{{ShowInfo|[[Image:Note_error.png]]|'''Note:'''|This page is a transcription of Kash's A/B Mescaline Extraction <ref>Kash's A/B Mescaline Extraction
Revision 1.0[https://www.dmt-nexus.me/forum/default.aspx?g=posts&t=43034]</ref>. The content is to remain accurate as such.}}

== Mescaline Extraction==

Here is a solid A/B tek on cacti for any who are interested, as well as a good method to obtain snow white crystals every time. Although SWIM came up with this tek on his own, there were contributing influences by House's resin extraction, dg's titration, and various postings. I like this method alot becuase the reagents are cheap, it is relatively easy, and doesnt take too long. It is VERY easy with fresh diced cacti but also fine using cacti powder. That said, let us begin.

== Procedure ==

<table cellpadding="10">
<tr>
<td valign="top">
{{ProcedureMain
|Mescaline HCl Extract
|Begin by adding 100g cacti powder or diced 12in cacti cutting(s) to a pot. Add 30g citric acid. If using cacti powder, add enough water to make it wet but not watery.
|To this add 2L H2O and simmer for 2hrs. Mix occasionally. Any cacti snot will boil off eventually and the tea should become nonviscous and watery.
|Filter out liquid from plant matter with a cloth filter and funnel, and add the liquid to another pot. Reduce this to a low volume by boiling. Add plant material back to original pot, cover with 2L H2O, and simmer for 1hr. Mix occasionally.
|Repeat step 3 atleast four to six times total until the liquid filtered out has very little color. Discard plant material after final time and reduce all the aqueous cacti extract to around 500 ml. This can be put in a glass pickle jar.
|Now it is time to basify. Mix 50g NaOH in 100ml H2O. It will get VERY hot, it is recommended to cool the mixing container while stirring with a cold water bath or under the faucet. Add the NaOH solution to the aqueous cacti extract.
|Add 200ml toluene (or xylene) and mix for 10-15 minutes. Let the mixture settle and use a hot water bath to seperate the layers from the emulsion if necessary. The layers will seperate quickly. Seperate the layers with a pipet, separatory funnel, or syringe. Save the toluene in another glass container and put basic aqueous cacti solution back in original container.
|Repeat previous step atleast 4 times total. Discard basic aqueous layer after, saving the toluene extract which contains the alkaloids.
|To the toluene extract add 100ml H2O. Add 0.5ml concentrated HCl to this and mix well for 5 minutes. Check the pH. If it is still basic (pH 9+) then add incriments of 0.5ml HCl with mixing and checking pH until it tests acidic (below pH 7). Continue mixing for 5 minutes after. Only one acid salting pull is necessary.
|Seperate layers, hot water bath may be necessary to seperate emulsion quickly. Filter and save acidic H2O layer and discard/recycle toluene. Evaporate the aqueous layer on a dish with aid of a fan and/or hot water bath. Never use direct heat it will scorch your product. Scrape up the crystals.
|Wash crystals with 50ml cold MEK (or anhydrous acetone, ethyl acetate). You will notice the solvent become discolored and the crystals become cleaner. Decant off the solvent carefully, leaving behind the cleaned crystals.

-You will usually be left with light tan Mescaline HCl if pachanoi was used. Yield will be largely dependent on how efficiently you performed the extraction, but most importantly the quality of cacti used in the beginning. 0.5-1.5% yield of dry starting weight is average, but can range anywhere from 0-3%. Enjoy!
}}

==== Procedure Notes ====
'''-Reducing the initial liquid:''' After each filtration the liquid is put into a pot, the "reducing pot". This can be boiled on high heat, just make sure it doesnt boil over. Once the liquid has boiled down to a low volume, stop reducing it when it becomes different in appearance and syrupy. Make sure not to reduce beyond this point and obviously dont boil it completely dry. Doing so will destroy alkaloids.

'''-Filtering plant material:''' This can be quite a frustrating step if working with cacti powder, though you get the hang of it over time. It is easiest to seperate out the liquid from cacti material by using cloth cut from a shirt and then pouring the sludge into a funnel through the cloth filter. Get a pair of rubber gloves and squeeze out the liquid from the filter. Dont squeeze too hard or cacti sludge will press through. Filtering is easiest to do while the liquid is hot and should be done atleast twice after each water boil. It also gets easier after each boil.

'''-Checking pH:''' The pH can be checked with pH paper by dipping it in the toluene/H2O solution while mixing. The paper must come in contact with the water layer as pH cannot be read from the nonpolar layer.

'''-Washing the crystals:''' It is important to wash your end crystals with a solvent like MEK or anhydrous acetone to remove impurities. The solvent dissolves resins and impurities, leaving behind cleaner non-sticky crystals.

