The Nexian DMT Handbook

2010-01-12T17:16:54Z

Narmz:

{{ShowInfo|[[Image:Exclamation.png]]||This handbook propounds to illuminate all manner of DMT practice for informational purposes and for implementation '''only where it is legal to do so'''. That being said, DMT's production and use should not be condoned or endorsed where it is illegal to do so. Even where it is legal to do so, the operator must proceed with caution and in adherence to local laws, as '''many of the chemicals required for production can be hazardous to health or otherwise dangerous.'''}}

{{ShowInfo|[[Image:Note_error.png]]|'''Note:'''|This page is a work in progress -- its content throughout is not yet complete.}}

The production and use of '''DMT (N,N-Dimethyltryptamine)''', otherwise known as '''"Spice"''', is a practice that resonates strongly with the complementary qualities of ancient shamanic and alchemical spiritual practice as well as contemporary DIY (Do It Yourself) ethic. The production of spice is a discipline unlike that of most other commonly manufactured drugs, as it is not as well suited for bulk-production nor production for the purpose of sale as most well-known and intensively manufactured substances. As such, its use is generally inseparable from its production in practice and in spirit.

The production of DMT most commonly entails its extraction from botanical sources and only very rarely entails its synthesis. In this way, its production still strongly resembles its more ancient preparations by manner of brewing, a simple form of aqueous extraction still commonly performed to this day. This is the simplest and most readily administered form of extract if used as a component of a harmaloid-based preparation or -huasca brew.

----

Please take the time to seek further elaboration at the following resources:
: [http://www.dmt-nexus.com/ The DMT-Nexus]
: [http://deoxy.org/dmt.htm deoxy.org/dmt]
: [http://www.erowid.org/chemicals/dmt/ Erowid's DMT Vault]
: [http://en.wikipedia.org/wiki/Dimethyltryptamine Wikipedia's Article on DMT]

=='''Source Selection'''==
[[Image:DMT.png|thumb]]
DMT, its analogues, and other related alkaloids can be found in a wide variety of lifeforms, varying from trace amounts to considerable amounts. It is impossible, therefore, to include all of the sources from which DMT can be extracted, so the following discussion will focus primarily on the most commonly used and significant botanical sources.

==='''Botanical Considerations'''===

Several species of plants contain a variety of constituents apart from DMT. This consideration is of the utmost importance when selecting the source plant from which an extraction is to be performed, as it may become the determining factor in the material requirements of the extraction process. Some plants may even contain toxic alkaloids, so thorough research must be conducted prior to selection, extraction, and administration.

====='''Common Botanical Sources'''=====

{{:Mimosa hostilis}}

{{:Diplopterys cabrerana}}

{{:Psychotria viridis}}

See also:
:[[DMT Containing Plants]]
:[http://dmt-nexus.com/forum/default.aspx?g=posts&t=1123 Plants that Contain DMT forum topic]

====='''Methods of Refinery'''=====

Before extracting alkaloids from the variety of plants named above, one generally needs to clean and prepare the plant source, to include washing, pulverization, or any other necessary pre-treatment. Oftentimes, plants obtained through vendors have been prepared to some extent, and only require some degree of pulverization unless obtained in pre-powdered form. Pulverization is generally achieved by use of a household coffee grinder or a blender, though some materials must be prepared for pulverization by hand or any other method to avoid damaging the grinder. The process can be quite messy and painstaking, depending on the material an methods used.

====='''Defatting Concerns'''=====

Depending on the extraction methods used, foliage will require a defatting phase in order to better facilitate a proper extraction. This generally reguires that the material undergo extraction by acidic water prior to defatting. The product will be rendered water soluble and will remain in an aqueous phase as the solution is washed with an [[NPS]] to remove fats and oils.

==='''Vendor Considerations'''===

Though none of the plants containing DMT are illegal, the alkaloids contained within generally are. Vendors generally must take it upon themselves not to advertise the illicit contents of their products, otherwise risking putting themselves and their customers in jeopardy. Ordering these botanicals from across borders into countries where their contents are considered illegal is ill-advised but not necessarily risky, especially not if intended for legitimate use. Always be sure to research the reputation of a vendor prior to purchase, as the potentially taboo nature of their products may inspire unethical business practice, such as unreliable delivery or poor product quality; though such cases are not necessarily specifically limited specifically to these sorts of vendors, of course.

