br /> Once it has finished crashing out filter and dry the product (lab filters or coffee filters should work fine). <br /> <br /> <br /> Well done this should have been a quick and easy run. '''3.7%+''' is usually the minimum percentage pulled on first run. The process can be repeated on spent material and re-pulled with hot EA to get over '''5%'''.<br /> Final product is usually off white almost greyish in color harmala. It doesn't necessarily represent purity in this Tek and color appears to be dependent on how much water was used during dissolving and basing step. If you <br /> look at lab sample B vs C, sample C had extra clean up steps added (and although the signals appear slightly clearer) sample C came out more of a tan color than off white/grey. <br /> If one is after a purer looking product you can do a 5% ammonia wash during the final filter before drying (this has reported to clean up harmala).<br /> <br /> [[File:Download.jpeg.jpg ‎]]<br /> <br /> <br /> No need to leave the product overnight to crash, if left for too long (say 24hrs+) some impurities appear to crash out with it. The final product in this step should crash out quick and should/ can be filtered within a hour or 2 (often quicker). <br /> Once filtered and dried you have the final product.<br /> <br /> (Keep the sodium carbonated water after filtering, more harmala may crash out overnight. It usually appears more impure by color and may contain impurities though an analysis has not been confirmed. It is likely still useable)<br /> <br /> == Convert FB Harmala to Harmala Citrate for Pharmahuasca ==<br /> Initially the citric acid crashes out a goo. However, once clean freebase (FB) Haramla is obtained one can dissolve it in hot EA (with the help of a few shakes of the jar) and then add citirc acid at about 20mg per ml of EA. This should give you nice clean yellowish harmala citrate crystals. They may be slightly sticky.<br /> <br /> 200mg FB harmala is a good dose to convert for pharmahuasca (for full MAO-inhibition).<br /> FB harmala can also be used for pharmahuasca depending on your stomachs sensitivity (however, it all gets converted to HCL in your stomach anyway). How the dose is taken varies from person to person and Nexus forums have discussed this extensively, please check the forum and or experiment to see what works for you.<br /> <br /> == Lab Analysis ==<br /> [[File: A1.jpg]]<br /> <br /> Above is harmala lab analysis results.<br /> Figure A is the traditional 3x Manske, figure B &amp; C are from the EA approach (B &amp; C were conducted with slightly different variations). Figure B is the standard EA approach TEK as written above.<br /> The peaks indicate very clean harmine/harmaline. All main peaks can be attributed to harmala even 197 represent harmala with the loss -CH3 or and 169 is likely loss of -OCH3 functional groups during LC-MS. Results run in positive mode adds M 1+.<br /> <br /> == Further investigations ==<br /> -Sodium Carbonate should be usable as a base for this Tek but it's yet to be confirmed.<br /> <br /> -Chemical drying solvent after pulls only slightly changes the end result/ purity and is not necessary based of lab results..<br /> <br /> -A mini A/B at the end for clean up does not appear to change end result/ purity (it will likely make the harmala darker in appearance, reasons unknown).<br /> <br /> -Other acids are yet to be tested. Fumaric acid was briefly tested and should work. Phosphoric acid has been limitedly tested appears to behave like citric acid.<br /> <br /> -Microwave route may be unnecessary as eventually discovered with the Cielo Tek. If this is the case, water content in the first step may need to be reduced below 300ml. This may be like the Cielo Tek and require more water to facilitate efficient pulls, thus may need to be fine tuned. And like the Cielo tek may not need microwaving. However for now, those ratios and the microwave step should work fine so stick with these values and the use of a microwave.<br /> <br /> -Dissolving the goo in more water appears to give a purer looking product, using too little amount of water gives a very impure looking product. The ideal ratio is yet to be worked out. This may not affect purity to a great degree. Lab results have shown color doesn't necessarily equal purity in this tek. More water may lengthen the time needed to crash out harmala and or reduce yields. Note, this doesn't seem to be the case but further tests are needed.<br /> <br /> -This process will likely work with B. Caapi but has yet been tested.<br /> <br /> -Butyl acetate does not appear to work.<br /> <br /> == Reuse ==<br /> Reusing solvents is encouraged&lt;ref&gt;On reusing non polar solvent[https://www.dmt-nexus.me/forum/default.aspx?g=posts&amp;t=31398]&lt;/ref&gt; at the DMT nexus.<br /> <br /> <br /> Wash spent extract with sodium carbonate saturated water (35% by weight). About 1/5 of the solvent volume as saturated water is enough. Shake vigorously (emulsions do not form). CO2 bubbles may be visible during citric acid neutralization. Keep an eye on any bubbles and release any pressure buildup regularly. Neutralization can be optionally verified with pH paper. Rest washed solution until clear (up to a day or more).<br /> <br /> <br /> Remove the water layer with a pipette or separatory funnel. Freezing the solvent and filtering the ice slush that forms with a metal strainer is also an option. Finally, decant off any excess solid sodium carbonate/citrate. CaCl2 (sold as deicer, calcium hardener for pools and sometimes is the only ingredient in moisture absorbers tubs) can be used to ensure there is no water still left in the EA.<br /> <br /> == References ==<br /> &lt;references/&gt;</div>

Trip https://wiki.dmt-nexus.me/DMT-Nexus_Wiki:THH_Reduction 2023-03-29T11:30:00Z

<p>Trip: /* Bases */</p> <hr /> <div><br /> <br /> = THH Zinc Reduction =<br /> <br /> ==Introduction==<br /> Purpose of this conversion Tek is to convert harmaline to THH via zinc reduction. Using zinc to react with vinegar, hydrogen atoms form and are donated to the harmaline to form Tetrahydroharmine.<br /> <br /> ==Consumables==<br /> -10g Harmaline<br /> <br /> -400ml of Vinegar<br /> <br /> -10g Zinc (metal) Dust or 4g of Fine Magnesium Ribbon (zinc is strongly reccommended over magnesium)<br /> <br /> -10% Ammonia<br /> <br /> -Coffee or lab filters<br /> <br /> -Stirring utensil (strongly suggest a magnetic stirrer)<br /> <br /> ==Detailed Process==<br /> -Using a glass receptacle, place 10g of Harmaline in 400ml of vinegar stir until dissolved.<br /> <br /> -Add 10g of Zinc dust (or magnesium ribbon) leave on magnetic stirrer until the zinc/ magnesium reaction has completed and no more hydrogen bubbles are forming (this will take a number of hours). 6hours minimum for the zinc, magnesium may be shorter depending on the thickness. Note the magnesium will give a clearer hydrogen reaction.<br /> <br /> -Using a coffee filter, filter out any left over zinc/ magnesium metal. Note lab filters will likely be required if using zinc as it is very fine (cotton balls/ funnel combination has been reported to work too).<br /> <br /> -Add ammonia to the vinegar solution until a PH of 9.5. Tetrahydroharmine should crash out of the solution.<br /> <br /> -Filter and dry the THH.<br /> <br /> ==Alternative==<br /> Fine Magnesium ribbon can be used in the place of zinc dust. Zinc is generally considered a better option for conversion but will take longer.<br /> This method is less tested and may not render a complete conversion.<br /> <br /> ==Bases==<br /> Other bases like sodium carbonate will form other salts that can be hard to separate. When using ammonia, amonnia salts formed will stay in the solution. So stick with ammonia.<br /> <br /> ==Confirmation of THH conversion==<br /> <br /> Using Marquis reagent THH should form a green color reaction. After 5-10mins the reaction will turn to brown.<br /> <br /> [[File:Marquis_harmala.jpeg]]<br /> <br /> Harmaline Vs THH. Photo courtesy of Merkin<br /> <br /> ==Future concepts (untested)==<br /> <br /> [[File:4685 2b0909e8-9501-4209-b338-55bbad14ba59 harmaline oxidoreduction.jpg]]<br /> <br /> Harmaline reduction could be possible via ascorbic acid or hydrogen peroxide reactions. Graphics courtesy of Downwardsfromzero.</div>