== Additional Purification ==

{{ProcedureMain
|White Mescaline
{{ShowInfo/In Article|[[Image:Information.png]]|'''NOTE'''|
Doesnt change effects much, but increases purity and looks awful pretty! This procedure can be used to obtain pure white mescaline, and solvent ratios must be followed exactly. Solvent ratio affects the rate crystals precipitate out and more importantly their size. If they are too small/precipitate too quickly, they will be too fine to filter or decant liquid from. More nonpolar-> decreases solubility, more methanol-> increases solubility.
|0px
|
}}
|To a glass container with 1g cleaned Mescaline Hcl add 50ml H2O + 1ml HCl. Mix well until crystals completely dissolve.
|Add 50ml toluene.
|Mix 10g NaOH with 50ml water and add this to the solution, turning it basic. Mix well for 10 minutes.
|Seperate layers, saving toluene and discarding aqueous.
|To another glass container pour 40ml methanol (HEET antifreeze remover) and add 0.5g fumaric acid. Mix well until fumaric acid dissolves.
|Add the fumaric methanol to the toluene and mix it alittle. After a short time, the solution turns cloudy and crystals begin to form. Once crystals settle, mix it alittle more and pour into a dish.
|Very carefully decant by pouring off liquid and leaving behind white crystals. With no remaining liquid on the plate, let crystals dry and scrape up, yielding pure white Mescaline Fumarate. Enjoy!
}}

==== Additional Purification Notes ====

It is important to remove all the liquid to avoid fumaric acid contamination. Alternatively to decanting, you can filter if the crystals are big enough. This purification SWIM imagines could be used for 0-5g of mescaline before needing to change reagent amounts. It is also possible to use other solvent combinations and acids for precipitation, though this is left up to you. One could also get a pretty pure product if they simply did another hcl salting from the toluene instead of precipitation.
</td>

<td valign="top">
{{Materials_list
|
*100g cacti powder or 1-2 12in cutting(s).
|
*1L Toluene or Xylene
*50ml MEK, anhydrous acetone, or ethyl acetate
*H2O
*40ml Methanol (Optional)
|
*30g Citric Acid
*50g NaOH (Lye)
*Hcl (Muriatic Acid)
*0.5g Fumaric Acid (Optional)
|
*Pots
*Glassware
*1L glass pickle jar
*Evaporating dish/bowl
*Stir utensils
*Pipet/syringe/separatory funnel
*Coffee filters and funnel
*Cloth filters (shirt)
*Rubber gloves
{{ShowInfo/In Article|[[Image:Alert.png]]|'''NOTE'''| <small>All materials contained in this list can be found at hardware stores, grocery stores, or online by every-day consumers.</small>
|0px
|
}}
}}
</td>
</tr>
</table>

== Dosage Information ==

The good thing about making a purified mescaline extract is that you can easily measure exactly how much you are consuming and the experience is more clear. Mescaline is a very "friendly" feeling substance that is probably the least edgy of the traditional psychedelics imho. The experience is usually associated with euphoria, brightened colors, increased sociability, altered thinking, and morphing rainbows/patterns/environment. While dosages vary for everyone, I believe this to be a fairly accurate scale of dosage for the extraction procedure:

* '''Threshold''' <100 mg
* '''Light''' 100 - 200 mg
* '''Common''' 200 - 400 mg
* '''Strong''' 400 - 600 mg
* '''Heavy''' >600 mg

== Pictures ==
[[File:M_hcl_1_temp.jpg‎]][[File:M_fumarate_2-temp.jpg]][[File:M_fumarate_4.jpg]]

== Reference ==
<references/>

[[Category:Extraction Tek]]
[[Category:Mescaline]]

Kash's A/B Mescaline Extraction

2013-05-15T03:10:29Z

Kash: /* Procedure */

{{ShowInfo|[[Image:Note_error.png]]|'''Note:'''|This page is a transcription of Kash's A/B Mescaline Extraction <ref>Kash's A/B Mescaline Extraction
Revision 1.0[https://www.dmt-nexus.me/forum/default.aspx?g=posts&t=43034]</ref>. The content is to remain accurate as such.}}

== Mescaline Extraction==

Here is a solid A/B tek on cacti for any who are interested, as well as a good method to obtain snow white crystals every time. Although SWIM came up with this tek on his own, there were contributing influences by House's resin extraction, dg's titration, and various postings. I like this method alot becuase the reagents are cheap, it is relatively easy, and doesnt take too long. It is VERY easy with fresh diced cacti but also fine using cacti powder. That said, let us begin.