:[http://www.dmt-nexus.com/forum/default.aspx?g=topics&f=39 Suppliers Forum Topic]

==='''Considerations Regarding Cultivation'''===

Again, as these plants are usually no illegal, neither is their cultivation. Often these plants are only native to very specific regions, thus requiring very specific growing conditions, but many can be successfully cultivated indoors or seasonally outside of their native regions. Cultivation for the expressed or deduced purpose of refinery, use or sale of an illicit substance can result in harsh legal consequences, however.

:[http://www.dmt-nexus.com/forum/default.aspx?g=topics&f=38 The Ethnobotanical Garden Forum Topic]

=='''Extraction'''==

[[Image:800px-Dimethyltryptamine-3d-sticks.png|thumb]]

Extraction generally refers to the process of isolating a product from a source. The basic idea is to utilize the unique properties of the product—whether reactive, electromagnetic, or otherwise structural—to draw it out of the source and into a target solvent. To accomplish this the product must either be naturally soluble in the solvent or must undergo reaction to increase its solubility. The difference between a high and low yield is firstly determined by how much more soluble the product is in the target solvent, than in its source material or solution, and secondly by how thoroughly the target solvent is mechanically brought into contact with the target solvent; this is generally determined by a combination of the droplet size and dispersion of a solvent and/or the surface area exposure and structural consistency of the source material.

See also:
:[http://dmt-nexus.com/forum/default.aspx?g=posts&t=1085 DMT Extraction Overview]

{{:Straight-To-Base Extraction}}

{{:Acid/Base Extraction}}

{{:Dry Technique Extraction}}

{{:Limtek Extraction}}

=='''Crystallization'''==

[[Image:Dmtx400tt9.jpg|thumb]]

Crystallization is the process by which a product is isolated from a solvent. This is accomplished by either allowing the solvent to completely evaporate or by causing a precipitation to occur within the solvent, which can then be isolated from the solvent by several methods and then dried of any residual solvent.

=== Evaporation ===

In extraction, evaporation is the process by which a solvent disperses from its liquid form into the air as a vapor and a gas. When this occurs, the less volatile constituents of the solvent solution are left behind, and as such, it is a common method of isolating solutes from solvent.

Considerations:
* Many common solvents contain impurities which may not be quite as volatile as the pure solvent and may leave these impurities behind as a residue.
* Solvents often emit fumes and odors which may be hazardous to health, flammable, or may alarm those within proximity of the odor.
* Some solvents may require an excessive length of time to evaporate.
* Some solvents may absorb ambient moisture, resulting in a less expedient evaporation.
* Excessive air flow may cause the oxidization of the product.
* Solvent may become Trapped within the crystal structure of the product, resulting in a less solid and less pure product.

{{:Freeze Precipitation}}

=== Manual Crystallization ===

=== Salting ===

Salting is the process by which freebase DMT is reacted with an acid to create a salt form which is generally water-soluble. The natural form of DMT in botanical sources tends to be a salt-form, thus facilitating the simple aqueous extraction used to prepare DMT-containing brews. It is quite common to perform aqueous acid extractions from the material, however—whether for the purposes of a brew or for A/B extraction. The salt-form itself rarely lends itself to proper crystallization and usually can only be isolated as an oil unless very specific methods and materials are employed.

==== The Use of Fumaric Acid ====

Few salt-forms of DMT facilitate crystallization, but DMT fumarate currently stands alone as a solid crystalline salt-form of DMT.

{{:The FASA Method}}
{{:The FASW Method}}
{{:The FASIPA Method}}

==== Discussion of Other Salt-Forms ====

==== Further Elaboration and Technical Support ====

: [http://dmt-nexus.com/forum/default.aspx?g=topics&f=23 Forum on the Topic of FASA]

=='''Purification'''==

[[Image:Dmt crystal.jpg|thumb]]

The purification of DMT product has several purposes and is accomplished by several different methods, but all of them essentially involve the washing of product in some way or another. Purification either involves the isolation of product from unwanted impurities from the plant source or from the process of extraction, or it involves the isolation of product from active impurities which may or may not be collected after isolation.

==='''Recrystallization'''===

The general purpose of recrystallization is to crystallize the product in a fresh solvent after it has already been isolated from a solvent containing a considerable amount of impurities. This is meant to lessen the interference of impurities on the process of crystallization. Often this process results in more well-formed crystals with less discoloration. The advantage of this method of purification is that the solvent choice for recrystalliztion may be different and more suitable than that chosen for extraction.

{{:Washing Spice}}

==='''Freebase Conversion from Salt'''===

The methods used for converting crystalline salt-form DMT into freebase are not dissimilar from those used in extraction. The only significant difference between the processes is that the conversion involves far fewer impurities and less material than the extraction. Because of of this and the fact that it involves the isolation of the product from an acid, the conversion acts as a sort of purification method.