Trip https://wiki.dmt-nexus.me/DMT-Nexus_Wiki:THH_Reduction 2023-03-29T11:27:46Z

<p>Trip: /* Consumables */</p> <hr /> <div><br /> <br /> = THH Zinc Reduction =<br /> <br /> ==Introduction==<br /> Purpose of this conversion Tek is to convert harmaline to THH via zinc reduction. Using zinc to react with vinegar, hydrogen atoms form and are donated to the harmaline to form Tetrahydroharmine.<br /> <br /> ==Consumables==<br /> -10g Harmaline<br /> <br /> -400ml of Vinegar<br /> <br /> -10g Zinc (metal) Dust or 4g of Fine Magnesium Ribbon (zinc is strongly reccommended over magnesium)<br /> <br /> -10% Ammonia<br /> <br /> -Coffee or lab filters<br /> <br /> -Stirring utensil (strongly suggest a magnetic stirrer)<br /> <br /> ==Detailed Process==<br /> -Using a glass receptacle, place 10g of Harmaline in 400ml of vinegar stir until dissolved.<br /> <br /> -Add 10g of Zinc dust (or magnesium ribbon) leave on magnetic stirrer until the zinc/ magnesium reaction has completed and no more hydrogen bubbles are forming (this will take a number of hours). 6hours minimum for the zinc, magnesium may be shorter depending on the thickness. Note the magnesium will give a clearer hydrogen reaction.<br /> <br /> -Using a coffee filter, filter out any left over zinc/ magnesium metal. Note lab filters will likely be required if using zinc as it is very fine (cotton balls/ funnel combination has been reported to work too).<br /> <br /> -Add ammonia to the vinegar solution until a PH of 9.5. Tetrahydroharmine should crash out of the solution.<br /> <br /> -Filter and dry the THH.<br /> <br /> ==Alternative==<br /> Fine Magnesium ribbon can be used in the place of zinc dust. Zinc is generally considered a better option for conversion but will take longer.<br /> This method is less tested and may not render a complete conversion.<br /> <br /> ==Bases==<br /> Other bases like sodium carbonate will form other salts that can be hard to separate. When using ammonia, amonnia salts formed will stay in the solution.<br /> <br /> ==Confirmation of THH conversion==<br /> <br /> Using Marquis reagent THH should form a green color reaction. After 5-10mins the reaction will turn to brown.<br /> <br /> [[File:Marquis_harmala.jpeg]]<br /> <br /> Harmaline Vs THH. Photo courtesy of Merkin<br /> <br /> ==Future concepts (untested)==<br /> <br /> [[File:4685 2b0909e8-9501-4209-b338-55bbad14ba59 harmaline oxidoreduction.jpg]]<br /> <br /> Harmaline reduction could be possible via ascorbic acid or hydrogen peroxide reactions. Graphics courtesy of Downwardsfromzero.</div>

Trip https://wiki.dmt-nexus.me/DMT-Nexus_Wiki:THH_Reduction 2023-03-29T11:27:06Z

<p>Trip: /* Alternative */</p> <hr /> <div><br /> <br /> = THH Zinc Reduction =<br /> <br /> ==Introduction==<br /> Purpose of this conversion Tek is to convert harmaline to THH via zinc reduction. Using zinc to react with vinegar, hydrogen atoms form and are donated to the harmaline to form Tetrahydroharmine.<br /> <br /> ==Consumables==<br /> -10g Harmaline<br /> <br /> -400ml of Vinegar<br /> <br /> -10g Zinc (metal) Dust or 4g of Fine Magnesium Ribbon<br /> <br /> -10% Ammonia<br /> <br /> -Coffee or lab filters<br /> <br /> -Stirring utensil (strongly suggest a magnetic stirrer)<br /> <br /> ==Detailed Process==<br /> -Using a glass receptacle, place 10g of Harmaline in 400ml of vinegar stir until dissolved.<br /> <br /> -Add 10g of Zinc dust (or magnesium ribbon) leave on magnetic stirrer until the zinc/ magnesium reaction has completed and no more hydrogen bubbles are forming (this will take a number of hours). 6hours minimum for the zinc, magnesium may be shorter depending on the thickness. Note the magnesium will give a clearer hydrogen reaction.<br /> <br /> -Using a coffee filter, filter out any left over zinc/ magnesium metal. Note lab filters will likely be required if using zinc as it is very fine (cotton balls/ funnel combination has been reported to work too).<br /> <br /> -Add ammonia to the vinegar solution until a PH of 9.5. Tetrahydroharmine should crash out of the solution.<br /> <br /> -Filter and dry the THH.<br /> <br /> ==Alternative==<br /> Fine Magnesium ribbon can be used in the place of zinc dust. Zinc is generally considered a better option for conversion but will take longer.<br /> This method is less tested and may not render a complete conversion.<br /> <br /> ==Bases==<br /> Other bases like sodium carbonate will form other salts that can be hard to separate. When using ammonia, amonnia salts formed will stay in the solution.<br /> <br /> ==Confirmation of THH conversion==<br /> <br /> Using Marquis reagent THH should form a green color reaction. After 5-10mins the reaction will turn to brown.<br /> <br /> [[File:Marquis_harmala.jpeg]]<br /> <br /> Harmaline Vs THH. Photo courtesy of Merkin<br /> <br /> ==Future concepts (untested)==<br /> <br /> [[File:4685 2b0909e8-9501-4209-b338-55bbad14ba59 harmaline oxidoreduction.jpg]]<br /> <br /> Harmaline reduction could be possible via ascorbic acid or hydrogen peroxide reactions. Graphics courtesy of Downwardsfromzero.</div>