== Procedure ==

<table cellpadding="10">
<tr>
<td valign="top">
{{ProcedureMain
|Mescaline HCl Extract
|Begin by adding 100g cacti powder or diced 12in cacti cutting(s) to a pot. Add 30g citric acid. If using cacti powder, add enough water to make it wet but not watery.
|To this add 2L H2O and simmer for 2hrs. Mix occasionally. Any cacti snot will boil off eventually and the tea should become nonviscous and watery.
|Filter out liquid from plant matter with a cloth filter and funnel, and add the liquid to another pot. Reduce this to a low volume by boiling. Add plant material back to original pot, cover with 2L H2O, and simmer for 1hr. Mix occasionally.
|Repeat step 3 atleast four to six times total until the liquid filtered out has very little color. Discard plant material after final time and reduce all the aqueous cacti extract to around 500 ml. This can be put in a glass pickle jar.
|Now it is time to basify. Mix 50g NaOH in 100ml H2O. It will get VERY hot, it is recommended to cool the mixing container while stirring with a cold water bath or under the faucet. Add the NaOH solution to the aqueous cacti extract.
|Add 200ml toluene (or xylene) and mix for 10-15 minutes. Let the mixture settle and use a hot water bath to seperate the layers from the emulsion if necessary. The layers will seperate quickly. Seperate the layers with a pipet, separatory funnel, or syringe. Save the toluene in another glass container and put basic aqueous cacti solution back in original container.
|Repeat previous step atleast 4 times total. Discard basic aqueous layer after, saving the toluene extract which contains the alkaloids.
|To the toluene extract add 100ml H2O. Add 0.5ml concentrated HCl to this and mix well for 5 minutes. Check the pH. If it is still basic (pH 9+) then add incriments of 0.5ml HCl with mixing and checking pH until it tests acidic (below pH 7). Only one acid salting pull is necessary.
|Seperate layers, hot water bath may be necessary to seperate emulsion quickly. Filter and save acidic H2O layer and discard/recycle toluene. Evaporate the aqueous layer on a dish with aid of a fan and/or hot water bath. Never use direct heat it will scorch your product. Scrape up the crystals.
|Wash crystals with 50ml cold MEK (or anhydrous acetone, ethyl acetate). You will notice the solvent become discolored and the crystals become cleaner. Decant off the solvent carefully, leaving behind the cleaned crystals.

-You will usually be left with light tan Mescaline HCl if pachanoi was used. Yield will be largely dependent on how efficiently you performed the extraction, but most importantly the quality of cacti used in the beginning. 0.5-1.5% yield of dry starting weight is average, but can range anywhere from 0-3%. Enjoy!
}}

==== Procedure Notes ====
'''-Reducing the initial liquid:''' After each filtration the liquid is put into a pot, the "reducing pot". This can be boiled on high heat, just make sure it doesnt boil over. Once the liquid has boiled down to a low volume, stop reducing it when it becomes different in appearance and syrupy. Make sure not to reduce beyond this point and obviously dont boil it completely dry. Doing so will destroy alkaloids.

'''-Filtering plant material:''' This can be quite a frustrating step if working with cacti powder, though you get the hang of it over time. It is easiest to seperate out the liquid from cacti material by using cloth cut from a shirt and then pouring the sludge into a funnel through the cloth filter. Get a pair of rubber gloves and squeeze out the liquid from the filter. Dont squeeze too hard or cacti sludge will press through. Filtering is easiest to do while the liquid is hot and should be done atleast twice after each water boil. It also gets easier after each boil.

'''-Checking pH:''' The pH can be checked with pH paper by dipping it in the toluene/H2O solution while mixing. The paper must come in contact with the water layer as pH cannot be read from the nonpolar layer.

'''-Washing the crystals:''' It is important to wash your end crystals with a solvent like MEK or anhydrous acetone to remove impurities. The solvent dissolves resins and impurities, leaving behind cleaner non-sticky crystals.

== Additional Purification ==

{{ProcedureMain
|White Mescaline
{{ShowInfo/In Article|[[Image:Information.png]]|'''NOTE'''|
Doesnt change effects much, but increases purity and looks awful pretty! This procedure can be used to obtain pure white mescaline, and solvent ratios must be followed exactly. Solvent ratio affects the rate crystals precipitate out and more importantly their size. If they are too small/precipitate too quickly, they will be too fine to filter or decant liquid from. More nonpolar-> decreases solubility, more methanol-> increases solubility.
|0px
|
}}
|To a glass container with 1g cleaned Mescaline Hcl add 50ml H2O + 1ml HCl. Mix well until crystals completely dissolve.
|Add 50ml toluene.
|Mix 10g NaOH with 50ml water and add this to the solution, turning it basic. Mix well for 10 minutes.
|Seperate layers, saving toluene and discarding aqueous.
|To another glass container pour 40ml methanol (HEET antifreeze remover) and add 0.5g fumaric acid. Mix well until fumaric acid dissolves.
|Add the fumaric methanol to the toluene and mix it alittle. After a short time, the solution turns cloudy and crystals begin to form. Once crystals settle, mix it alittle more and pour into a dish.
|Very carefully decant by pouring off liquid and leaving behind white crystals. With no remaining liquid on the plate, let crystals dry and scrape up, yielding pure white Mescaline Fumarate. Enjoy!
}}