{{:Drytek Freebase Conversion of DMT}}

{{:Crystalline Freebase Conversion of DMT}}

{{:Nontoxic Freebase Conversion of DMT}}

{{:STB Freebase Conversion of DMT}}

====='''Further Elaboration and Technical Support'''=====

: [[:Category:Conversion Tek|Directory of Conversion Teks]]
: [http://www.dmt-nexus.com/forum/default.aspx?g=topics&f=23 Forum on the Topic of FASA]

=='''Administration'''==

{{:Leaf Enhancement}}

==='''Vaporization'''===

The vaporization method of administration pertains to the use of pure freebase product with no additional material. This method generally makes use of heating an apparatus that is intended to distribute the heat to the product until it reaches the point of vaporization and can be inhaled.

====='''Glass-Pipe Vaporizers'''=====

Glass-pipe vaporizers are glass pieces that are meant to be heated directly in order to indirectly disperse that heat into the product. The glass used must be thin enough for the heat to pass through its structure and potentially distribute the heat evenly. The piece must have a chamber within which the product will undergo vaporization. It must be assembled in a manner that will allow for air intake and output: The output being the inhalation nozzle, and the input being a sort of carb.

{{procedure
|the Improvisation of a Glass Pipe Vaporizer
|
}}

{{:The Machine}}

====='''Effective Use and Maintenance'''=====

As the term indicates, vaporizers are intended to vaporize, not to burn product, as such, the product should never come into contact with the flame or be overly heated to the point of burning. Generally, a vacuum must be generated in order to direct the heat through the product and to direct the vapor into the chamber. Which should not be allowed to sit for too long, as it may begin to precipitate within the chamber. Every toke should be held in the lungs as long as necessary for the vapor to be completely absorbed, as no vapor should be exhaled.

Heat-Source:
: Though many prefer a butane torch for expedient heating, and though many manners of vaporizer demand its use, a standard lighter will produce adequate heat for vaporization. A standard lighter is generally ideal for vaporizers that generate a strong enough vacuum to pull the flame toward the heat sink.

Common Methods of Inhalation:
* Some prefer to vaporize their entire dose before inhaling so as to administer one strong toke. This method can be quite harsh and difficult on the lungs and throat and may induce coughing. However, this is reportedly the most intense method of administration, almost always inducing a "breakthrough" if held in the lungs for adequate absorption.
* Others prefer to administer one dose within multiple tokes, which is reportedly slightly longer-lasting and much easier on the lungs and throat though possibly less intense. Usually the amount of tokes taken depends on the intended depth of the experience. In many cases, three is found to be more than adequate and four is said to be a "breakthrough" dose. Any subsequent tokes to the first toke must occur within the first minute, due to both tolerance and lack of motor skills building up rapidly

Cleaning the Apparatus:
* The apparatus used for vaporization can be cleaned using the same solvents used for extraction. However, volatility and toxicity concerns should be a strong consideration in choosing the proper solvent.
* It is preferable to choose a solvent that evaporates quickly and cleanly and able to dissolve a broad range of products, as oxidization is likely to have occurred.
* Residual solvent residue may be hazardous, as the user may inhale harmful fumes or potentially ignite the solvent.

: The residual product dissolved by the cleaning solvent may be salvaged by appropriate methods of crystallization. However, it is likely to contain a variety of inactive constituents, so proper purification measures would be advisable.

====='''Concerns Regarding the Experience'''=====

* The primary effects of smoked DMT, induced within minutes of administration, last for about 5-10 minutes and are characterized by strong visual hallucination, a strong psychedelic quality, and minor auditory hallucination, while the secondary effects of a much more mild character may last for up to an hour.
* Tolerance is reportedly induced rapidly and often dissipates rapidly, though repeated or high doses may induce a slightly longer term tolerance. Some believe it is best to wait at least one hour between doses.
* The experience of smoking DMT is said to be quite overwhelming. It is often necessary for the user to have a "sitter" nearby to tend to the smoking apparatus so as to not risk the possibility of the user damaging it or accidentally inflicting burns. It can also be temporarily debilitating, so the user may be advised to refrain from any physical activity.
* Set and setting are of the utmost importance, as the user is often rendered temporarily vulnerable and emotionally fragile. The user must determine the appropriate conditions in which administration is to take place but is advised to initially seek out a setting containing minimal stimuli.
* It may also behoove the user to seek out a more experienced sitter for guidance and support. Often this is unavailable, and as such, it would be more advisable for the user to perform the rite in solitude. An inexperienced sitter may inadvertently induce anxiety in the user out of negligence or unnecessary concern.