Trip https://wiki.dmt-nexus.me/DMT-Nexus_Wiki:THH_Reduction 2023-03-29T11:25:00Z

<p>Trip: /* Alternative */</p> <hr /> <div><br /> <br /> = THH Zinc Reduction =<br /> <br /> ==Introduction==<br /> Purpose of this conversion Tek is to convert harmaline to THH via zinc reduction. Using zinc to react with vinegar, hydrogen atoms form and are donated to the harmaline to form Tetrahydroharmine.<br /> <br /> ==Consumables==<br /> -10g Harmaline<br /> <br /> -400ml of Vinegar<br /> <br /> -10g Zinc (metal) Dust or 4g of Fine Magnesium Ribbon<br /> <br /> -10% Ammonia<br /> <br /> -Coffee or lab filters<br /> <br /> -Stirring utensil (strongly suggest a magnetic stirrer)<br /> <br /> ==Detailed Process==<br /> -Using a glass receptacle, place 10g of Harmaline in 400ml of vinegar stir until dissolved.<br /> <br /> -Add 10g of Zinc dust (or magnesium ribbon) leave on magnetic stirrer until the zinc/ magnesium reaction has completed and no more hydrogen bubbles are forming (this will take a number of hours). 6hours minimum for the zinc, magnesium may be shorter depending on the thickness. Note the magnesium will give a clearer hydrogen reaction.<br /> <br /> -Using a coffee filter, filter out any left over zinc/ magnesium metal. Note lab filters will likely be required if using zinc as it is very fine (cotton balls/ funnel combination has been reported to work too).<br /> <br /> -Add ammonia to the vinegar solution until a PH of 9.5. Tetrahydroharmine should crash out of the solution.<br /> <br /> -Filter and dry the THH.<br /> <br /> ==Alternative==<br /> Fine Magnesium ribbon can be used in the place of zinc dust. Zinc is generally considered a better option for conversion but will take longer.<br /> <br /> ==Bases==<br /> Other bases like sodium carbonate will form other salts that can be hard to separate. When using ammonia, amonnia salts formed will stay in the solution.<br /> <br /> ==Confirmation of THH conversion==<br /> <br /> Using Marquis reagent THH should form a green color reaction. After 5-10mins the reaction will turn to brown.<br /> <br /> [[File:Marquis_harmala.jpeg]]<br /> <br /> Harmaline Vs THH. Photo courtesy of Merkin<br /> <br /> ==Future concepts (untested)==<br /> <br /> [[File:4685 2b0909e8-9501-4209-b338-55bbad14ba59 harmaline oxidoreduction.jpg]]<br /> <br /> Harmaline reduction could be possible via ascorbic acid or hydrogen peroxide reactions. Graphics courtesy of Downwardsfromzero.</div>

Trip https://wiki.dmt-nexus.me/DMT-Nexus_Wiki:THH_Reduction 2023-03-29T11:17:33Z

<p>Trip: /* Confirmation of THH conversion */</p> <hr /> <div><br /> <br /> = THH Zinc Reduction =<br /> <br /> ==Introduction==<br /> Purpose of this conversion Tek is to convert harmaline to THH via zinc reduction. Using zinc to react with vinegar, hydrogen atoms form and are donated to the harmaline to form Tetrahydroharmine.<br /> <br /> ==Consumables==<br /> -10g Harmaline<br /> <br /> -400ml of Vinegar<br /> <br /> -10g Zinc (metal) Dust or 4g of Fine Magnesium Ribbon<br /> <br /> -10% Ammonia<br /> <br /> -Coffee or lab filters<br /> <br /> -Stirring utensil (strongly suggest a magnetic stirrer)<br /> <br /> ==Detailed Process==<br /> -Using a glass receptacle, place 10g of Harmaline in 400ml of vinegar stir until dissolved.<br /> <br /> -Add 10g of Zinc dust (or magnesium ribbon) leave on magnetic stirrer until the zinc/ magnesium reaction has completed and no more hydrogen bubbles are forming (this will take a number of hours). 6hours minimum for the zinc, magnesium may be shorter depending on the thickness. Note the magnesium will give a clearer hydrogen reaction.<br /> <br /> -Using a coffee filter, filter out any left over zinc/ magnesium metal. Note lab filters will likely be required if using zinc as it is very fine (cotton balls/ funnel combination has been reported to work too).<br /> <br /> -Add ammonia to the vinegar solution until a PH of 9.5. Tetrahydroharmine should crash out of the solution.<br /> <br /> -Filter and dry the THH.<br /> <br /> ==Alternative==<br /> Fine Magnesium ribbon can be used in the place of zinc dust. Zinc is generally considered a better option for conversion but will take longer.<br /> <br /> ==Confirmation of THH conversion==<br /> <br /> Using Marquis reagent THH should form a green color reaction. After 5-10mins the reaction will turn to brown.<br /> <br /> [[File:Marquis_harmala.jpeg]]<br /> <br /> Harmaline Vs THH. Photo courtesy of Merkin<br /> <br /> ==Future concepts (untested)==<br /> <br /> [[File:4685 2b0909e8-9501-4209-b338-55bbad14ba59 harmaline oxidoreduction.jpg]]<br /> <br /> Harmaline reduction could be possible via ascorbic acid or hydrogen peroxide reactions. Graphics courtesy of Downwardsfromzero.</div>