==== Additional Purification Notes ====

It is important to remove all the liquid to avoid fumaric acid contamination. Alternatively to decanting, you can filter if the crystals are big enough. This purification SWIM imagines could be used for 0-5g of mescaline before needing to change reagent amounts. It is also possible to use other solvent combinations and acids for precipitation, though this is left up to you. One could also get a pretty pure product if they simply did another hcl salting from the toluene instead of precipitation.
</td>

<td valign="top">
{{Materials_list
|
*100g cacti powder or 1-2 12in cutting(s).
|
*1L Toluene or Xylene
*50ml MEK, anhydrous acetone, or ethyl acetate
*H2O
*40ml Methanol (Optional)
|
*30g Citric Acid
*50g NaOH (Lye)
*Hcl (Muriatic Acid)
*0.5g Fumaric Acid (Optional)
|
*Pots
*Glassware
*1L glass pickle jar
*Evaporating dish/bowl
*Stir utensils
*Pipet/syringe/separatory funnel
*Coffee filters and funnel
*Cloth filters (shirt)
*Rubber gloves
{{ShowInfo/In Article|[[Image:Alert.png]]|'''NOTE'''| <small>All materials contained in this list can be found at hardware stores, grocery stores, or online by every-day consumers.</small>
|0px
|
}}
}}
</td>
</tr>
</table>

== Dosage Information ==

The good thing about making a purified mescaline extract is that you can easily measure exactly how much you are consuming and the experience is more clear. Mescaline is a very "friendly" feeling substance that is probably the least edgy of the traditional psychedelics imho. The experience is usually associated with euphoria, brightened colors, increased sociability, altered thinking, and morphing rainbows/patterns/environment. While dosages vary for everyone, I believe this to be a fairly accurate scale of dosage for the extraction procedure:

* '''Threshold''' <100 mg
* '''Light''' 100 - 200 mg
* '''Common''' 200 - 400 mg
* '''Strong''' 400 - 600 mg
* '''Heavy''' >600 mg

== Pictures ==
[[File:M_hcl_1_temp.jpg‎]][[File:M_fumarate_2-temp.jpg]][[File:M_fumarate_4.jpg]]

== Reference ==
<references/>

[[Category:Extraction Tek]]
[[Category:Mescaline]]

File:M fumarate 2-temp.jpg

2013-05-15T01:53:33Z

Kash: uploaded a new version of "File:M fumarate 2-temp.jpg"

Kash's A/B Mescaline Extraction

2013-05-15T01:53:11Z

Kash: /* Pictures */

{{ShowInfo|[[Image:Note_error.png]]|'''Note:'''|This page is a transcription of Kash's A/B Mescaline Extraction <ref>Kash's A/B Mescaline Extraction
Revision 1.0[https://www.dmt-nexus.me/forum/default.aspx?g=posts&t=43034]</ref>. The content is to remain accurate as such.}}

== Mescaline Extraction==

Here is a solid A/B tek on cacti for any who are interested, as well as a good method to obtain snow white crystals every time. Although SWIM came up with this tek on his own, there were contributing influences by House's resin extraction, dg's titration, and various postings. I like this method alot becuase the reagents are cheap, it is relatively easy, and doesnt take too long. It is VERY easy with fresh diced cacti but also fine using cacti powder. That said, let us begin.