====='''Further Elaboration and Technical Support'''=====

: [http://forums.mycotopia.net/attachments/botanicals-cactus-misc-entheogens-psychedelics/67822d1195320961-dmt-pipe-83484machine.jpg "The Machine" Article from The Entheogen Review]

==='''Potentiation'''===

: The effects of DMT, as with most psychedelic substances, can be lengthened, strengthened, altered, or otherwise potentiated through the use of various psychoactive or bioactive compounds. The potentiation of DMT is actually the oldest method of administration, as its necessarily potentiated oral administration serves as the compound's longest known history of use. DMT is generally considered to be orally inactive without some form of potentiation, such as a harmaloid preparation. DMT's potentiation is not limited to oral use, however, as many of the same potentiating agents may be used in conjunction with vaporized or otherwise administered DMT.

{{:Harmaloids}}

{{:Jungle Spice}}

====='''Further Potentiation'''=====

=='''Appendices'''==

==='''Storage Concerns'''===
: DMT should be stored in a cool and dry place, preferably in a sealed container.

{{:DMT N-Oxide}}

=== Analogues ===

{{:5-MeO-DMT}}

{{:Bufotenine}}

=== References ===

{{Page Footer|The Nexian DMT Handbook|DMT}}

Bufotenin

2010-01-12T17:12:30Z

Narmz: /* Freebase Bufotenine Solubility */

<noinclude>{{Handbook Transclusion Header}}</noinclude>
<onlyinclude>
==== [[Bufotenine]] ====

==Freebase Bufotenine Solubility==
Acetone @ 20 C: soluble (5 g/100 ml) 
Chloroform @ 20 C: soluble 
Dichloromethane @ 20 C: soluble 
Dimethyl sulfoxide (DMSO) @ 20 C: soluble (6 g/100 ml) 
D-Limonene (Orange Oil) @ 20 C: insoluble 
D-Limonene (Orange Oil) @ 176 C: soluble (more than 1.7 g/100 ml) 
Ethanol @ 20 C: soluble 
Ether @ 20 C: soluble 
Ethyl acetate @ 20 C: soluble 
Heptane @ 20 C: insoluble 
Heptane with 40% MEK @ 20 C: soluble (0.53 g/100 ml) 
Heptane with 50% MEK @ 20 C: soluble (1.22 g/100 ml) 
IPA @ 20 C: soluble 
MEK @ 20 C: soluble 
Methanol @ 20 C: soluble 
Naphtha @ 20 C: insoluble 
Water @ 20 C: nearly insoluble in pure water (no acid or alkali added) 
Xylene @ 20 C: nearly insoluble (less than 0.03 g/100 ml) 
Xylene @ 144 C: soluble (1.5 g/100 ml) 

[http://dmt-nexus.com/forum/default.aspx?g=posts&t=3053 Sourced Post]

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{{Page Footer|Allies and Associated Alkaloids}}

Bufotenin

2010-01-12T17:10:35Z

Narmz: /* Bufotenin */

<noinclude>{{Handbook Transclusion Header}}</noinclude>
<onlyinclude>
==== [[Bufotenine]] ====

==Freebase Bufotenine Solubility==
Acetone @ 20 C: soluble (5 g/100 ml)
Chloroform @ 20 C: soluble
Dichloromethane @ 20 C: soluble
Dimethyl sulfoxide (DMSO) @ 20 C: soluble (6 g/100 ml)
D-Limonene (Orange Oil) @ 20 C: insoluble
D-Limonene (Orange Oil) @ 176 C: soluble (more than 1.7 g/100 ml)
Ethanol @ 20 C: soluble
Ether @ 20 C: soluble
Ethyl acetate @ 20 C: soluble
Heptane @ 20 C: insoluble
Heptane with 40% MEK @ 20 C: soluble (0.53 g/100 ml)
Heptane with 50% MEK @ 20 C: soluble (1.22 g/100 ml)
IPA @ 20 C: soluble
MEK @ 20 C: soluble
Methanol @ 20 C: soluble
Naphtha @ 20 C: insoluble
Water @ 20 C: nearly insoluble in pure water (no acid or alkali added)
Xylene @ 20 C: nearly insoluble (less than 0.03 g/100 ml)
Xylene @ 144 C: soluble (1.5 g/100 ml)

[http://dmt-nexus.com/forum/default.aspx?g=posts&t=3053 Sourced Post]

</onlyinclude>
{{Page Footer|Allies and Associated Alkaloids}}

DMT-Nexus Wiki - User contributions [en]

The Nexian DMT Handbook

Bufotenin

Bufotenin