Trip https://wiki.dmt-nexus.me/DMT-Nexus_Wiki:THH_Reduction 2023-03-29T01:03:54Z

<p>Trip: /* Detailed Process */</p> <hr /> <div><br /> <br /> = THH Zinc Reduction =<br /> <br /> ==Introduction==<br /> Purpose of this conversion Tek is to convert harmaline to THH via zinc reduction. Using zinc to react with vinegar, hydrogen atoms form and are donated to the harmaline to form Tetrahydroharmine.<br /> <br /> ==Consumables==<br /> -10g Harmaline<br /> <br /> -400ml of Vinegar<br /> <br /> -10g Zinc (metal) Dust or 4g of Fine Magnesium Ribbon<br /> <br /> -10% Ammonia<br /> <br /> -Coffee or lab filters<br /> <br /> -Stirring utensil (strongly suggest a magnetic stirrer)<br /> <br /> ==Detailed Process==<br /> -Using a glass receptacle, place 10g of Harmaline in 400ml of vinegar stir until dissolved.<br /> <br /> -Add 10g of Zinc dust (or magnesium ribbon) leave on magnetic stirrer until the zinc/ magnesium reaction has completed and no more hydrogen bubbles are forming (this will take a number of hours). 6hours minimum for the zinc, magnesium may be shorter depending on the thickness. Note the magnesium will give a clearer hydrogen reaction.<br /> <br /> -Using a coffee filter, filter out any left over zinc/ magnesium metal. Note lab filters will likely be required if using zinc as it is very fine (cotton balls/ funnel combination has been reported to work too).<br /> <br /> -Add ammonia to the vinegar solution until a PH of 9.5. Tetrahydroharmine should crash out of the solution.<br /> <br /> -Filter and dry the THH.<br /> <br /> ==Alternative==<br /> Fine Magnesium ribbon can be used in the place of zinc dust. Zinc is generally considered a better option for conversion but will take longer.<br /> <br /> ==Confirmation of THH conversion==<br /> <br /> Using Marquis reagent THH should form a green color reaction.<br /> <br /> [[File:Marquis_harmala.jpeg]]<br /> <br /> Harmaline Vs THH. Photo courtesy of Merkin<br /> <br /> <br /> ==Future concepts (untested)==<br /> <br /> [[File:4685 2b0909e8-9501-4209-b338-55bbad14ba59 harmaline oxidoreduction.jpg]]<br /> <br /> Harmaline reduction could be possible via ascorbic acid or hydrogen peroxide reactions. Graphics courtesy of Downwardsfromzero.</div>

Trip https://wiki.dmt-nexus.me/DMT-Nexus_Wiki:THH_Reduction 2023-03-29T01:02:29Z

<p>Trip: /* Detailed Process */</p> <hr /> <div><br /> <br /> = THH Zinc Reduction =<br /> <br /> ==Introduction==<br /> Purpose of this conversion Tek is to convert harmaline to THH via zinc reduction. Using zinc to react with vinegar, hydrogen atoms form and are donated to the harmaline to form Tetrahydroharmine.<br /> <br /> ==Consumables==<br /> -10g Harmaline<br /> <br /> -400ml of Vinegar<br /> <br /> -10g Zinc (metal) Dust or 4g of Fine Magnesium Ribbon<br /> <br /> -10% Ammonia<br /> <br /> -Coffee or lab filters<br /> <br /> -Stirring utensil (strongly suggest a magnetic stirrer)<br /> <br /> ==Detailed Process==<br /> -Using a glass receptacle, place 10g of Harmaline in 400ml of vinegar stir until dissolved.<br /> <br /> -Add 10g of Zinc dust (or magnesium ribbon) leave on magnetic stirrer until the zinc/ magnesium reaction has completed and no more hydrogen bubbles are forming (this will take a number of hours). 6hours minimum for the zinc, magnesium may be shorter depending on the thickness. Note the magnesium will give a clearer hydrogen reaction.<br /> <br /> -Using a coffee filter, filter out any left over zinc/ magnesium metal. Note lab filters will likely be required of using zinc as it is very fine (cotton balls/ funnel combination has been reported to work too).<br /> <br /> -Add ammonia to the vinegar solution until a PH of 9.5. Tetrahydroharmine should crash out of the solution.<br /> <br /> -Filter and dry the THH.<br /> <br /> ==Alternative==<br /> Fine Magnesium ribbon can be used in the place of zinc dust. Zinc is generally considered a better option for conversion but will take longer.<br /> <br /> ==Confirmation of THH conversion==<br /> <br /> Using Marquis reagent THH should form a green color reaction.<br /> <br /> [[File:Marquis_harmala.jpeg]]<br /> <br /> Harmaline Vs THH. Photo courtesy of Merkin<br /> <br /> <br /> ==Future concepts (untested)==<br /> <br /> [[File:4685 2b0909e8-9501-4209-b338-55bbad14ba59 harmaline oxidoreduction.jpg]]<br /> <br /> Harmaline reduction could be possible via ascorbic acid or hydrogen peroxide reactions. Graphics courtesy of Downwardsfromzero.</div>

Trip https://wiki.dmt-nexus.me/DMT-Nexus_Wiki:THH_Reduction 2023-03-29T00:53:56Z

<p>Trip: /* Detailed Process */</p> <hr /> <div><br /> <br /> = THH Zinc Reduction =<br /> <br /> ==Introduction==<br /> Purpose of this conversion Tek is to convert harmaline to THH via zinc reduction. Using zinc to react with vinegar, hydrogen atoms form and are donated to the harmaline to form Tetrahydroharmine.<br /> <br /> ==Consumables==<br /> -10g Harmaline<br /> <br /> -400ml of Vinegar<br /> <br /> -10g Zinc (metal) Dust or 4g of Fine Magnesium Ribbon<br /> <br /> -10% Ammonia<br /> <br /> -Coffee or lab filters<br /> <br /> -Stirring utensil (strongly suggest a magnetic stirrer)<br /> <br /> ==Detailed Process==<br /> -Using a glass receptacle, place 10g of Harmaline in 400ml of vinegar stir until dissolved.<br /> <br /> -Add 10g of Zinc dust (or magnesium ribbon) leave on magnetic stirrer until the zinc/ magnesium reaction has completed and no more hydrogen bubbles are forming (this will take a number of hours). 6hours minimum for the zinc, magnesium may be shorter depending on the thickness. Note the magnesium will give a clearer hydrogen reaction.<br /> <br /> -Using a coffee filter, filter out any left over zinc metal.<br /> <br /> -Add ammonia to the vinegar solution until a PH of 9.5. Tetrahydroharmine should crash out of the solution.<br /> <br /> -Filter and dry the THH.<br /> <br /> ==Alternative==<br /> Fine Magnesium ribbon can be used in the place of zinc dust. Zinc is generally considered a better option for conversion but will take longer.<br /> <br /> ==Confirmation of THH conversion==<br /> <br /> Using Marquis reagent THH should form a green color reaction.<br /> <br /> [[File:Marquis_harmala.jpeg]]<br /> <br /> Harmaline Vs THH. Photo courtesy of Merkin<br /> <br /> <br /> ==Future concepts (untested)==<br /> <br /> [[File:4685 2b0909e8-9501-4209-b338-55bbad14ba59 harmaline oxidoreduction.jpg]]<br /> <br /> Harmaline reduction could be possible via ascorbic acid or hydrogen peroxide reactions. Graphics courtesy of Downwardsfromzero.</div>