== Procedure ==

<table cellpadding="10">
<tr>
<td valign="top">
{{ProcedureMain
|Mescaline HCl Extract
|Begin by adding 100g cacti powder or diced 12in cacti cutting(s) to a pot. Add 30g citric acid. If using cacti powder, add enough water to make it wet but not watery.
|To this add 2L H2O and simmer for 2hrs. Any cacti snot will boil off eventually and the tea should become nonviscous and watery.
|Filter out liquid from plant matter with a cloth filter and funnel, and add the liquid to another pot. Reduce this to a low volume by boiling. Add plant material back to original pot, cover with 2L H2O, and simmer for 1hr.
|Repeat step 3 atleast four to six times total until the liquid filtered out has very little color. Discard plant material after final time and reduce all the aqueous cacti extract to around 500 ml. This can be put in a glass pickle jar.
|Now it is time to basify. Mix 50g NaOH in 100ml H2O. It will get VERY hot, it is recommended to cool the mixing container while stirring with a cold water bath or under the faucet. Add the NaOH solution to the aqueous cacti extract.
|Add 200ml toluene (or xylene) and mix for 10-15 minutes. Let the mixture settle and use a hot water bath to seperate the layers from the emulsion if necessary. The layers will seperate quickly. Seperate the layers with a pipet, separatory funnel, or syringe. Save the toluene in another glass container and put basic aqueous cacti solution back in original container.
|Repeat previous step atleast 4 times total. Discard basic aqueous layer after, saving the toluene extract which contains the alkaloids.
|To the toluene extract add 100ml H2O. Add 0.5ml concentrated HCl to this and mix well for 5 minutes. Check the pH. If it is still basic (pH 9+) then add incriments of 0.5ml HCl with mixing and checking pH until it tests acidic (below pH 7). Only one acid salting pull is necessary.
|Seperate layers, hot water bath may be necessary to seperate emulsion quickly. Filter and save acidic H2O layer and discard/recycle toluene. Evaporate the aqueous layer on a dish with aid of a fan and/or hot water bath. Never use direct heat it will scorch your product. Scrape up the crystals.
|Wash crystals with 50ml cold MEK (or anhydrous acetone, ethyl acetate). You will notice the solvent become discolored and the crystals become cleaner. Decant off the solvent carefully, leaving behind the cleaned crystals.

-You will usually be left with light tan Mescaline HCl if pachanoi was used. Yield will be largely dependent on how efficiently you performed the extraction, but most importantly the quality of cacti used in the beginning. 0.5-1.5% yield of dry starting weight is average, but can range anywhere from 0-3%. Enjoy!
}}

==== Procedure Notes ====
'''-Reducing the initial liquid:''' After each filtration the liquid is put into a pot, the "reducing pot". This can be boiled on high heat, just make sure it doesnt boil over. Once the liquid has boiled down to a low volume, stop reducing it when it becomes different in appearance and syrupy. Make sure not to reduce beyond this point and obviously dont boil it completely dry. Doing so will destroy alkaloids.

'''-Filtering plant material:''' This can be quite a frustrating step if working with cacti powder, though you get the hang of it over time. It is easiest to seperate out the liquid from cacti material by using cloth cut from a shirt and then pouring the sludge into a funnel through the cloth filter. Get a pair of rubber gloves and squeeze out the liquid from the filter. Dont squeeze too hard or cacti sludge will press through. Filtering is easiest to do while the liquid is hot and should be done atleast twice after each water boil. It also gets easier after each boil.

'''-Checking pH:''' The pH can be checked with pH paper by dipping it in the toluene/H2O solution while mixing. The paper must come in contact with the water layer as pH cannot be read from the nonpolar layer.

'''-Washing the crystals:''' It is important to wash your end crystals with a solvent like MEK or anhydrous acetone to remove impurities. The solvent dissolves resins and impurities, leaving behind cleaner non-sticky crystals.

== Additional Purification ==

{{ProcedureMain
|White Mescaline
{{ShowInfo/In Article|[[Image:Information.png]]|'''NOTE'''|
Doesnt change effects much, but increases purity and looks awful pretty! This procedure can be used to obtain pure white mescaline, and solvent ratios must be followed exactly. Solvent ratio affects the rate crystals precipitate out and more importantly their size. If they are too small/precipitate too quickly, they will be too fine to filter or decant liquid from. More nonpolar-> decreases solubility, more methanol-> increases solubility.
|0px
|
}}
|To a glass container with 1g cleaned Mescaline Hcl add 50ml H2O + 1ml HCl. Mix well until crystals completely dissolve.
|Add 50ml toluene.
|Mix 10g NaOH with 50ml water and add this to the solution, turning it basic. Mix well for 10 minutes.
|Seperate layers, saving toluene and discarding aqueous.
|To another glass container pour 40ml methanol (HEET antifreeze remover) and add 0.5g fumaric acid. Mix well until fumaric acid dissolves.
|Add the fumaric methanol to the toluene and mix it alittle. After a short time, the solution turns cloudy and crystals begin to form. Once crystals settle, mix it alittle more and pour into a dish.
|Very carefully decant by pouring off liquid and leaving behind white crystals. With no remaining liquid on the plate, let crystals dry and scrape up, yielding pure white Mescaline Fumarate. Enjoy!
}}

==== Additional Purification Notes ====

It is important to remove all the liquid to avoid fumaric acid contamination. Alternatively to decanting, you can filter if the crystals are big enough. This purification SWIM imagines could be used for 0-5g of mescaline before needing to change reagent amounts. It is also possible to use other solvent combinations and acids for precipitation, though this is left up to you. One could also get a pretty pure product if they simply did another hcl salting from the toluene instead of precipitation.
</td>

<td valign="top">
{{Materials_list
|
*100g cacti powder or 1-2 12in cutting(s).
|
*1L Toluene or Xylene
*50ml MEK, anhydrous acetone, or ethyl acetate
*H2O
*40ml Methanol (Optional)
|
*30g Citric Acid
*50g NaOH (Lye)
*Hcl (Muriatic Acid)
*0.5g Fumaric Acid (Optional)
|
*Pots
*Glassware
*1L glass pickle jar
*Evaporating dish/bowl
*Stir utensils
*Pipet/syringe/separatory funnel
*Coffee filters and funnel
*Cloth filters (shirt)
*Rubber gloves
{{ShowInfo/In Article|[[Image:Alert.png]]|'''NOTE'''| <small>All materials contained in this list can be found at hardware stores, grocery stores, or online by every-day consumers.</small>
|0px
|
}}
}}
</td>
</tr>
</table>

== Dosage Information ==

The good thing about making a purified mescaline extract is that you can easily measure exactly how much you are consuming and the experience is more clear. Mescaline is a very "friendly" feeling substance that is probably the least edgy of the traditional psychedelics imho. The experience is usually associated with euphoria, brightened colors, increased sociability, altered thinking, and morphing rainbows/patterns/environment. While dosages vary for everyone, I believe this to be a fairly accurate scale of dosage for the extraction procedure:

* '''Threshold''' <100 mg
* '''Light''' 100 - 200 mg
* '''Common''' 200 - 400 mg
* '''Strong''' 400 - 600 mg
* '''Heavy''' >600 mg

== Pictures ==
[[File:M_hcl_1_temp.jpg‎]][[File:M_fumarate_2-temp.jpg]][[File:M_fumarate_4.jpg]]

== Reference ==
<references/>

[[Category:Extraction Tek]]
[[Category:Mescaline]]

File:M fumarate 4.jpg

2013-05-15T01:52:20Z

Kash: uploaded a new version of "File:M fumarate 4.jpg"

File:M fumarate 4.jpg

2013-05-15T01:49:09Z

Kash:

File:M fumarate 2-temp.jpg

2013-05-15T01:48:23Z

Kash:

2013-02-19T03:23:59Z

Kash: /* Comments */

{{ShowInfo|[[Image:Note_error.png]]|'''Note:'''|This page is a transcription of Kash's Advanced LSA Extraction tek<ref>Kash's Advanced LSA Extraction tek
Revision 1.3[https://www.dmt-nexus.me/forum/default.aspx?g=posts&m=376477&#post376477]</ref>. The content is to remain accurate as such.}}

== Pure LSA Extraction, Visually Active with no Nausea or Bodyload ==

=== Procedure ===

<table cellpadding="10">
<tr>
<td valign="top">
{{ProcedureMain
|Clean Liquid LSA Extract
|Begin by preparing anhydrous acetone reagent. Do this by microwaving 1/2 cup of MgSO4 for a few minutes until all the water in it boils away. Take the dry MgSO4 and add it to a glass of 300ml acetone, mixing well for 15 minutes. Filter out the solids with a coffee filter and you now have 300 ml anhydrous acetone.
|Pulverize your seeds into a powder using a coffee grinder or your method of choice.
|Thoroughly mix in a glass the seed powder and 100 ml of anhydrous acetone. Mix frequently for 2-3 hrs, the more mixing the better.
|After this, filter solution and set aside acetone extract in a glass and cover with plastic wrap to prevent early evaporation. Put seed mush back into the original cup and cover with 100 ml new anhydrous acetone.
|Repeat steps 3-4 two more times so you have 3 extractions. After third extraction, discard seed mush and combine the extracts into an evaporation dish/bowl. Set up a fan blowing on the extraction to speed evaporation. Doesn't take too long. Evap to dryness, making sure there is no more acetone smell.
|Mix in a glass 100 ml distilled water and a pinch of citric acid (pH 3-5). Add to the dry crude LSA extract and mix well for 10 minutes. Not everything will dissolve. Filter out the solids. There should now be 100 ml of aqueous LSA citrate.
|Defat this solution with 50 ml naptha, mixing well for 10 minutes. Seperate layers with a 10 ml syringe and discard naptha. Repeat. Make sure the second time that there is no remaining naptha floating in your LSA extract after defat.
|Now its time to freebase the LSA so it can be extracted from the water layer. Add a small amount of ammonia (around 1 ml) to solution until it changes to a light yellow color. PH should be roughly 8.5-9.5.
|Quickly add 50 ml toluene or DCM to the solution and mix well for 15-20 minutes. After, seperate the layers with syringe and set aside the 50 ml of toluene or DCM in a glass. Repeat this step 1 or 2 more times depending on how scrupulous you want to be. Afterwards, discard your yellow/green water layer.
|Now with your combined toluene or DCM extracts, set them to evaporate in an evaporation dish/bowl with the aid of a fan. This again shouldnt take too long, and you end up with a pure white crystal residue once dry. This could be consumed, but will oxidize pretty quickly over a few days if left out of solution.
|Once your pure extract is dry and there is absolutely no smell of solvent in your evap dish, add 10 ml distilled H2O and 5 ml 75% drinkable ethanol. Sprinkle in a pinch of tartaric acid and mix thoroughly for 10 minutes. Filter this, and store in a vial away from heat and light.
}}