Trip https://wiki.dmt-nexus.me/DMT-Nexus_Wiki:THH_Reduction 2023-03-29T00:53:18Z

<p>Trip: /* Detailed Process */</p> <hr /> <div><br /> <br /> = THH Zinc Reduction =<br /> <br /> ==Introduction==<br /> Purpose of this conversion Tek is to convert harmaline to THH via zinc reduction. Using zinc to react with vinegar, hydrogen atoms form and are donated to the harmaline to form Tetrahydroharmine.<br /> <br /> ==Consumables==<br /> -10g Harmaline<br /> <br /> -400ml of Vinegar<br /> <br /> -10g Zinc (metal) Dust or 4g of Fine Magnesium Ribbon<br /> <br /> -10% Ammonia<br /> <br /> -Coffee or lab filters<br /> <br /> -Stirring utensil (strongly suggest a magnetic stirrer)<br /> <br /> ==Detailed Process==<br /> -Using a glass receptacle, place 10g of Harmaline in 400ml of vinegar stir until dissolved.<br /> <br /> -Add 10g of Zinc dust (or magnesium ribbon) leave on magnetic stirrer until the zinc/ magnesium reaction has completed and no more hydrogen bubbles are forming (this will take a number of hours). 6hours minimum for the zinc, magnesium may be shorter depending on the thickness.<br /> <br /> -Using a coffee filter, filter out any left over zinc metal.<br /> <br /> -Add ammonia to the vinegar solution until a PH of 9.5. Tetrahydroharmine should crash out of the solution.<br /> <br /> -Filter and dry the THH.<br /> <br /> ==Alternative==<br /> Fine Magnesium ribbon can be used in the place of zinc dust. Zinc is generally considered a better option for conversion but will take longer.<br /> <br /> ==Confirmation of THH conversion==<br /> <br /> Using Marquis reagent THH should form a green color reaction.<br /> <br /> [[File:Marquis_harmala.jpeg]]<br /> <br /> Harmaline Vs THH. Photo courtesy of Merkin<br /> <br /> <br /> ==Future concepts (untested)==<br /> <br /> [[File:4685 2b0909e8-9501-4209-b338-55bbad14ba59 harmaline oxidoreduction.jpg]]<br /> <br /> Harmaline reduction could be possible via ascorbic acid or hydrogen peroxide reactions. Graphics courtesy of Downwardsfromzero.</div>

Trip https://wiki.dmt-nexus.me/DMT-Nexus_Wiki:THH_Reduction 2023-03-29T00:52:09Z

<p>Trip: /* Alternative */</p> <hr /> <div><br /> <br /> = THH Zinc Reduction =<br /> <br /> ==Introduction==<br /> Purpose of this conversion Tek is to convert harmaline to THH via zinc reduction. Using zinc to react with vinegar, hydrogen atoms form and are donated to the harmaline to form Tetrahydroharmine.<br /> <br /> ==Consumables==<br /> -10g Harmaline<br /> <br /> -400ml of Vinegar<br /> <br /> -10g Zinc (metal) Dust or 4g of Fine Magnesium Ribbon<br /> <br /> -10% Ammonia<br /> <br /> -Coffee or lab filters<br /> <br /> -Stirring utensil (strongly suggest a magnetic stirrer)<br /> <br /> ==Detailed Process==<br /> -Using a glass receptacle, place 10g of Harmaline in 400ml of vinegar stir until dissolved.<br /> <br /> -Add 4g of Zinc dust leave on magnetic stirrer until the zinc reaction has completed and no more hydrogen bubbles are forming (this will take a number of hours).<br /> <br /> -Using a coffee filter, filter out any left over zinc metal.<br /> <br /> -Add ammonia to the vinegar solution until a PH of 9.5. Tetrahydroharmine should crash out of the solution.<br /> <br /> -Filter and dry the THH.<br /> <br /> ==Alternative==<br /> Fine Magnesium ribbon can be used in the place of zinc dust. Zinc is generally considered a better option for conversion but will take longer.<br /> <br /> ==Confirmation of THH conversion==<br /> <br /> Using Marquis reagent THH should form a green color reaction.<br /> <br /> [[File:Marquis_harmala.jpeg]]<br /> <br /> Harmaline Vs THH. Photo courtesy of Merkin<br /> <br /> <br /> ==Future concepts (untested)==<br /> <br /> [[File:4685 2b0909e8-9501-4209-b338-55bbad14ba59 harmaline oxidoreduction.jpg]]<br /> <br /> Harmaline reduction could be possible via ascorbic acid or hydrogen peroxide reactions. Graphics courtesy of Downwardsfromzero.</div>

Trip https://wiki.dmt-nexus.me/DMT-Nexus_Wiki:THH_Reduction 2023-03-29T00:51:34Z

<p>Trip: /* Consumables */</p> <hr /> <div><br /> <br /> = THH Zinc Reduction =<br /> <br /> ==Introduction==<br /> Purpose of this conversion Tek is to convert harmaline to THH via zinc reduction. Using zinc to react with vinegar, hydrogen atoms form and are donated to the harmaline to form Tetrahydroharmine.<br /> <br /> ==Consumables==<br /> -10g Harmaline<br /> <br /> -400ml of Vinegar<br /> <br /> -10g Zinc (metal) Dust or 4g of Fine Magnesium Ribbon<br /> <br /> -10% Ammonia<br /> <br /> -Coffee or lab filters<br /> <br /> -Stirring utensil (strongly suggest a magnetic stirrer)<br /> <br /> ==Detailed Process==<br /> -Using a glass receptacle, place 10g of Harmaline in 400ml of vinegar stir until dissolved.<br /> <br /> -Add 4g of Zinc dust leave on magnetic stirrer until the zinc reaction has completed and no more hydrogen bubbles are forming (this will take a number of hours).<br /> <br /> -Using a coffee filter, filter out any left over zinc metal.<br /> <br /> -Add ammonia to the vinegar solution until a PH of 9.5. Tetrahydroharmine should crash out of the solution.<br /> <br /> -Filter and dry the THH.<br /> <br /> ==Alternative==<br /> Fine Magnesium ribbon can be used in the place of zinc dust<br /> <br /> ==Confirmation of THH conversion==<br /> <br /> Using Marquis reagent THH should form a green color reaction.<br /> <br /> [[File:Marquis_harmala.jpeg]]<br /> <br /> Harmaline Vs THH. Photo courtesy of Merkin<br /> <br /> <br /> ==Future concepts (untested)==<br /> <br /> [[File:4685 2b0909e8-9501-4209-b338-55bbad14ba59 harmaline oxidoreduction.jpg]]<br /> <br /> Harmaline reduction could be possible via ascorbic acid or hydrogen peroxide reactions. Graphics courtesy of Downwardsfromzero.</div>