==== Comments ====
This product of clean liquid LSA extract glows bright blue under black light and '''MUST BE COMBINED WITH A SMALL AMOUNT OF PEPPERMINT OIL''' 20 minutes before consuming for an amazing psychedlic experience. If solution turns milky after peppermint oil addition, add alittle alcohol to increase solubility. Inferior extraction recipes can leave you with stomach cramps and vasoconstriction, not to mention nausea, and the effects may not even be very impressive. A PURE clean LSA extraction using this tek however... Absolutely no nausea or bodyload. It is a euphoric feeling psychedelic similar to LSD lasting about 6-9hrs, with very active visuals made up of colors, vibrant pulsing tracers, flashy looking stars and symbols, and intricate geometric patterns. Good luck to all and I hope this tek creates many memorable experiences.
</td>
<td valign="top">
{{Materials_list
|
* 100 HBWR seeds Hawaiian Strain. Never buy Ghana strain. (Morning Glory seeds may be substituted in as well)
|
* 300 ml acetone.
* 110 ml distilled H2O.
* 100 ml naptha.
* 100 ml toluene or DCM.
* 5 ml drinkable ethanol (everclear works well).
|
* 1/2 cup Epsom Salt (MgSO4).
* 1 pinch citric acid.
* 1 ml ammonia.
* 1 pinch tartaric acid.
|
* Coffee filters and funnel.
* Evaporating dish/bowl.
* Syringe 10 ml.
* Stir stick.
* Glassware.
* Vial 15ml or more (preferably amberglass).
{{ShowInfo/In Article|[[Image:Alert.png]]|'''NOTE'''| <small>All materials contained in this list can be found at hardware stores, grocery stores, or online by every-day consumers.</small>
|0px
|
}}
}}
</td>
</tr>
</table>

=== Dosage Information ===

It is difficult to accurately measure doses of LSA extract, since potency can vary. In general you can get a rough idea by comparing the ratio of seeds to liquid extract volume. A few drops of peppermint oil should be added to the LSA extract 10 minutes prior to comsuming. I believe this to be a fairly accurate scale of dosage for this extraction procedure:

* '''Threshold''' < 10 seeds worth
* '''Light''' 10-19 seeds worth
* '''Common''' 20-34 seeds worth
* '''Strong''' 35-50 seeds worth
* '''Heavy''' > 50 seeds worth

=== Pictures ===

Here's a picture of final evap and a vial of clear LSA extract under black light.

[[File:P8150039.jpg]]
[[File:P8080036.jpg]]

== Reference ==
<references/>

[[Category:Extraction Tek]]
[[Category:LSA]]

Kash's Advanced LSA Extraction

2013-02-13T08:45:06Z

Kash:

{{ShowInfo|[[Image:Note_error.png]]|'''Note:'''|This page is a transcription of Kash's Advanced LSA Extraction tek<ref>Kash's Advanced LSA Extraction tek
Revision 1.3[https://www.dmt-nexus.me/forum/default.aspx?g=posts&m=376477&#post376477]</ref>. The content is to remain accurate as such.}}