Trip https://wiki.dmt-nexus.me/DMT-Nexus_Wiki:THH_Reduction 2023-02-18T07:19:07Z

<p>Trip: </p> <hr /> <div><br /> <br /> = THH Zinc Reduction =<br /> <br /> ==Introduction==<br /> Purpose of this conversion Tek is to convert harmaline to THH via zinc reduction. Using zinc to react with vinegar, hydrogen atoms form and are donated to the harmaline to form Tetrahydroharmine.<br /> <br /> ==Consumables==<br /> -10g Harmaline<br /> <br /> -400ml of Vinegar<br /> <br /> -4g Zinc (metal) Dust<br /> <br /> -10% Ammonia<br /> <br /> -Coffee or lab filters<br /> <br /> -Stirring utensil (strongly suggest a magnetic stirrer)<br /> <br /> ==Detailed Process==<br /> -Using a glass receptacle, place 10g of Harmaline in 400ml of vinegar stir until dissolved.<br /> <br /> -Add 4g of Zinc dust leave on magnetic stirrer until the zinc reaction has completed and no more hydrogen bubbles are forming (this will take a number of hours).<br /> <br /> -Using a coffee filter, filter out any left over zinc metal.<br /> <br /> -Add ammonia to the vinegar solution until a PH of 9.5. Tetrahydroharmine should crash out of the solution.<br /> <br /> -Filter and dry the THH.<br /> <br /> ==Alternative==<br /> Fine Magnesium ribbon can be used in the place of zinc dust<br /> <br /> ==Confirmation of THH conversion==<br /> <br /> Using Marquis reagent THH should form a green color reaction.<br /> <br /> [[File:Marquis_harmala.jpeg]]<br /> <br /> Harmaline Vs THH. Photo courtesy of Merkin<br /> <br /> <br /> ==Future concepts (untested)==<br /> <br /> [[File:4685 2b0909e8-9501-4209-b338-55bbad14ba59 harmaline oxidoreduction.jpg]]<br /> <br /> Harmaline reduction could be possible via ascorbic acid or hydrogen peroxide reactions. Graphics courtesy of Downwardsfromzero.</div>

Trip https://wiki.dmt-nexus.me/Category:Extraction_Tek 2023-02-12T08:27:57Z

<p>Trip: /* Dry Tek */</p> <hr /> <div>An Extraction Tek is a manual to extract certain chemicals from a given source.<br /> <br /> To learn more about extractions in general and how they work, check the [http://wiki.dmt-nexus.me/FAQ#Where_to_start.3F FAQ], the [http://wiki.dmt-nexus.me/DMT_Extraction_Overview extraction overview], as well as read a few different teks, even if you don't plan on doing them, because many of them explain the processes and why each step is done.<br /> <br /> One does not need to be a chemist to perform an extraction. Don't worry about not understanding everything at first. Keep reading, inform yourself, take safety precautions, don't throw anything away before you're done with your extraction and don't consume anything you are not sure its clean.<br /> <br /> {{Main Page/Portal|[[Image:Information.png]]|'''[[:Category:Extraction_Tek|Extraction Teks]]'''|<br /> &lt;table&gt;<br /> &lt;tr&gt;<br /> &lt;td&gt;<br /> <br /> &lt;/td&gt;<br /> &lt;/tr&gt;<br /> &lt;/table&gt;<br /> }}<br /> <br /> ==DMT==<br /> ===A/B===<br /> <br /> * [[Lextek]]<br /> * [[Marsofold's tek]]<br /> * [[Shaggy's Jungle Tek]]<br /> * [[The DMT Handbook]]<br /> * [[Vovin's tek]]<br /> * [[ACRB Tek By Thick-Light]]<br /> * [https://www.dmt-nexus.me/forum/default.aspx?g=posts&amp;t=58064 ACRB TEK 100g &quot;PICS&quot; (Newbie Friendly)]<br /> * [[The Wanderer's Tek]]<br /> * [https://wiki.dmt-nexus.me/User_talk:Justamessenger SP's ACRB Extraction Tek]<br /> <br /> ===STB===<br /> <br /> * [[Jorkest's D-Limonene and Fumaric Acid Approach]]<br /> * [[Lazyman's tek]]<br /> * [[Noman's tek]]<br /> * [[STC - Dream Weaver's tek]]<br /> <br /> ===STB-A/B hybrid===<br /> <br /> * [[BLAB_-_The_Big_Leisurely_AB|BLAB]]<br /> * [[PanoraMIX European AB]]<br /> * [[Nontoxic_limonene_tek|SyZyGyPSy's Nontoxic Limomene Tek]]<br /> * [[Cyb's Hybrid ATB 'Salt' Tek]]<br /> * [https://www.dmt-nexus.me/forum/default.aspx?g=posts&amp;m=459391#post459391 Cyb's MAX ION Tek]<br /> <br /> ===Dry tek===<br /> <br /> * [[Amor fati's Nontoxic Approach to Spice Extraction]]<br /> * [[Q21Q21's Vinegar/Lime A/B Extraction Tek]]<br /> * [[HIELO]]<br /> <br /> ==MESCALINE==<br /> <br /> ===A/B===<br /> <br /> * [[Kash's A/B Mescaline Extraction]]<br /> <br /> ===STB===<br /> <br /> * [[LucidLemonade's sunflower oil mescaline extraction]]<br /> <br /> ===Crude extract===<br /> <br /> * [[House's cacti preparation tek]]<br /> <br /> ===Dry tek===<br /> <br /> * [[69ron's D-Limonene Mescaline Extraction]]<br /> * [[CIELO]]<br /> <br /> ==BUFOTENINE==<br /> <br /> ===Dry tek===<br /> <br /> * [[Jorkest's D-Limonene Bufotenine Extraction]]<br /> * [[http://www.dmt-nexus.me/forum/default.aspx?g=posts&amp;t=10071 No smell bufo extraction]]<br /> * [[BW's Bufotenine Dry Tek]]<br /> <br /> ===IPA extract===<br /> <br /> * [[Bufotenine IPA Extraction and Bufojam Changa Tek]]<br /> <br /> ==HARMALAS==<br /> <br /> ===A/B===<br /> <br /> * [[Harmalas Extraction and Separation Guide]]<br /> * [[EASY Harmaloid Freebase TEK]]<br /> * [[Easy Caapi Vine Alkaloid Extraction Guide]]<br /> * [[Enoons Cold Caapi Tek]]<br /> * [[The Tao of Rue Extraction]]<br /> <br /> ===Crude Manske (salt) Extract===<br /> <br /> * [[Harmine Crystals from Syrian Rue]]<br /> <br /> ===Dry Tek===<br /> * [[Ethyl Acetate Approach Harmala]]<br /> <br /> ==LSA==<br /> <br /> ===IPA extract===<br /> <br /> * [[PanoraMIX HBWR Extract]]<br /> <br /> ===Acetone extract===<br /> <br /> * [[Kash's Advanced LSA Extraction]]<br /> <br /> ==SALVIA==<br /> <br /> ===Acetone extract===<br /> <br /> * [[PanoraMIX salvia extact]]<br /> * [[Chilled Acetone with IPA and Naphtha re-X]]<br /> <br /> [[Category:Tek]]<br /> <br /> ==Conversion teks==<br /> <br /> [[DMT Fumarate to DMT Freebase]].<br /> <br /> [[THH_reduction]]</div>

Trip https://wiki.dmt-nexus.me/Ethyl_Acetate_Approach_Harmala 2023-02-12T08:26:58Z

<p>Trip: Trip moved page DMT-Nexus Wiki:Ethyl Acetate Approach Harmala to Ethyl Acetate Approach Harmala</p> <hr /> <div>= Introduction =<br /> This Tek was inspired by Loveall's Cielo Tek, with the aim of cutting out manske steps to aid in yields and substantially quicken the process while maintaining purity. The quickest run has been 2.5hours with decent yields and purity.<br /> <br /> Thanks to everyone who has contributed or helped experiment to aid in refining/ improving this process: Loveall, Benzyme, Downwardsfromzero, _Trip_, and others.<br /> <br /> This Tek is still a work in progress&lt;ref&gt;Forum Link[https://www.dmt-nexus.me/forum/default.aspx?g=posts&amp;t=93378]&lt;/ref&gt; however lab and test results have been confirmed and are very promising for a quick Tek. Feel free to contribute. More photo's to follow soon.<br /> <br /> Please take your time with your first extraction, although this is a quick and easy Tek you don't want to rush it and make a mistake.<br /> <br /> = Safety = <br /> Review ethyl acetate&lt;ref&gt;Ethyl acetate safety[https://www.msdsonline.com/2015/04/10/ethyl-acetate-a-sweet-smelling-safety-hazard/#:~:text=Ethyl%20acetate%20is%20highly%20flammable,with%20the%20eyes%20or%20skin.]&lt;/ref&gt; and citric acid&lt;ref&gt;Citric Acid Safety[https://wiki.dmt-nexus.me/Citric_Acid_Safety#Process_.F0.9F.A5.9E]&lt;/ref&gt; safety information. Verify solvent MSDS, plastic compatibility, and clean evaporation.<br /> <br /> This TEK is food safe if food grade materials are used.<br /> <br /> <br /> Following this advice does not guarantee safety. It is up to each adult individual to make their own personal decisions.<br /> <br /> <br /> ==Consumables==<br /> *300ml water/ 600-800ml of distilled water (tap water works fine too) <br /> *25g Ca(OH)<br /> *100g of Syrian Rue seeds (B. Caapi should work too but is yet to be tested).<br /> *1lt ethyl acetate (sometimes sold as &quot;MEK substitute&quot;)<br /> *10-15g of citric acid <br /> *Sodium Carbonate<br /> *1lt Jar<br /> <br /> ==Equipment==<br /> *Blender<br /> *French press <br /> *Kitchen scale <br /> *Coffee filters, support basket, and funnel Or lab filter and vacuum pump.<br /> *1lt mason glass jars with lids<br /> *Fridge <br /> *Milligram scale <br /> *Microwave<br /> <br /> <br /> <br /> = Detailed Process =<br /> <br /> <br /> == Base Water ==<br /> -Add 300ml of water to 25g of calcium hydroxide and mix to form 'base water'.<br /> Alternatively one can use sodium carbonate (this may negate the need for filtering later). <br /> Note: Sodium Carbonate has not been fully tested start to finish.<br /> <br /> == Powder ==<br /> -Get 100g of rue seeds and grind them up, mix with 'base water'. A glass bender is quickest.<br /> <br /> == Microwave ==<br /> -Microwave the rue/base mix until close to 2/3rd's of the water content is steamed off (use kitchen scales to measure this). As a guide a 750 watt microwave at 5-7min bursts should work fine. Mix between bursts. Several bursts will be required. <br /> <br /> If interested, see further investigations for microwaving below.<br /> <br /> == Water Bath ==<br /> -Prepare a warm water bath with boiling water and warm 1lt of EA. No open flames. (This step helps yields).<br /> <br /> == Pulling ==<br /> -Place ground up 'base paste rue seed mix' in a french press. Using the french press conduct 6 pulls with the 1lt of warm EA. So 6x 160ml pulls approx (keep in mind rue seeds will absorb a little bit of EA). Carefully decant into 1lt jar(6x warm pulls at 1-2 mins each). Decant from the french press after each pull. Keep rue base mix and fresh EA in the warm water bath to improve yield (obviously in their respective containers).<br /> <br /> == Recovery/ Filter ==<br /> -Approx just over 800ml of EA should be recovered and then filtered (filtering may not be necessary if one has used sodium carbonate as a base, this is still under investigation). Lab filter is recommended, coffee filters should work too.<br /> <br /> <br /> [[File:Download.jpeg-2.jpg]] [[File:Images.jpeg-6.jpg]] ‎<br /> <br /> <br /> <br /> <br /> <br /> Recovered vs Filtered<br /> <br /> == Salting ==<br /> -Add 15g of citirc acid to the combined EA pulls (the approx 800ml of EA) and shake for 5-10mins (red/orange/yellow oil should form very fast). Orange/red goo forms at the base of the jar and the rest of the jar gets covered with sticky yellow goo (making it easy to decant). (This goo should crystalize if left for 24hours+. This is not necessary though, the goo makes decanting easy so one can decant right away).<br /> <br /> [[File:Download.jpeg-1.jpg ]] (Initial clouding when adding citric acid).<br /> <br /> [[File:Images.jpeg-10.jpg]] <br /> (Don't let the photo deceive you the whole Jar is covered in sticky yellow harmala citrate residue).<br /> <br /> == Decant &amp; Reclaim ==<br /> -Decant EA (this can be cleaned and reused next extraction). One can also add a little bit of EA to the citrate stuck to the jar to clean it up a little bit but it is not necessary. Again decant this EA.<br /> <br /> == Dissolve Goo ==<br /> -After the tiny amount of EA still left in the jar evaporates off the goo, add minimum 850ml of warm water to the citrate goo, it will dissolve fairly quickly. <br /> <br /> (One can ratio it down if using less seeds). The more water used gives a cleaner product (in appearance anyway). One can use even more water 1lt-1.5lt to achieve a whiter end result (see further investigation notes on use of too much water in this step).<br /> <br /> <br /> <br /> [[File:20220415 182000.jpg]] <br /> <br /> <br /> <br /> Above is a photo comparing the final end result, more vs less water used in this step. (1lt vs 300ml)<br /> <br /> == Base ==<br /> -Base slowly with sodium carbonate (you can shake up the jar to get excess sodium carbonate to dissolve once the acid is neutralized). Add enough sodium carbonate until the harmala starts to crash out then add a little bit more.<br /> <br /> [[File:Images.jpeg-9.jpg ]] Initial basing &amp; precipitation.<br /> <br /> == Crash/ Filter TEK Complete ==<br /> -Harmala will crash out quickly. Some of the FB harmala will float to the top, this needs to be left to cool.<br /> (Sticking the jar in a freezer '''appears''' to speed up the process and harmala crashes as it cools. The floating harmala should settle. This should not take long). <br /> <br /> [[File:Index1.jpg]] Crashing of Harmala (some will float to the top some settles to the bottom).