== Pure LSA Extraction, Visually Active with no Nausea or Bodyload ==

=== Procedure ===

<table cellpadding="10">
<tr>
<td valign="top">
{{ProcedureMain
|Clean Liquid LSA Extract
|Begin by preparing anhydrous acetone reagent. Do this by microwaving 1/2 cup of MgSO4 for a few minutes until all the water in it boils away. Take the dry MgSO4 and add it to a glass of 300ml acetone, mixing well for 15 minutes. Filter out the solids with a coffee filter and you now have 300 ml anhydrous acetone.
|Pulverize your seeds into a powder using a coffee grinder or your method of choice.
|Thoroughly mix in a glass the seed powder and 100 ml of anhydrous acetone. Mix frequently for 2-3 hrs, the more mixing the better.
|After this, filter solution and set aside acetone extract in a glass and cover with plastic wrap to prevent early evaporation. Put seed mush back into the original cup and cover with 100 ml new anhydrous acetone.
|Repeat steps 3-4 two more times so you have 3 extractions. After third extraction, discard seed mush and combine the extracts into an evaporation dish/bowl. Set up a fan blowing on the extraction to speed evaporation. Doesn't take too long. Evap to dryness, making sure there is no more acetone smell.
|Mix in a glass 100 ml distilled water and a pinch of citric acid (pH 3-5). Add to the dry crude LSA extract and mix well for 10 minutes. Not everything will dissolve. Filter out the solids. There should now be 100 ml of aqueous LSA citrate.
|Defat this solution with 50 ml naptha, mixing well for 10 minutes. Seperate layers with a 10 ml syringe and discard naptha. Repeat. Make sure the second time that there is no remaining naptha floating in your LSA extract after defat.
|Now its time to freebase the LSA so it can be extracted from the water layer. Add a small amount of ammonia (around 1 ml) to solution until it changes to a light yellow color. PH should be roughly 8.5-9.5.
|Quickly add 50 ml toluene or DCM to the solution and mix well for 15-20 minutes. After, seperate the layers with syringe and set aside the 50 ml of toluene or DCM in a glass. Repeat this step 1 or 2 more times depending on how scrupulous you want to be. Afterwards, discard your yellow/green water layer.
|Now with your combined toluene or DCM extracts, set them to evaporate in an evaporation dish/bowl with the aid of a fan. This again shouldnt take too long, and you end up with a pure white crystal residue once dry. This could be consumed, but will oxidize pretty quickly over a few days if left out of solution.
|Once your pure extract is dry and there is absolutely no smell of solvent in your evap dish, add 10 ml distilled H2O and 5 ml 75% drinkable ethanol. Sprinkle in a pinch of tartaric acid and mix thoroughly for 10 minutes. Filter this, and store in a vial away from heat and light.
}}

==== Comments ====
This product of clean liquid LSA extract glows bright blue under black light and '''MUST BE COMBINED WITH A SMALL AMOUNT OF PEPPERMINT OIL''' 10 minutes before consuming for an amazing psychedlic experience. If solution turns milky after peppermint oil addition, add alittle alcohol to increase solubility. Inferior extraction recipes can leave you with stomach cramps and vasoconstriction, not to mention nausea, and the effects may not even be very impressive. A PURE clean LSA extraction using this tek however... Absolutely no nausea or bodyload. It is a euphoric feeling psychedelic similar to LSD lasting about 6-9hrs, with very active visuals made up of colors, vibrant pulsing tracers, flashy looking stars and symbols, and intricate geometric patterns. Good luck to all and I hope this tek creates many memorable experiences.
</td>
<td valign="top">
{{Materials_list
|
* 100 HBWR seeds Hawaiian Strain. Never buy Ghana strain. (Morning Glory seeds may be substituted in as well)
|
* 300 ml acetone.
* 110 ml distilled H2O.
* 100 ml naptha.
* 100 ml toluene or DCM.
* 5 ml drinkable ethanol (everclear works well).
|
* 1/2 cup Epsom Salt (MgSO4).
* 1 pinch citric acid.
* 1 ml ammonia.
* 1 pinch tartaric acid.
|
* Coffee filters and funnel.
* Evaporating dish/bowl.
* Syringe 10 ml.
* Stir stick.
* Glassware.
* Vial 15ml or more (preferably amberglass).
{{ShowInfo/In Article|[[Image:Alert.png]]|'''NOTE'''| <small>All materials contained in this list can be found at hardware stores, grocery stores, or online by every-day consumers.</small>
|0px
|
}}
}}
</td>
</tr>
</table>

=== Dosage Information ===

It is difficult to accurately measure doses of LSA extract, since potency can vary. In general you can get a rough idea by comparing the ratio of seeds to liquid extract volume. A few drops of peppermint oil should be added to the LSA extract 10 minutes prior to comsuming. I believe this to be a fairly accurate scale of dosage for this extraction procedure:

* '''Threshold''' < 10 seeds worth
* '''Light''' 10-19 seeds worth
* '''Common''' 20-34 seeds worth
* '''Strong''' 35-50 seeds worth
* '''Heavy''' > 50 seeds worth

=== Pictures ===

Here's a picture of final evap and a vial of clear LSA extract under black light.

[[File:P8150039.jpg]]
[[File:P8080036.jpg]]

== Reference ==
<references/>

[[Category:Extraction Tek]]
[[Category:LSA]]