<br /> <br /> [[File:Images.jpeg-8.jpg]] '''As a rule of thumb I wait for majority of the floating harmala to settle to the bottom'''. This rarely exceeds the 2 hour mark, again usually a lot quicker - as little as half an hour. <br /> <br /> <br /> <br /> Once it has finished crashing out filter and dry the product (lab filters or coffee filters should work fine). <br /> <br /> <br /> Well done this should have been a quick and easy run. '''3.7%+''' is usually the minimum percentage pulled on first run. The process can be repeated on spent material and re-pulled with hot EA to get over '''5%'''.<br /> Final product is usually off white almost greyish in color harmala. It doesn't necessarily represent purity in this Tek and color appears to be dependent on how much water was used during dissolving and basing step. If you <br /> look at lab sample B vs C, sample C had extra clean up steps added (and although the signals appear slightly clearer) sample C came out more of a tan color than off white/grey. <br /> If one is after a purer looking product you can do a 5% ammonia wash during the final filter before drying (this has reported to clean up harmala).<br /> <br /> [[File:Download.jpeg.jpg ‎]]<br /> <br /> <br /> No need to leave the product overnight to crash, if left for too long (say 24hrs+) some impurities appear to crash out with it. The final product in this step should crash out quick and should/ can be filtered within a hour or 2 (often quicker). <br /> Once filtered and dried you have the final product.<br /> <br /> (Keep the sodium carbonated water after filtering, more harmala may crash out overnight. It usually appears more impure by color and may contain impurities though an analysis has not been confirmed. It is likely still useable)<br /> <br /> == Convert FB Harmala to Harmala Citrate for Pharmahuasca ==<br /> Initially the citric acid crashes out a goo. However, once clean freebase (FB) Haramla is obtained one can dissolve it in hot EA (with the help of a few shakes of the jar) and then add citirc acid at about 20mg per ml of EA. This should give you nice clean yellowish harmala citrate crystals. They may be slightly sticky.<br /> <br /> 200mg FB harmala is a good dose to convert for pharmahuasca (for full MAO-inhibition).<br /> FB harmala can also be used for pharmahuasca depending on your stomachs sensitivity (however, it all gets converted to HCL in your stomach anyway). How the dose is taken varies from person to person and Nexus forums have discussed this extensively, please check the forum and or experiment to see what works for you.<br /> <br /> == Lab Analysis ==<br /> [[File: A1.jpg]]<br /> <br /> Above is harmala lab analysis results.<br /> Figure A is the traditional 3x Manske, figure B &amp; C are from the EA approach (B &amp; C were conducted with slightly different variations). Figure B is the standard EA approach TEK as written above.<br /> The peaks indicate very clean harmine/harmaline. All main peaks can be attributed to harmala even 197 represent harmala with the loss -CH3 or and 169 is likely loss of -OCH3 functional groups during LC-MS. Results run in positive mode adds M 1+.<br /> <br /> == Further investigations ==<br /> -Sodium Carbonate should be usable as a base for this Tek but it's yet to be confirmed.<br /> <br /> -Chemical drying solvent after pulls only slightly changes the end result/ purity and is not necessary based of lab results..<br /> <br /> -A mini A/B at the end for clean up does not appear to change end result/ purity (it will likely make the harmala darker in appearance, reasons unknown).<br /> <br /> -Other acids are yet to be tested. Fumaric acid was briefly tested and should work. Phosphoric acid has been limitedly tested appears to behave like citric acid.<br /> <br /> -Microwave route may be unnecessary as eventually discovered with the Cielo Tek. If this is the case, water content in the first step may need to be reduced below 300ml. This may be like the Cielo Tek and require more water to facilitate efficient pulls, thus may need to be fine tuned. And like the Cielo tek may not need microwaving. However for now, those ratios and the microwave step should work fine so stick with these values and the use of a microwave.<br /> <br /> -Dissolving the goo in more water appears to give a purer looking product, using too little amount of water gives a very impure looking product. The ideal ratio is yet to be worked out. This may not affect purity to a great degree. Lab results have shown color doesn't necessarily equal purity in this tek. More water may lengthen the time needed to crash out harmala and or reduce yields. Note, this doesn't seem to be the case but further tests are needed.<br /> <br /> -This process will likely work with B. Caapi but has yet been tested.<br /> <br /> -Butyl acetate is currently being tested as an alternative to EA.<br /> <br /> == Reuse ==<br /> Reusing solvents is encouraged&lt;ref&gt;On reusing non polar solvent[https://www.dmt-nexus.me/forum/default.aspx?g=posts&amp;t=31398]&lt;/ref&gt; at the DMT nexus.<br /> <br /> <br /> Wash spent extract with sodium carbonate saturated water (35% by weight). About 1/5 of the solvent volume as saturated water is enough. Shake vigorously (emulsions do not form). CO2 bubbles may be visible during citric acid neutralization. Keep an eye on any bubbles and release any pressure buildup regularly. Neutralization can be optionally verified with pH paper. Rest washed solution until clear (up to a day or more).<br /> <br /> <br /> Remove the water layer with a pipette or separatory funnel. Freezing the solvent and filtering the ice slush that forms with a metal strainer is also an option. Finally, decant off any excess solid sodium carbonate/citrate. CaCl2 (sold as deicer, calcium hardener for pools and sometimes is the only ingredient in moisture absorbers tubs) can be used to ensure there is no water still left in the EA.<br /> <br /> == References ==<br /> &lt;references/&gt;</div>

Trip https://wiki.dmt-nexus.me/DMT-Nexus_Wiki:Ethyl_Acetate_Approach_Harmala 2023-02-12T08:26:58Z

<p>Trip: Trip moved page DMT-Nexus Wiki:Ethyl Acetate Approach Harmala to Ethyl Acetate Approach Harmala</p> <hr /> <div>#REDIRECT [[Ethyl Acetate Approach Harmala]]</div>

Trip https://wiki.dmt-nexus.me/DMT-Nexus_Wiki:EA 2023-02-12T08:26:12Z

<p>Trip: Trip moved page DMT-Nexus Wiki:EA to EA</p> <hr /> <div>#REDIRECT [[EA]]</div>

Trip